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Search for "spectroscopy" in Full Text gives 1415 result(s) in Beilstein Journal of Nanotechnology. Showing first 200.

Durable antimicrobial activity of fabrics functionalized with zeolite ion-exchanged nanomaterials against Staphylococcus aureus and Escherichia coli

  • Perla Sánchez-López,
  • Kendra Ramirez Acosta,
  • Sergio Fuentes Moyado,
  • Ruben Dario Cadena-Nava and
  • Elena Smolentseva

Beilstein J. Nanotechnol. 2026, 17, 262–274, doi:10.3762/bjnano.17.18

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  • plasma optical emission spectroscopy (ICP-OES). The results confirmed silver, copper, and zinc contents of around 1.0–1.5 atom % [4]. Energy-dispersive X-ray spectroscopy (EDS) analysis performed on the functionalized fabrics in the present work confirmed the presence of silver (1.3 wt %), as well as
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Published 06 Feb 2026

Multilayered hyperbolic Au/TiO2 nanostructures for enhancing the nonlinear response around the epsilon-near-zero point

  • Fernando Arturo Araiza-Sixtos,
  • Mauricio Gomez-Robles,
  • Rafael Salas-Montiel and
  • Raúl Rangel-Rojo

Beilstein J. Nanotechnol. 2026, 17, 251–261, doi:10.3762/bjnano.17.17

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  • layered Ag/TiO2 and determined via spectroscopy that its ENZ point laid within the visible spectrum [7]. Since then, a wide array of layered metal–dielectric configurations have been demonstrated, including silver-based combinations such as Ag/SiO2 [1], Ag/Al2O3 [6], Ag/LiF [8], Ag/TiO2 [9], Ag/Ge [10
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Published 05 Feb 2026

Gold nanoparticle-decorated reduced graphene oxide as a highly effective catalyst for the selective α,β-dehydrogenation of N-alkyl-4-piperidones

  • Brenda Flore Kenyim,
  • Mihir Tzalis,
  • Marilyn Kaul,
  • Robert Oestreich,
  • Aysenur Limon,
  • Chancellin Pecheu Nkepdep and
  • Christoph Janiak

Beilstein J. Nanotechnol. 2026, 17, 218–238, doi:10.3762/bjnano.17.15

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  • diffraction (PXRD) (see Supporting Information File 1). An ice-cold solution of sodium borohydride (NaBH4) was added dropwise to an aqueous solution containing KAuCl4 and the sodium salt of SiW9, resulting in the formation of an orange-brown dispersion (Figure 1b). UV–vis spectroscopy revealed the
  • the average size of nanoparticles based on X-ray diffraction data. To verify the gold loading in the Au-SiW9/rGO composite, a carefully weighed aliquot was dissolved in a microwave digestion system using conc. HNO3 (70%) and diluted HCl (5%) for atomic absorption spectroscopy (AAS). The measured gold
  • functionalities of rGO were investigated by X-ray photoelectron spectroscopy (XPS) in the composite Au-SiW9/rGO. The Au 4f region (Figure 11a) shows two dominant peaks at 84.1 eV (Au 4f7/2) and 87.8 eV (Au 4f5/2), which correspond to metallic Au0, which is the initial catalytically active form in oxidative
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Published 30 Jan 2026

Time of flight secondary ion mass spectrometry imaging of contaminant species in chemical vapour deposited graphene on copper

  • Barry Brennan,
  • Vlad-Petru Veigang-Radulescu,
  • Philipp Braeuninger-Weimer,
  • Stephan Hofmann and
  • Andrew J. Pollard

Beilstein J. Nanotechnol. 2026, 17, 200–213, doi:10.3762/bjnano.17.13

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  • single crystals [3][20][21][22][23], utilising Raman spectroscopy to confirm the physical structure of the graphene [24][25][26] and X-ray photoelectron spectroscopy (XPS) to confirm the sp2 bonding configuration [27][28]. However, there is typically little consideration given to possible chemical
  • of 30 nA were used for sputtering cycles. The interleaved image spectra were acquired using 25 keV Bi3+ ions from a liquid metal ion gun, orientated at 45° to the sample surface. This was operated at an ion current of 0.1 pA, in an interlaced mode with a cycle time of 100 µs, in spectroscopy mode to
  • of copper or copper oxide. However, as recent studies have shown through energy-dispersive X-ray spectroscopy mapping [30], there are significant other contaminants detectable on high-purity Cu foils that can influence graphene nucleation and can remain after growth [31]. A more detailed examination
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Published 21 Jan 2026

