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Search for "one-pot synthesis" in Full Text gives 30 result(s) in Beilstein Journal of Nanotechnology.

Growth evolution and phase transition from chalcocite to digenite in nanocrystalline copper sulfide: Morphological, optical and electrical properties

  • Priscilla Vasthi Quintana-Ramirez,
  • Ma. Concepción Arenas-Arrocena,
  • José Santos-Cruz,
  • Marina Vega-González,
  • Omar Martínez-Alvarez,
  • Víctor Manuel Castaño-Meneses,
  • Laura Susana Acosta-Torres and
  • Javier de la Fuente-Hernández

Beilstein J. Nanotechnol. 2014, 5, 1542–1552, doi:10.3762/bjnano.5.166

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  • promising p-type inorganic semiconductor for optoelectronic devices such as solar cells, due its small band gap energy and its electrical properties. In this work nanocrystalline copper sulfide (CuxS), with two stoichiometric ratios (x = 2, 1.8) was obtained by one-pot synthesis at 220, 230, 240 and 260 °C
  • cells. Experimental Crystalline copper sulfide nanostructures were obtained by one-pot synthesis in an organic solvent while raising the reaction temperature from 220 to 260 °C. Amorphous copper sulfide was also synthesized by a chemical reaction in aqueous solution at 40 °C. Films, colloid and powder
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Published 15 Sep 2014

One pot synthesis of silver nanoparticles using a cyclodextrin containing polymer as reductant and stabilizer

  • Arkadius Maciollek and
  • Helmut Ritter

Beilstein J. Nanotechnol. 2014, 5, 380–385, doi:10.3762/bjnano.5.44

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  • Arkadius Maciollek Helmut Ritter Institute of Organic Chemistry and Macromolecular Chemistry, Heinrich-Heine-University Duesseldorf, Universitaetsstraße 1, 40225 Duesseldorf, Germany 10.3762/bjnano.5.44 Abstract A facile and one pot synthesis of silver nanoparticles with narrow size distributions
  • -β-cyclodextrin [20] as reduction and steric stabilization agent without any additional reduction agent or energy source. Silver nitrate has been reduced under pH neutral conditions at room temperature. In this green one pot synthesis neither commonly used toxic reduction agent nor additional energy
  • well as the optical properties are fully reversible upon cooling to room temperature. Conclusion In summary, we present the facile one pot synthesis of long time stable silver nanoparticles using a copolymer from N-isopropylacrylamide (NIPAM) and mono-(1H-triazolylmethyl)-2-methylacryl-β-cyclodextrin
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Published 31 Mar 2014

Influence of particle size and fluorination ratio of CFx precursor compounds on the electrochemical performance of C–FeF2 nanocomposites for reversible lithium storage

  • Ben Breitung,
  • M. Anji Reddy,
  • Venkata Sai Kiran Chakravadhanula,
  • Michael Engel,
  • Christian Kübel,
  • Annie K. Powell,
  • Horst Hahn and
  • Maximilian Fichtner

Beilstein J. Nanotechnol. 2013, 4, 705–713, doi:10.3762/bjnano.4.80

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  • -pot synthesis, which enables a reactive intercalation of nanoscale Fe particles in a CFx matrix, and the reaction of these components to an electrically conductive C–FeF2 compound. The pretreatment and the structure of the utilized CFx precursors play a crucial role in the synthesis and influence the
  • Inorganic Chemistry, Engesserstrasse 15, D-76128 Karlsruhe, Germany 10.3762/bjnano.4.80 Abstract Systematical studies of the electrochemical performance of CFx-derived carbon–FeF2 nanocomposites for reversible lithium storage are presented. The conversion cathode materials were synthesized by a simple one
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Published 01 Nov 2013

Synthesis and catalytic applications of combined zeolitic/mesoporous materials

  • Jarian Vernimmen,
  • Vera Meynen and
  • Pegie Cool

Beilstein J. Nanotechnol. 2011, 2, 785–801, doi:10.3762/bjnano.2.87

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  • zeolite nanoparticles are formed beforehand in a separate reaction vessel. Subsequently, these nanoparticles are added to a mesotemplate solution, hence the term “two-pot”. In a one-pot synthesis on the other hand, the micro- and mesotemplates, together with the silica (and heteroelement) source, are all
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Published 30 Nov 2011

Optical properties of fully conjugated cyclo[n]thiophenes – An experimental and theoretical approach

  • Elena Mena-Osteritz,
  • Fan Zhang,
  • Günther Götz,
  • Peter Reineker and
  • Peter Bäuerle

Beilstein J. Nanotechnol. 2011, 2, 720–726, doi:10.3762/bjnano.2.78

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  • cyclothiophene. By this “metal–template approach”, among other derivatives the series was extended to C8T as the smallest member and the overall yield was improved to around 10% [6][7]. More recently, by applying Pt(II)-oligothienyl complexes [27], a more direct general and highly effective “one-potsynthesis
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Published 25 Oct 2011
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