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Beilstein J. Org. Chem. 2019, 15, 710–720, doi:10.3762/bjoc.15.66
Graphical Abstract
Figure 1: Schematic representation of β-CD with glucopyranose atom numbering and with alphabetic labeling of ...
Scheme 1: Syntheses of 6A,6X-diazido-β-CDs as reference compounds using the “capping” literature method [11,12].
Scheme 2: Syntheses of homo-difunctionalized β-CDs using different reaction conditions.
Figure 2: HPLC chromatograms of the authentic 6A,6X-diazido-β-CDs with known regiochemistry (references 1–3, Scheme 1...
Figure 3: NMR spectral regions of the three ditosyl regioisomers in D2O (500 MHz). The signals of the tosylat...
Scheme 3: Syntheses of 6A-monoazido-6X-monotosyl-β-CDs using starting materials obtained from different react...
Figure 4: Reversed-phase HPLC chromatograms of 6A-monoazido-6X-monotosyl-β-CDs prepared through reactions 4–8....
Figure 5: HPLC separation of regioisomers and pseudoenantiomers of 6A-monoazido-6X-monotosyl-β-CD prepared in...
Figure 6: Reversed-phase HPLC chromatograms of 6A,6X-diazido-β-CDs prepared in reactions 9–13.
Beilstein J. Org. Chem. 2016, 12, 537–548, doi:10.3762/bjoc.12.53
Figure 1: Structures of fluorescent xanthene dyes. Rhodamine B·HCl 1 and fluorescein disodium salt 2.
Figure 2: Reaction scheme for the synthesis of rhodamine-appended β-CD.
Figure 3: TLC plates at different development stages for monitoring the composition of Rho-β-CD crude (left p...
Figure 4: 1H NMR spectrum of Rho-β-CD with partial assignments (D2O, 500 MHz, 298 K).
Figure 5: Expansion of DEPT-ed-HSQC spectrum of Rho-β-CD with partial assignments (D2O, 500 MHz, 298 K).
Figure 6: Cartoon models for the possible intermolecular inclusion mode of Rho-β-CD in solution (3D perspecti...
Figure 7: 1H NMR spectrum of Flu-β-CD with partial assignments (D2O, 500 MHz, 298 K).
Figure 8: Cartoon models for the possible intermolecular inclusion mode of Flu-β-CD in solution (3D perspecti...
Beilstein J. Org. Chem. 2014, 10, 3007–3018, doi:10.3762/bjoc.10.319
Scheme 1: Schematic representation of the various synthetic routes for the introduction of an anchoring group...
Scheme 2: Synthetic strategy for the rhodaminylation of β-CD polymer.
Figure 1: TLC study of β-CD iodination showing the proceeding of 6-monoiodination with increasing reaction ti...
Figure 2: HSQC-DEPT spectrum of compound 1 with partial assignment.
Figure 3: IR spectra of compound 1 (black line) and compound 2 (red line) showing the disappearance of the az...
Scheme 3: Schematic representation for the coumarinylation of methylated β-CD-polymer, n, m, p and q mean the...
Figure 4: HSQC-DEPT spectra of compound 4 with partial assignment; in the upper part the full spectrum is sho...
Scheme 4: Schematic representation for the introduction of NBF in a cationic β-CD-polymer.
Scheme 5: Schematic representation for the introduction of fluorescein into a β-CD-polymer.