Structure-dependent thermochromism of PAZO thin films: theory and experiment

  • Georgi Mateev,
  • Dean Dimov,
  • Nataliya Berberova-Buhova,
  • Nikoleta Kircheva,
  • Todor Dudev,
  • Ludmila Nikolova,
  • Elena Stoykova,
  • Keehoon Hong,
  • Dimana Nazarova,
  • Silvia Angelova and
  • Lian Nedelchev

Beilstein J. Nanotechnol. 2026, 17, 186–199, doi:10.3762/bjnano.17.12

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  • other molecules (the interactions between polymer chains can be considered as major factors in the case of a polymer thin film). Infrared (IR) spectroscopy is a powerful tool for understanding the effects of thermal treatment on polymers that can cause significant changes in their IR spectra, revealing
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Published 20 Jan 2026

Development and in vitro evaluation of liposomes and immunoliposomes containing 5-fluorouracil and R-phycoerythrin as a potential phototheranostic system for colorectal cancer

  • Raissa Rodrigues Camelo,
  • Vivianne Cortez Sombra Vandesmet,
  • Octavio Vital Baccallini,
  • José de Brito Vieira Neto,
  • Thais da Silva Moreira,
  • Luzia Kalyne Almeida Moreira Leal,
  • Claudia Pessoa,
  • Daniel Giuliano Cerri,
  • Maria Vitória Lopes Badra Bentley,
  • Josimar O. Eloy,
  • Ivanildo José da Silva Júnior and
  • Raquel Petrilli

Beilstein J. Nanotechnol. 2026, 17, 97–121, doi:10.3762/bjnano.17.7

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  • from [e.g., n = 507] HSPC-50-R-PE control liposomes and [e.g., n = 788] HSPC-IM-R-PE immunoliposomes, which were obtained from six and eight independent AFM images, respectively. 2.4 Fourier transform infrared spectroscopy Drug–nanoparticle interactions were studied by subjecting the previously
  • lyophilized samples to Fourier-transform infrared (FTIR) spectroscopy in an FTIR spectrophotometer (IRTracer-100, Shimazdzu, Japan), with a horizontal attenuated total reflectance accessory. The scan was performed in the range of 500 to 4000 cm−1 [27]. 2.5 Stability study After physicochemical
  • protein corona formation under physiological conditions [63]. These findings highlight the importance of surface characterization by AFM in the development and optimization of nanoparticles. 3.4 Fourier-transform infrared spectroscopy assays The FTIR spectra obtained for the formulations showed the
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Published 09 Jan 2026

Functional surface engineering for cultural heritage protection: the role of superhydrophobic and superoleophobic coatings – a comprehensive review

  • Giuseppe Cesare Lama,
  • Marino Lavorgna,
  • Letizia Verdolotti,
  • Federica Recupido,
  • Giovanna Giuliana Buonocore and
  • Bharat Bhushan

Beilstein J. Nanotechnol. 2026, 17, 63–96, doi:10.3762/bjnano.17.6

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  • formulation allows for the creation of thick, durable coatings (up to 80 µm) without sacrificing polymerization efficiency, as confirmed by Raman spectroscopy. Because of its UV-curing capability, the coating forms a hardened, protective layer within just 1–2 min. By incorporating vinylated alkyd oligomers
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Published 07 Jan 2026

Reduced graphene oxide paper electrode for lithium-ion cells – towards optimized thermal reduction

  • Agata Pawłowska,
  • Magdalena Baran,
  • Stefan Marynowicz,
  • Aleksandra Izabela Banasiak,
  • Adrian Racki,
  • Adrian Chlanda,
  • Tymoteusz Ciuk,
  • Marta Wolczko and
  • Andrzej Budziak

