Supporting Information
| Supporting Information File 1: General experimental conditions, experimental procedures and data, copies of 1H NMR and 13C NMR spectra for compounds 3, syn-5, 8, and 10–13. | ||
| Format: PDF | Size: 1.6 MB | Download |
| Supporting Information File 2: CIF-file of compound syn-5b. | ||
| Format: CIF | Size: 21.7 KB | Download |
Cite the Following Article
Asymmetric synthesis of γ-chloro-α,β-diamino- and β,γ-aziridino-α-aminoacylpyrrolidines and -piperidines via stereoselective Mannich-type additions of N-(diphenylmethylene)glycinamides across α-chloro-N-sulfinylimines
Gert Callebaut, Sven Mangelinckx, Pieter Van der Veken, Karl W. Törnroos, Koen Augustyns and Norbert De Kimpe
Beilstein J. Org. Chem. 2012, 8, 2124–2131.
https://doi.org/10.3762/bjoc.8.239
How to Cite
Callebaut, G.; Mangelinckx, S.; Van der Veken, P.; Törnroos, K. W.; Augustyns, K.; De Kimpe, N. Beilstein J. Org. Chem. 2012, 8, 2124–2131. doi:10.3762/bjoc.8.239
Download Citation
Citation data can be downloaded as file using the "Download" button or used for copy/paste from the text window
below.
Citation data in RIS format can be imported by all major citation management software, including EndNote,
ProCite, RefWorks, and Zotero.
Citations to This Article
Up to 20 of the most recent references are displayed here.
Scholarly Works
- Kaur, N. Aziridine synthesis from imines-I. Synthesis of Aziridines and Oxaziridines from Imines; Elsevier, 2024; pp 1–25. doi:10.1016/b978-0-443-22059-3.00015-7
- Mei, Y.; Zhang, T.; Hao, X.; Jin, K.; Zhang, R.; Duan, C.; Li, Y. Visible-light-mediated α-amino alkylation of ketimines and aldimines for the synthesis of 1,2-diamines. Organic & biomolecular chemistry 2023, 21, 6192–6196. doi:10.1039/d3ob00808h
- Wu, G.; Wang, J.; Liu, C.; Sun, M.; Zhang, L.; Ma, Y.; Cheng, R.; Ye, J. Transition metal-free, visible-light-mediated construction of α,β-diamino esters via decarboxylative radical addition at room temperature. Organic Chemistry Frontiers 2019, 6, 2245–2249. doi:10.1039/c9qo00407f
- Zhang, H.; Yang, Z.; Zhao, B. N.; Li, G. Group-Assisted Purification Chemistry for Asymmetric Mannich-type Reaction of Chiral N-Phosphonyl Imines with Azlactones Leading to Syntheses of α-Quaternary α,β-Diamino Acid Derivatives †. The Journal of organic chemistry 2017, 83, 644–655. doi:10.1021/acs.joc.7b02556
- Pellissier, H.; Lattanzi, A.; Dalpozzo, R. doi:10.1002/9783527802029.ch2
- Li, Y.; Xiang, L.; Shang, H.; Chen, X.; Ren, X. Diastereoselective Mannich Reactions Using Fluorinated Ketones: Synthesis of Stereogenic Carbon–Fluorine Units. The Journal of organic chemistry 2016, 81, 9858–9866. doi:10.1021/acs.joc.6b01979
- Guerola, M.; Sánchez-Roselló, M.; Mulet, C.; del Pozo, C.; Fustero, S. Asymmetric intramolecular aza-Michael reaction in desymmetrization processes. Total synthesis of hippodamine and epi-hippodamine. Organic letters 2015, 17, 960–963. doi:10.1021/acs.orglett.5b00054
- Pellissier, H. Recent Developments in Asymmetric Aziridination. Advanced Synthesis & Catalysis 2014, 356, 1899–1935. doi:10.1002/adsc.201400312
- Callebaut, G.; Meiresonne, T.; De Kimpe, N.; Mangelinckx, S. Synthesis and reactivity of 2-(carboxymethyl)aziridine derivatives. Chemical reviews 2014, 114, 7954–8015. doi:10.1021/cr400582d
- Callebaut, G.; Colpaert, F.; Nonn, M.; Kiss, L.; Sillanpää, R.; Törnroos, K. W.; Fülöp, F.; De Kimpe, N.; Mangelinckx, S. Asymmetric synthesis of chloroisothreonine derivatives via syn-stereoselective Mannich-type additions across N-sulfinyl-α-chloroimines. Organic & biomolecular chemistry 2014, 12, 3393–3405. doi:10.1039/c4ob00243a
- Kattamuri, P. V.; Xiong, Y.; Pan, Y.; Li, G. N,N-DIIsopropyl-N-phosphonyl imines lead to efficient asymmetric synthesis of aziridine-2-carboxylic esters. Organic & biomolecular chemistry 2013, 11, 3400–3408. doi:10.1039/c3ob40251g
- Callebaut, G. Ph.D. Thesis, Jan 1, 2013.
Patents
- レレティ ラジェンダー レッディ; コッツリ シャラドシュリカー; ナリヴェラ クマラ スワミー; パテル チラーグ; ラバル プージャバーェン; ザラバディヤ ヴィンカル. ビシナルジアミンのジアステレオ選択合成のための改良プロセス. JP 2021530564 A, Nov 11, 2021.
