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2 article(s) from Kubik, Stefan

Optical detection of di- and triphosphate anions with mixed monolayer-protected gold nanoparticles containing zinc(II)–dipicolylamine complexes

Lena Reinke,
Julia Bartl,
Marcus Koch and
Stefan Kubik

Beilstein J. Org. Chem. 2020, 16, 2687–2700, doi:10.3762/bjoc.16.219

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Figure 1: Schematic illustration of the analyte-induced crosslinking of gold nanoparticles containing a mixtu...

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Scheme 1: Syntheses of the ligands rac-1 and (R)-1. Conditions: i) TsCl, NaOH, THF, 0 °C, 60 min → 25 °C, 80 ...

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Scheme 2: Synthesis of ligand 2. Conditions: i) potassium phthalimide, DMF, 25 °C, 18 h, 67%; ii) 2,2'-dipico...

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Figure 2: Photographs of solutions of NP^rac^-¹ in water (0.25 mg/mL) containing different sodium salts at a co...

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Figure 3: Sections of the ¹H NMR spectra of solutions of NP²⁵ in D₂O/CD₃OD 1:2 (v/v) between 8.9 and 3.9 ppm ...

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Figure 4: Images of vials containing solutions of NP^10-Zn (0.25 mg/mL) in water/methanol 1:2 (v/v) and additi...

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Figure 5: Photograph of the solutions of the competition experiment. Vial (a) only contained NP^10-Zn (and the...

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Figure 6: UV–vis spectra of NP^10-Zn (0.25 mg/mL in the initial measurement) in water/methanol 1:2 (v/v) conta...

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Figure 7: TEM images of NP^10-Zn (0.25 mg/mL) in water/methanol 1:2 (v/v) before (a) and after the addition of...

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Published 02 Nov 2020

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Highly efficient cyclosarin degradation mediated by a β-cyclodextrin derivative containing an oxime-derived substituent

Michael Zengerle,
Florian Brandhuber,
Christian Schneider,
Franz Worek,
Georg Reiter and
Stefan Kubik

Beilstein J. Org. Chem. 2011, 7, 1543–1554, doi:10.3762/bjoc.7.182

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Figure 1: Schematic representation of the general structural design of the investigated cyclodextrin derivati...

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Scheme 1: Structure of cyclosarin (GF).

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Scheme 2: Cyclodextrin derivatives tested as potential GF scavengers.

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Scheme 3: General strategies used for the preparation of the investigated cyclodextrin derivatives.

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Scheme 4: Reaction conditions used for the preparation of cyclodextrin derivatives 1a–e from tosylate 3.

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Scheme 5: Synthesis of 3-(aminomethyl)benzaldehyde oxime (5). Reagents and conditions: i. NaBH₄, EtOH, 1 h, 2...

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Scheme 6: Synthesis of 3-((hydroxyimino)methyl)-1-(prop-2-ynyl)pyridinium bromide (6). Reagents and condition...

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Scheme 7: Syntheses of 6-ethynyl-formylpyridine oximes (7a–c). Reagents and conditions: i. CuI, (PPh₃)₂PdCl₂,...

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Scheme 8: Reaction conditions used for the preparation of cyclodextrin derivatives 2a–d from azide 4.

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Figure 2: Diagram summarizing the observed Δk₁ values for cyclodextrins 1a–e and 2a–d. For comparison, the re...

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Figure 3: Time-dependent decrease of GF concentration in the presence of 1b (top row), 1c (middle row), and 2a...

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Scheme 9: Schematic protocol for the qualitative assay.

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Scheme 10: Schematic protocol of the quantitative assay.

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Published 22 Nov 2011

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