Beilstein J. Nanotechnol. 2026, 17, 24–37, doi:10.3762/bjnano.17.3

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  • samples per material, that is, M300, T400, T600, and T800. Raman spectroscopy The structural properties of the rGO paper sheets were studied with Raman spectroscopy (InVia Renishaw spectrometer). The spectra were collected with three accumulations, a 10 s exposure time, and 1% laser power (laser
  • functionalities within the rGO paper, Fourier-transform infrared (FTIR) spectroscopy was applied in attenuated total reflectance mode. The equipment involved a Perkin Elmer Frontier FTIR spectrometer. The spectra were obtained in the 520–4000 cm−1 wavenumber range with baseline calibration and normalized (0 to
  • 100). XPS X-ray photoelectron spectroscopy was applied to determine the surface concentrations of chemical bonds. The equipment applied was a PHI VersaProbeII Scanning XPS system with monochromatic Al Kα (1486.6 eV) X-rays (100 μm spot focused). High-energy-resolution spectra were obtained with 46.95
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Published 05 Jan 2026

Terahertz-range on-chip local oscillator based on Josephson junction arrays for superconducting quantum-limited receivers

  • Fedor V. Khan,
  • Lyudmila V. Filippenko,
  • Andrey B. Ermakov,
  • Mikhail Yu. Fominsky and
  • Valery P. Koshelets

Beilstein J. Nanotechnol. 2025, 16, 2296–2305, doi:10.3762/bjnano.16.158

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  • proven itself for many times both in laboratory and in real-life conditions. The terahertz SIS-mixer integrated on the same chip with the LO based on a flux-flow oscillator (FFO) and a receiving antenna [13] was used to study the irradiation of the human body [15], gas spectroscopy [16], and the
  • ]. The measurements from the previous section show that this requirement is confidently met. Second, the LO radiation must be sufficiently monochromatic (spectral ratio ≥90%) in order to prevent signal spectra change while down-conversion to IF. Furthermore, for applications in spectroscopy, phase
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Published 22 Dec 2025

Improving magnetic properties of Mn- and Zn-doped core–shell iron oxide nanoparticles by tuning their size

  • Dounia Louaguef,
  • Ghouti Medjahdi,
  • Sébastien Diliberto,
  • Klaus M. Seemann,
  • Thomas Gries,
  • Joelle Bizeau,
  • Damien Mertz,
  • Eric Gaffet and
  • Halima Alem

Beilstein J. Nanotechnol. 2025, 16, 2285–2295, doi:10.3762/bjnano.16.157

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  • least tenfold). The designed core NPs are composed of a Zn0.4Fe2.6O4 core and a MnFe2O4 shell. Their size and morphology were determined by transmission electron microscopy, Fourier-transform infrared spectroscopy was used to investigate their chemical composition. The iron oxide phase was confirmed by
  • while expecting good biocompatibility. The use of size-controlled synthesis enables the exploration of size-dependent magnetic properties, while the direct characterization of the core–shell structure using Fourier-transform infrared spectroscopy (FTIR) and high-resolution transmission electron
  • on a JEOL JEM-ARM 200F cold-FEG microscope operating at 200 kV and equipped with a spherical aberration probe corrector (Cs). The chemical compositions were determined by energy-dispersive X-ray spectroscopy The elemental maps were recorded on a SDD, Jeol DRY SD 30 GV X-ray spectrometer. NP shapes
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Published 15 Dec 2025

Visualizing nanostructures in supramolecular hydrogels: a correlative study using confocal and cryogenic scanning electron microscopy

  • Shaun M. Smith,
  • Ferdinando Malagreca,
  • Jacqueline Hicks,
  • Giuseppe Mantovani,
  • David B. Amabilino,
  • Christopher Parmenter and
  • Lluïsa Pérez-García

Beilstein J. Nanotechnol. 2025, 16, 2274–2284, doi:10.3762/bjnano.16.156

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  • observed upon mixing aqueous and ethanolic solutions, and gelation generally occurred in less than one minute (as judged by vial inversion) to yield the gel materials containing the chosen fluorophore. Photophysical characterization of fluorophore@Gels UV–visible absorption spectroscopy was performed using
  • a Cary 5000 UV–visible spectrophotometer (Agilent). Fluorescence spectroscopy and absolute fluorescence quantum yield measurements (given in Supporting Information File 1) were carried out on a FLS 980 spectrometer (Edinburgh Instruments) equipped with a front face sample holder or integrating
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Published 12 Dec 2025

