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1 article(s) from Paululat, Thomas

Extension of the π-system of monoaryl-substituted norbornadienes with acetylene bridges: influence on the photochemical conversion and storage of light energy

Robin Schulte,
Dustin Schade,
Thomas Paululat,
Till J. B. Zähringer,
Christoph Kerzig and
Heiko Ihmels

Beilstein J. Org. Chem. 2024, 20, 3061–3068, doi:10.3762/bjoc.20.254

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Scheme 1: Photoinduced [2 + 2]-cycloaddition–cycloreversion cycle of norbornadiene (1a) and quadricyclane (2a...

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Figure 1: Representative bis- and tris-norbornadienyl-substituted benzene derivatives.

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Scheme 2: Synthesis of alkynyl-arene-linked norbornadienes 1h–n by Sonogashira–Hagihara coupling reactions.

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Scheme 3: Photoisomerization of norbornadiene derivatives 1h–l,n (20 µM) to quadricyclanes 2h–l,n in cyclohex...

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Figure 2: Photometric monitoring of the irradiation of 1h (A), 1i (B), 1j (C), 1k (D), 1l (E), and 1n (F); λ_ex...

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Scheme 4: Triplet-sensitized photoisomerization of norbornadiene 1o to quadricyclane 2o.

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Figure 3: Photometric monitoring of the irradiation of 1i (A) and 1l (B) in the presence of [Ru(phen)₃](PF₆)₂...

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Published 21 Nov 2024

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