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1 article(s) from Prisner, Thomas F

Phosphoramidite building blocks with protected nitroxides for the synthesis of spin-labeled DNA and RNA

Timo Weinrich,
Eva A. Jaumann,
Ute M. Scheffer,
Thomas F. Prisner and
Michael W. Göbel

Beilstein J. Org. Chem. 2018, 14, 1563–1569, doi:10.3762/bjoc.14.133

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Figure 1: Structures of TEMPO-labeled oligonucleotides and of phosphoramidites 5–8.

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Scheme 1: Synthesis of phosphoramidite 5. Reagents and conditions: (a) 1. 2,4,6-triisopropylbenzenesulfonyl c...

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Scheme 2: Synthesis of phosphoramidite 7. Reagents and conditions: (a) Addition of 10, diisopropylethylamine,...

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Scheme 3: Synthesis of phosphoramidite 8. Reagents and conditions: (a) Addition of 10, diisopropylethylamine,...

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Figure 2: Structures of palindromic oligonucleotides prepared from amidites 5 (22a, 23a), 7 (24a, 25a), and 8...

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Figure 3: PELDOR measurement of 24c (12mer dA). The background-corrected time trace (original time trace in Supporting Information File 1,...

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Published 26 Jun 2018

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