Extrusion – back to the future: Using an established technique to reform automated chemical synthesis

Deborah E. Crawford
Beilstein J. Org. Chem. 2017, 13, 65–75. https://doi.org/10.3762/bjoc.13.9

Cite the Following Article

Extrusion – back to the future: Using an established technique to reform automated chemical synthesis
Deborah E. Crawford
Beilstein J. Org. Chem. 2017, 13, 65–75. https://doi.org/10.3762/bjoc.13.9

How to Cite

Crawford, D. E. Beilstein J. Org. Chem. 2017, 13, 65–75. doi:10.3762/bjoc.13.9

Download Citation

Citation data can be downloaded as file using the "Download" button or used for copy/paste from the text window below.
Citation data in RIS format can be imported by all major citation management software, including EndNote, ProCite, RefWorks, and Zotero.

Presentation Graphic

Picture with graphical abstract, title and authors for social media postings and presentations.
Format: PNG Size: 2.0 MB Download

Citations to This Article

Up to 20 of the most recent references are displayed here.

Scholarly Works

  • Zhao, J.; Liu, Y.; Wang, H.; Fu, X. c.; Deng, N. m. Continuous, solvent-free, and mechanochemical synthesis of UIO-66 (Mn) by gas-solid two-phase flow and mechanism research. Journal of Solid State Chemistry 2024, 338, 124863. doi:10.1016/j.jssc.2024.124863
  • Gul-E-Nayyab; Zakaria, M. R. S. B.; Abid, M. B.; Shamim, A.; Suradi, S. S.; Marsi, N. B.; Kormin, F. B. A Review on Biodegradable Composite Films Containing Organic Material as a Natural Filler. Journal of Inorganic and Organometallic Polymers and Materials 2024. doi:10.1007/s10904-024-03217-x
  • Mukherjee, N. Mechanochemistry: A Resurgent Force in Chemical Synthesis. Synlett 2024. doi:10.1055/a-2422-0992
  • Hamzehpoor, E.; Effaty, F.; Borchers, T. H.; Stein, R. S.; Wahrhaftig‐Lewis, A.; Ottenwaelder, X.; Friščić, T.; Perepichka, D. F. Mechanochemical Synthesis of Boroxine‐linked Covalent Organic Frameworks. Angewandte Chemie 2024. doi:10.1002/ange.202404539
  • Yu, J.; Zhang, Y.; Zheng, Z.; Su, W. Total mechano-synthesis of 2-cyclopropyl-4-(4-fluorophenyl)quinoline-3-acrylaldehyde—a pivotal intermediate of pitavastatin. RSC Mechanochemistry 2024, 1, 367–374. doi:10.1039/d4mr00036f
  • Bolt, R. R. A.; Smallman, H. R.; Leitch, J. A.; Bluck, G. W.; Barreteau, F.; Iosub, A. V.; Constable, D.; Dapremont, O.; Richardson, P.; Browne, D. L. Solvent Minimized Synthesis of Amides by Reactive Extrusion. Angewandte Chemie 2024, 136. doi:10.1002/ange.202408315
  • Bolt, R. R. A.; Smallman, H. R.; Leitch, J. A.; Bluck, G. W.; Barreteau, F.; Iosub, A. V.; Constable, D.; Dapremont, O.; Richardson, P.; Browne, D. L. Solvent Minimized Synthesis of Amides by Reactive Extrusion. Angewandte Chemie (International ed. in English) 2024, 63, e202408315. doi:10.1002/anie.202408315
  • Cortés-Lobo, A.; Hernández, J. G. Calcium Carbide (CaC2) as a C2-Synthon by Mechanochemistry. ChemPlusChem 2024, 89, e202400257. doi:10.1002/cplu.202400257
  • Basoccu, F.; De Luca, L.; Porcheddu, A. Mechanochemistry in Organic Synthesis: An Italian Journey through Innovations. European Journal of Organic Chemistry 2024, 27. doi:10.1002/ejoc.202400425
