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1 article(s) from MacDonald, Connor R M

Applications of microscopy and small angle scattering techniques for the characterisation of supramolecular gels

Connor R. M. MacDonald and
Emily R. Draper

Beilstein J. Org. Chem. 2024, 20, 2608–2634, doi:10.3762/bjoc.20.220

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Graphical Abstract

Figure 1: Hierarchical assembly occurring across length scales. Molecular interactions result in fibres which...

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Figure 2: Three-dimensional CLSM image of a multicomponent supramolecular structure. The three-dimensional CL...

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Figure 3: AFM images of air-dried aqueous Fmoc-FF, Fmoc-S, and 1:1 Fmoc-FF:Fmoc-S solutions. Figure 3 was reprinted f...

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Figure 4: (a) 3D CLSM images of macroscopically a self-sorting gel network, where all fibres were stained gre...

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Figure 5: (a) 3D AFM topographic image of dried elastin fibre. (b) Indicative height and diameter profile plo...

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Figure 6: The nano-to-micro imaging range of SEM and TEM [30]. Cartoons represent the nanoparticles, pores, nanow...

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Figure 7: Cartoon of artifacts caused by blotting and thinning. a) Alignment of threadlike micelles (left) [32] a...

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Figure 8: (a) Chemical structures of monomer compounds and a schematic of the resulting chiral helical struct...

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Figure 9: Commonly observed entanglements of urea-based supramolecular helices. (a) Double helix, (b) quadrup...

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Figure 10: (a) SEM image of a single three-stranded braid showing a defect in which the braid separates into s...

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Figure 11: Visualization of individual atoms at 1.25 Å resolution. Three apoferritin residues are shown at hig...

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Figure 12: Cartoon of a general small-angle scattering setup.

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Figure 13: (a) SAXS data and fits for solution in H₂O (open symbols) and D₂O (closed symbols). Cryo-TEM data f...

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Figure 14: (a) A cartoon illustrating the orientation phases caused by shear alignment of WLMs. (b) Rheologica...

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Figure 15: (a) Chemical structure of 2NapFF and (b) a cartoon cross-section of the hollow cylinder structure f...

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Figure 16: Length scales of scattering and imaging techniques [16,54,55].

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Figure 17: A schematic of a hydrogel network showing the significance of various parameters extracted from SAN...

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Figure 18: The morphologies of a co-assembled complex dependent on the solvent composition. Figure 18 is from [89] and was ...

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Figure 19: Allowed and forbidden crossings of entangled helices. Figure 19 is from [44] and was adapted by permission from ...

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Figure 20: (a) Cryo-TEM density map of self-assembled (ʟ,ʟ)-2NapFF. (b) Computational model fit to cryo-TEM ma...

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Figure 21: Map showing an incomplete list of global scientific centres providing access to (a) cryo-EM in red ...

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Figure 22: SANS at a range of times. Solid lines are fits to a hollow cylinder model (T = 114 min and T = 202 ...

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Figure 23: SAXS data of 5 mg/mL alanine-functionalised perylene bisimide (PBI-A) in 20 v/v % MeOH at pH (a) 2;...

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Figure 24: Cryo-TEM sample prepared using plunge freezing in liquid nitrogen slush and sublimed for 30 minutes...

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Review

Published 16 Oct 2024

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