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Beilstein J. Org. Chem. 2024, 20, 2408–2420, doi:10.3762/bjoc.20.205
Graphical Abstract
Figure 1: The schematic diagram of the continuous flow microreactor system.
Scheme 1: Nitration of IO with mixed acid.
Figure 2: Two mixing setups: (a) a T-mixer and (b) a T-mixer combined with a homemade static mixer, and the e...
Figure 3: Determination of the number of reaction orders. a) ln(1−xIO) versus t; b) versus t; c) ln(1−xIO) v...
Figure 4: Determination of (M−1)cIO0k at different temperatures and H2SO4 mass fractions. (a) 88% H2SO4, (b) ...
Figure 5: Variations and fitting of as a function of a) the mass fraction of H2SO4 at 23 °C, 40 °C, and 60 °C...
Figure 6: Determination of thermodynamic parameters n and k0 and determination of the activation energy and p...
Figure 7: a) The value of apparent rate constant k at various H2SO4 mass fractions and different temperatures...