Geometry-controlled engineering of the low-temperature proximity effect in normal metal–superconductor junctions

  • Munisa A. Tomayeva,
  • Vyacheslav D. Neverov,
  • Andrey V. Krasavin,
  • Alexei Vagov and
  • Mihail D. Croitoru

Beilstein J. Nanotechnol. 2025, 16, 2265–2273, doi:10.3762/bjnano.16.155

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  • experiments, where the DOS remains nonzero at low energies. This broadening arises from inelastic scattering, interface imperfections, and finite quasiparticle lifetimes [46][53][57]. Experimentally, the proximity gap can be probed by tunneling spectroscopy by measuring the differential conductance dI/dV on
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Published 12 Dec 2025

Chiral plasmonic nanostructures fabricated with circularly polarized light

  • Tian Qiao and
  • Ming Lee Tang

Beilstein J. Nanotechnol. 2025, 16, 2245–2264, doi:10.3762/bjnano.16.154

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  • reported. The authors of [59] conducted single-particle circular differential scattering spectroscopy (CDS) on their Au nanocubes. In a recent study, enhanced structural chirality of all-metal PNSs was achieved through galvanic replacement reactions (GRRs) modulated by CPL when achiral seeds were
  • field. This section will cover the experimental methods for observing the near fields of cPNSs. Advanced techniques, such as near-field scanning optical microscopy (NSOM), cathodoluminescence (CL), electron energy loss spectroscopy (EELS), and photoemission electron microscopy (PEEM), offer spatial
  • optical spectroscopy, such as CD. However, characterizing local chiral domains can be more challenging. References [21][22] have offered valuable insights through simulations, crystallographic analysis, and high-resolution TEM. A more general model would be desirable through further in-depth studies. 4.2
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Published 08 Dec 2025

Optical bio/chemical sensors for vitamin B12 analysis in food and pharmaceuticals: state of the art, challenges, and future outlooks

  • Seyed Mohammad Taghi Gharibzahedi and
  • Zeynep Altintas

Beilstein J. Nanotechnol. 2025, 16, 2207–2244, doi:10.3762/bjnano.16.153

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  • different food and pharma formulations include high-performance liquid chromatography (HPLC) [14], HPLC coupled with inductively coupled plasma-mass spectrometry (ICP-MS) [15], and a diode array detector [16], atomic absorption spectroscopy [17], surface-enhanced Raman spectroscopy [18][19], capillary
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Published 05 Dec 2025

Electromagnetic study of a split-ring resonator metamaterial with cold-electron bolometers

  • Ekaterina A. Matrozova,
  • Alexander V. Chiginev,
  • Leonid S. Revin and
  • Andrey L. Pankratov

Beilstein J. Nanotechnol. 2025, 16, 2199–2206, doi:10.3762/bjnano.16.152

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  • achieve an optimal balance between power load, responsivity, and total noise [17][22]. This capability is particularly critical for applications like cosmic microwave background polarimetry or high-resolution spectroscopy, where the detector must operate photon-noise-limited under a specific background
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Published 05 Dec 2025

Ultrathin water layers on mannosylated gold nanoparticles

  • Maiara A. Iriarte Alonso,
  • Jorge H. Melillo,
  • Silvina Cerveny,
  • Yujin Tong and
  • Alexander M. Bittner

Beilstein J. Nanotechnol. 2025, 16, 2183–2198, doi:10.3762/bjnano.16.151

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  • light scattering, and infrared spectroscopy. We probed particles adsorbed on hydrophilic and hydrophobic surfaces with atomic force microscopy (AFM) and vibrational sum frequency generation (VSFG) spectroscopy, both operated under variable air humidity. For AFM, we additionally tested hydrophilic and
  • transmission of airborne viruses, such as influenza. Keywords: AFM; humidity; hydrophilicity; hydrophobicity; nanoparticles; sum frequency generation spectroscopy; viruses; water; wetting; Introduction Gold nanoparticles (AuNPs) have been a staple in biomedical and biophysical research [1][2] for almost a
  • inorganic surfaces, usually modified with organic layers, and probed by Fourier-transform infrared spectroscopy (FTIR), vibrational sum frequency generation (VSFG), and atomic force microscopy (AFM). For VSFG and AFM, we systematically varied the relative air humidity (RH). DLS and ZP yield particle size
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Published 04 Dec 2025

