Supporting Information
| Supporting Information File 1: Detailed experimental procedures, the synthesis of labelled compounds, crystallographic information for 15a-15N2 and 15b-15N2, computational data, and 1D 1H, 13C and 2D 15N-HMBC spectra of the synthesized compounds. | ||
| Format: PDF | Size: 3.6 MB | Download |
| Supporting Information File 2: Crystallographic data for 15a-15N2. | ||
| Format: CIF | Size: 20.1 KB | Download |
| Supporting Information File 3: Crystallographic data for 15b-15N2. | ||
| Format: CIF | Size: 20.2 KB | Download |
Cite the Following Article
15N-Labelling and structure determination of adamantylated azolo-azines in solution
Sergey L. Deev, Alexander S. Paramonov, Tatyana S. Shestakova, Igor A. Khalymbadzha, Oleg N. Chupakhin, Julia O. Subbotina, Oleg S. Eltsov, Pavel A. Slepukhin, Vladimir L. Rusinov, Alexander S. Arseniev and Zakhar O. Shenkarev
Beilstein J. Org. Chem. 2017, 13, 2535–2548.
https://doi.org/10.3762/bjoc.13.250
How to Cite
Deev, S. L.; Paramonov, A. S.; Shestakova, T. S.; Khalymbadzha, I. A.; Chupakhin, O. N.; Subbotina, J. O.; Eltsov, O. S.; Slepukhin, P. A.; Rusinov, V. L.; Arseniev, A. S.; Shenkarev, Z. O. Beilstein J. Org. Chem. 2017, 13, 2535–2548. doi:10.3762/bjoc.13.250
Download Citation
Citation data can be downloaded as file using the "Download" button or used for copy/paste from the text window
below.
Citation data in RIS format can be imported by all major citation management software, including EndNote,
ProCite, RefWorks, and Zotero.
Presentation Graphic
| Picture with graphical abstract, title and authors for social media postings and presentations. | ||
| Format: PNG | Size: 765.3 KB | Download |
Citations to This Article
Up to 20 of the most recent references are displayed here.
Scholarly Works
- Sumran, G.; Jain, N.; Kumar, P.; Aggarwal, R. Trifluoromethyl-β-dicarbonyls as Versatile Synthons in Synthesis of Heterocycles. Chemistry (Weinheim an der Bergstrasse, Germany) 2024, 30, e202303599. doi:10.1002/chem.202303599
- Wang, Q.; Jung, H.; Kim, D.; Chang, S. Iridium-Catalyzed Migratory Terminal C(sp3)-H Amidation of Heteroatom-Substituted Internal Alkenes via Olefin Chain Walking. Journal of the American Chemical Society 2023. doi:10.1021/jacs.3c09679
- Morgan, K. D. The use of nitrogen-15 in microbial natural product discovery and biosynthetic characterization. Frontiers in microbiology 2023, 14, 1174591. doi:10.3389/fmicb.2023.1174591
- Sheina, E. S.; Shestakova, T. S.; Deev, S. L.; Khalymbadzha, I. A.; Slepukhin, P. A.; Eltsov, O. S.; Novikov, A. S.; Shevyrin, V. A.; Charushin, V. N.; Chupakhin, O. N. Mesomeric Betaines Based on Adamantylated 1,2,4-Triazolo[4,3-a]pyrimidin-5-ones: Synthesis, Structure and Conversion into Anionic N-Heterocyclic Carbenes. Chemistry, an Asian journal 2023, 18, e202201306. doi:10.1002/asia.202201306
- Zhou, Z.; Kweon, J.; Jung, H.; Kim, D.; Seo, S.; Chang, S. Photoinduced Transition-Metal-Free Chan-Evans-Lam-Type Coupling: Dual Photoexcitation Mode with Halide Anion Effect. Journal of the American Chemical Society 2022, 144, 9161–9171. doi:10.1021/jacs.2c03343
- Artem'ev, G. A.; Rusinov, V. L.; Kopchuk, D. S.; Savchuk, M. I.; Santra, S.; Ulomsky, E. N.; Zyryanov, G. V.; Majee, A.; Du, W.; Charushin, V. N.; Chupakhin, О. N. Synthetic approaches to 1,2,4-triazolo[5,1-c][1,2,4]triazin-7-ones as basic heterocyclic structures of the antiviral drug Riamilovir ("Triazavirin®") active against SARS-CoV-2 (COVID-19). Organic & biomolecular chemistry 2022, 20, 1828–1837. doi:10.1039/d1ob02125g
- Claraz, A. Comprehensive Heterocyclic Chemistry IV - Bicyclic 5-6 Systems With One Bridgehead (Ring Junction) Nitrogen Atom: Four Extra Heteroatoms 2:2. Comprehensive Heterocyclic Chemistry IV; Elsevier, 2022; pp 802–858. doi:10.1016/b978-0-12-818655-8.00086-x
- Ivanov, S. M. Comprehensive Heterocyclic Chemistry IV - 1,2,4-Triazines and Their Benzo Derivatives. Comprehensive Heterocyclic Chemistry IV; Elsevier, 2022; pp 29–180. doi:10.1016/b978-0-12-818655-8.00062-7
- Xiao, G.; Xu, S.; Xie, C.; Zi, G.; Ye, W.; Zhou, Z.; Hou, G.; Zhang, Z. Enantioselective Synthesis of Chiral Substituted 2,4-Diketoimidazolidines and 2,5-Diketopiperazines via Asymmetric Hydrogenation. Organic letters 2021, 23, 5734–5738. doi:10.1021/acs.orglett.1c01894
- Ivanov, S. M. Reversed steric order of reactivity for tert‐butyl and adamantyl‐3‐cyanomethylene‐1,2,4‐triazines. Journal of Heterocyclic Chemistry 2021, 58, 1371–1378. doi:10.1002/jhet.4255
- Jaźwiński, J. Theoretical and practical aspects of indirect spin–spin couplings. Nuclear Magnetic Resonance; The Royal Society of Chemistry, 2020; pp 34–75. doi:10.1039/9781788010665-00034
- Deev, S. L.; Khalymbadzha, I. A.; Shestakova, T. S.; Charushin, V. N.; Chupakhin, O. N. 15N labeling and analysis of 13C-15N and 1H-15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles. RSC advances 2019, 9, 26856–26879. doi:10.1039/c9ra04825a
- Fischer, G. Recent advances in 1,2,4-triazolo[1,5-a]pyrimidine chemistry. Advances in Heterocyclic Chemistry; Elsevier, 2019; Vol. 128, pp 1–101. doi:10.1016/bs.aihch.2018.10.002
