Supporting Information
1H and 13C NMR spectra are provided in Supporting Information File 1. Synthetic procedures for the syntheses of compounds 2, 3, 10, 11, 13, 14, 17–19, and 21.
| Supporting Information File 1: Synthetic procedures and NMR spectra of the most typical compounds. | ||
| Format: PDF | Size: 938.8 KB | Download |
Cite the Following Article
Syntheses of 15N-labeled pre-queuosine nucleobase derivatives
Jasmin Levic and Ronald Micura
Beilstein J. Org. Chem. 2014, 10, 1914–1918.
https://doi.org/10.3762/bjoc.10.199
How to Cite
Levic, J.; Micura, R. Beilstein J. Org. Chem. 2014, 10, 1914–1918. doi:10.3762/bjoc.10.199
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Scholarly Works
- Stanishevskiy, V. V.; Shestakova, A. K.; Chertkov, V. A. Analysis of 2D Maps Based on Similarity in DFT-Calculated vs Experimental 13C–15N Spin Couplings for a Representative Sample of Conformationally Rigid and Structurally Fixed Nitrogen-Containing Organic Compounds. Applied Magnetic Resonance 2022, 53, 1693–1713. doi:10.1007/s00723-022-01503-w
- Flemmich, L.; Moreno, S.; Micura, R. Synthesis of O6-alkylated preQ1 derivatives. Beilstein journal of organic chemistry 2021, 17, 2295–2301. doi:10.3762/bjoc.17.147
- Neuner, E.; Frener, M.; Lusser, A.; Micura, R. Superior cellular activities of azido- over amino-functionalized ligands for engineered preQ1 riboswitches in E.coli. RNA biology 2018, 15, 1376–1383. doi:10.1080/15476286.2018.1534526
- Neuner, S.; Santner, T.; Kreutz, C.; Micura, R. The “Speedy” Synthesis of Atom-Specific 15N Imino/Amido-Labeled RNA. Chemistry (Weinheim an der Bergstrasse, Germany) 2015, 21, 11634–11643. doi:10.1002/chem.201501275
- Moschen, T.; Wunderlich, C. H.; Spitzer, R.; Levic, J.; Micura, R.; Tollinger, M.; Kreutz, C. Ligand‐Detected Relaxation Dispersion NMR Spectroscopy: Dynamics of preQ1–RNA Binding. Angewandte Chemie 2014, 127, 570–573. doi:10.1002/ange.201409779
- Moschen, T.; Wunderlich, C. H.; Spitzer, R.; Levic, J.; Micura, R.; Tollinger, M.; Kreutz, C. Ligand-Detected Relaxation Dispersion NMR Spectroscopy: Dynamics of preQ1–RNA Binding. Angewandte Chemie (International ed. in English) 2014, 54, 560–563. doi:10.1002/anie.201409779