  • Metawea, A.; Soto, R.; Khraisheh, M.; Walker, G.; Albadarin, A. B. Application of Raman and chemometrics to the mechanochemical synthesis of 4,4-bipyridine/cobalt based MOF using twin screw extrusion. Powder Technology 2024, 437, 119558. doi:10.1016/j.powtec.2024.119558
  • Ardila‐Fierro, K. J.; Hernández, J. G. Intermediates in Mechanochemical Reactions. Angewandte Chemie 2024, 136. doi:10.1002/ange.202317638
  • Ardila-Fierro, K. J.; Hernández, J. G. Intermediates in Mechanochemical Reactions. Angewandte Chemie (International ed. in English) 2024, 63, e202317638. doi:10.1002/anie.202317638
  • Kelly, C. B.; Compton, J. S.; Bryan, M. C.; Lambert, K. M.; Phelan, J. P. Going Green: Sustainable Alternatives in Organic Synthesis. Reference Module in Chemistry, Molecular Sciences and Chemical Engineering; Elsevier, 2024. doi:10.1016/b978-0-323-96025-0.00100-9
  • Brandão, P.; Pineiro, M. doi:10.1002/9781119889878.ch11
  • Atapalkar, R. S.; Kulkarni, A. A. Direct amidation of acids in a screw reactor for the continuous flow synthesis of amides. Chemical communications (Cambridge, England) 2023, 59, 9231–9234. doi:10.1039/d3cc02402d
  • Milotskyi, R.; Sharma, G.; Fujie, T.; Hirose, D.; Wada, N.; Takahashi, K. Continuous process of cellulose dissolution and transesterification reaction catalysed by ionic liquid in twin screw extruder. Reaction Chemistry & Engineering 2023, 8, 1395–1402. doi:10.1039/d2re00537a
  • Juaristi, E.; Avila-Ortiz, C. G. Salient Achievements in Synthetic Organic Chemistry Enabled by Mechanochemical Activation. Synthesis 2023, 55, 2439–2459. doi:10.1055/a-2085-3410
  • Purohit, P.; Bhatt, A.; Mittal, R. K.; Abdellattif, M. H.; Farghaly, T. A. Polymer Grafting and its chemical reactions. Frontiers in bioengineering and biotechnology 2023, 10, 1044927. doi:10.3389/fbioe.2022.1044927
  • Baier, D. M.; Rensch, T.; Dobreva, D.; Spula, C.; Fanenstich, S.; Rappen, M.; Bergheim, K.; Grätz, S.; Borchardt, L. The Mechanochemical Beckmann Rearrangement over Solid Acids: From the Ball Mill to the Extruder. Chemistry–Methods 2022, 3. doi:10.1002/cmtd.202200058
  • Zhuang, Y.; Saadatkhah, N.; Morgani, M. S.; Xu, T.; Martin, C.; Patience, G. S.; Ajji, A. Experimental methods in chemical engineering: Reactive extrusion. The Canadian Journal of Chemical Engineering 2022, 101, 59–77. doi:10.1002/cjce.24538

Patents

  • POELMA JUSTIN; ZHANG MU SAN; GU XINYU; ROLLAND JASON P; DESIMONE JOSEPH M. Reactive particulate materials useful for additive manufacturing. US 11390705 B2, July 19, 2022.
  • POELMA JUSTIN; ZHANG MU SAN; GU XINYU; ROLLAND JASON P; DESIMONE JOSEPH M. Sustainable chemistry systems for recyclable dental models and other additively manufactured products. US 11299576 B2, April 12, 2022.
  • POELMA JUSTIN; ZHANG MU SAN; GU XINYU; ROLLAND JASON P; DESIMONE JOSEPH M. REACTIVE PARTICULATE MATERIALS USEFUL FOR ADDITIVE MANUFACTURING. WO 2019217642 A1, Nov 14, 2019.
  • POELMA JUSTIN; ZHANG MU SAN; GU XINYU; ROLLAND JASON P; DESIMONE JOSEPH M. SUSTAINABLE CHEMISTRY SYSTEMS FOR RECYCLABLE DENTAL MODELS AND OTHER ADDITIVELY MANUFACTURED PRODUCTS. WO 2019217641 A1, Nov 14, 2019.
Other Beilstein-Institut Open Science Activities