Microplastic pollution in Himalayan lakes: assessment, risks, and sustainable remediation strategies

  • Sameeksha Rawat,
  • S. M. Tauseef and
  • Madhuben Sharma

Beilstein J. Nanotechnol. 2025, 16, 2144–2167, doi:10.3762/bjnano.16.148

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  • isolated locations is, however, limited by factors such as harsh climatic conditions, logistical challenges, and the need for expert analytical techniques like microscopy and spectroscopy. The present review considers sources, pathways, and ecological impacts of microplastics in Himalayan lakes compared to
  • understanding the full contamination profile in remote ecosystems [33]. An overview of MP sampling and analysis methods is given in Figure 3. 4.2 Analytical techniques for microplastic characterization 4.2.1 Spectroscopy. One of the key methods of analyzing MPs is spectroscopy. Fourier-transform infrared (FTIR
  • ) spectroscopy is used regularly to identify the chemical structure of MPs [34]. One of the most important developments for nanoplastic detection in complex environmental matrices is micro-FTIR to analyze particles smaller than 10 µm [35]. Raman spectroscopy improves on FTIR by using higher resolution and the
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Published 25 Nov 2025

Quality by design optimization of microemulsions for topical delivery of Passiflora setacea seed oil

  • Daniel T. Pereira,
  • Douglas Dourado,
  • Danielle T. Freire,
  • Dayanne L. Porto,
  • Cícero F. S. Aragão,
  • Myla L. de Souza,
  • Guilherme R. S. de Araujo,
  • Ana Maria Costa,
  • Wógenes N. Oliveira,
  • Anne Sapin-Minet,
  • Éverton N. Alencar and
  • Eryvaldo Sócrates T. Egito

Beilstein J. Nanotechnol. 2025, 16, 2116–2131, doi:10.3762/bjnano.16.146

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  • ), followed by gas chromatography coupled with mass spectroscopy (GC–MS) analysis. The relative composition of fatty acids is presented in Table 1, and the corresponding chromatogram is provided in Figure S1 (Supporting Information File 1). The major constituents identified in OPS were linoleic acid (64.69
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Published 20 Nov 2025

Stereodiscrimination of guests in chiral organosilica aerogels studied by ESR spectroscopy

  • Sebastian Polarz,
  • Yasar Krysiak,
  • Martin Wessig and
  • Florian Kuhlmann

Beilstein J. Nanotechnol. 2025, 16, 2034–2054, doi:10.3762/bjnano.16.140

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  • necessary to reach separation is an important point. We have employed the two enantiomers of a chiral, nitroxide-based spin probe as guests in organo-modified macroporous host materials and applied ESR spectroscopy as a tool to investigate their rotational mobility. Using a well-established and commercially
  • chemistry; ESR spectroscopy; organic inorganic hybrids; porous materials; Introduction Chiral materials represent an evolving research field that focuses on materials whose structures lack mirror symmetry [1][2][3]. The materials exhibit chirality, and a good overview of important developments was given by
  • measurements more difficult. There are other valuable methods for investigating transport in porous media such as gas-adsorption methods, X-ray tomography [24][25], neutron imaging techniques [26][27], optical imaging techniques [27][28], or impedance spectroscopy [29][30]. For all of them, it is difficult to
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Published 13 Nov 2025

Beyond the shell: exploring polymer–lipid interfaces in core–shell nanofibers to carry hyaluronic acid and β-caryophyllene

  • Aline Tavares da Silva Barreto,
  • Francisco Alexandrino-Júnior,
  • Bráulio Soares Arcanjo,
  • Paulo Henrique de Souza Picciani and
  • Kattya Gyselle de Holanda e Silva

