One-pot multistep mechanochemical synthesis of fluorinated pyrazolones

Scholarly Works

• Adak, L.; Roy, K.; Saha, A.; Sahoo, S.; Banerjee, S.; Mukhopadhyay, C. D.; Banerjee, S. Reaction under Ball-Milling: Solvent- and Metal-Free One-Pot Diastereoselective Synthesis of Tetrahydroquinoline Derivatives as Potential Antibacterial and Anticancer Agents. Synlett 2024. doi:10.1055/a-2378-1847
• Stankovianska, K.; Némethová, V.; Peňaška, T.; Borko, J.; Mečiarová, M.; Šebesta, R. Fluorinated Chiral Pyrans Obtained via Mechanochemical Organocatalytic Michael/oxa‐Michael Cascade. European Journal of Organic Chemistry 2024. doi:10.1002/ejoc.202400588
• Panda, S. P.; Dash, R.; Hota, S. K.; Murarka, S. Photodecarboxylative Radical Cascade Involving N-(Acyloxy)phthalimides for the Synthesis of Pyrazolones. Organic letters 2024, 26, 3667–3672. doi:10.1021/acs.orglett.4c01176
• Roy, R.; Kumar, R.; Ansari, M. N.; Deshmukh, G. S.; Rai, A. K.; Tripathi, G.; Kumar, A. Energy-efficient Approach to Multicomponent Reaction for the Synthesis of Therapeutically Relevant Heterocycles. Current Organic Chemistry 2023, 27, 1762–1778. doi:10.2174/0113852728264863231017071522
• Borodkin, G. I. Mechanochemical synthesis of organohalogen compounds: a synthetic chemist's view. Russian Chemical Reviews 2023, 92, RCR5091. doi:10.59761/rcr5091
• Debnath, S.; Chauhan, S.; Kumara Swamy, K. C. (3 + 3) Annulation of acetoxy allenoates with enolisable carbonyl substrates leading to fused pyrans. Organic & biomolecular chemistry 2023, 21, 5021–5032. doi:10.1039/d3ob00597f
• Roy, K.; Sahoo, S.; Saha, A.; Adak, L. Ball Milling in Organic Transformations. Current Organic Chemistry 2023, 27, 153–165. doi:10.2174/1385272827666221223143844
• Lopat'eva, E. R.; Budnikov, A. S.; Krylov, I. B.; Alekseenko, A. L.; Ilovaisky, A. I.; Glinushkin, A. P.; Terent'ev, A. O. 4-Disubstituted Pyrazolin-3-Ones—Novel Class of Fungicides against Phytopathogenic Fungi. Agrochemicals 2023, 2, 34–46. doi:10.3390/agrochemicals2010004
• Utecht-Jarzyńska, G.; Kowalczyk, A.; Jasiński, M. Fluorinated and Non-Fluorinated 1,4-Diarylpyrazoles via MnO2-Mediated Mechanochemical Deacylative Oxidation of 5-Acylpyrazolines. Molecules (Basel, Switzerland) 2022, 27, 8446. doi:10.3390/molecules27238446
• Kowalczyk, R. doi:10.1002/9783527832217.ch12
• Ma, X.; Zhang, W. Recent developments in one-pot stepwise synthesis (OPSS) of small molecules. iScience 2022, 25, 105005. doi:10.1016/j.isci.2022.105005
• Štrukil, V.; Margetić, D. doi:10.1002/9783527832002.ch10
• Antol, I.; Glasovac, Z.; Murata, Y.; Hashikawa, Y.; Margetić, D. Consecutive Utilization of Mechanochemical and Microwave Methods for the Synthesis of Boc‐2‐amino‐quinazolin‐4(3H)‐ones and DFT Study of Mechanism 6π‐Diazaelectrocyclization Process. ChemistrySelect 2022, 7. doi:10.1002/slct.202200633
• Hernández, J. G.; Ardila-Fierro, K. J.; Barišić, D.; Geneste, H. Multi-faceted reactivity of N-fluorobenzenesulfonimide (NFSI) under mechanochemical conditions: fluorination, fluorodemethylation, sulfonylation, and amidation reactions. Beilstein journal of organic chemistry 2022, 18, 182–189. doi:10.3762/bjoc.18.20
• Williams, M.; Morrill, L. C.; Browne, D. L. Mechanochemical Organocatalysis: Do High Enantioselectivites Contradict what we Might Expect?. ChemSusChem 2021, 15, e202102157. doi:10.1002/cssc.202102157
• Borodkin, G. I.; Shubin, V. G. Electrophilic and Oxidative Fluorination of Heterocyclic Compounds: Contribution to Green Chemistry. Russian Journal of Organic Chemistry 2021, 57, 1369–1397. doi:10.1134/s1070428021090013
• Zaikin, P. A.; Dyan, O. T.; Elanov, I. R.; Borodkin, G. I. Ionic Liquid-Assisted Grinding: An Electrophilic Fluorination Benchmark. Molecules (Basel, Switzerland) 2021, 26, 5756. doi:10.3390/molecules26195756
• Nicholson, W. I.; Howard, J. L.; Magri, G.; Seastram, A. C.; Khan, A.; Bolt, R. R. A.; Morrill, L. C.; Richards, E.; Browne, D. L. Ball‐Milling‐Enabled Reactivity of Manganese Metal**. Angewandte Chemie 2021, 133, 23312–23317. doi:10.1002/ange.202108752
• Nicholson, W. I.; Howard, J.; Magri, G.; Seastram, A. C.; Khan, A.; Bolt, R. R. A.; Morrill, L. C.; Richards, E.; Browne, D. L. Ball-Milling-Enabled Reactivity of Manganese Metal*. Angewandte Chemie (International ed. in English) 2021, 60, 23128–23133. doi:10.1002/anie.202108752
• Nicholson, W. I.; Barreteau, F.; Leitch, J. A.; Payne, R.; Priestley, I.; Godineau, E.; Battilocchio, C.; Browne, D. L. Direct Amidation of Esters via Ball Milling. Angewandte Chemie (International ed. in English) 2021, 60, 21868–21874. doi:10.1002/anie.202106412

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