Beilstein J. Nanotechnol. 2025, 16, 2015–2033, doi:10.3762/bjnano.16.139

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  • -sectional imaging, and attenuated total reflectance with Fourier transform infrared (ATR-FTIR) spectroscopy provided compelling evidence for the successful formation of the intended core–shell structure. The resulting nanofibers exhibited surface hydrophobicity, suggesting potential for anti-adhesive
  • to increased water ingress through the pores, facilitating access to the core [58]. This possibility is also described by Wang and Xu (2018), who successfully prepared tea polyphenol-loaded porous core–shell fibers by controlling coaxial electrospinning parameters [56]. ATR-FTIR spectroscopy has been
  • acid and β-caryophyllene. The application of coaxial electrospinning allowed the formation of well-defined core–shell structures, as confirmed by morphological, spectroscopic, and thermal analyses. Efficient core encapsulation was evidenced by confocal microscopy, FTIR spectroscopy, and selective core
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Published 12 Nov 2025

The cement of the tube-dwelling polychaete Sabellaria alveolata: a complex composite adhesive material

  • Emilie Duthoo,
  • Aurélie Lambert,
  • Pierre Becker,
  • Carla Pugliese,
  • Jean-Marc Baele,
  • Arnaud Delfairière,
  • Matthew J. Harrington and
  • Patrick Flammang

Beilstein J. Nanotechnol. 2025, 16, 1998–2014, doi:10.3762/bjnano.16.138

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  • composition of cement cell granules, we used energy-dispersive X-ray spectroscopy (EDS) coupled with scanning electron microscopy (SEM). Elemental composition was measured on four secretory granules of both types of cement cells in the parathoracic part of worms embedded in Spurr resin (TEM blocks). Using the
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Published 11 Nov 2025

Laser ablation in liquids for shape-tailored synthesis of nanomaterials: status and challenges

  • Natalie Tarasenka

Beilstein J. Nanotechnol. 2025, 16, 1963–1997, doi:10.3762/bjnano.16.137

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Published 10 Nov 2025

Evaluating metal-organic precursors for focused ion beam-induced deposition through solid-layer decomposition analysis

  • Benedykt R. Jany,
  • Katarzyna Madajska,
  • Aleksandra Butrymowicz-Kubiak,
  • Franciszek Krok and
  • Iwona B. Szymańska

Beilstein J. Nanotechnol. 2025, 16, 1942–1951, doi:10.3762/bjnano.16.135

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  • new metal-organic precursors, in the form of supported thick layers, to the ion beam irradiation is studied through analysis of the chemical composition and morphology of the resulting structures. This is done using SEM backscattered electron/energy-dispersive X-ray spectroscopy along with machine
  • -dispersive X-ray spectroscopy (EDX); focused ion beam (FIB); focused ion beam-induced deposition (FIBID); machine learning; scanning electron microscopy (SEM); Introduction A variety of nanomanufacturing techniques, such as optical and electron-beam lithography, nanoimprint lithography, atomic layer
  • adsorbed on the surface, such as electron-stimulated desorption, high-resolution electron energy loss spectroscopy, and focused electron beam secondary ion mass spectrometry [5]. To characterize compounds in terms of their applicability in the FIBID process, comparisons are made with the FEBID process, and
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Published 04 Nov 2025

PEGylated lipids in lipid nanoparticle delivery dynamics and therapeutic innovation

  • Peiyang Gao

Beilstein J. Nanotechnol. 2025, 16, 1914–1930, doi:10.3762/bjnano.16.133

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  • analyzed by high-field 1H NMR spectroscopy and diffusion-filter techniques. The ALC-0159 PEG lipid consists of a PEG2k chain conjugated to a C14–C14 dialkyl glycerol anchor. The surface PEG chain density was estimated at 27.3 PEG chains per 100 nm2 according to the average LNP diameter of 77 nm; this
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Published 30 Oct 2025

Low-temperature AFM with a microwave cavity optomechanical transducer

  • Ermes Scarano,
  • Elisabet K. Arvidsson,
  • August K. Roos,
  • Erik Holmgren,
  • Riccardo Borgani,
  • Mats O. Tholén and
  • David B. Haviland

Beilstein J. Nanotechnol. 2025, 16, 1873–1882, doi:10.3762/bjnano.16.130

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  • experiment, components after the cavity in the measurement chain introduce additional imprecision noise, expressed as an added number of noise photons nadd: The added noise in our setup (Figure 1d) is determined by the cryogenic low-noise amplifier (LNA) mounted at the 4 K stage. We use Planck spectroscopy
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Published 24 Oct 2025
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