Structural, optical, and bioimaging characterization of carbon quantum dots solvothermally synthesized from o-phenylenediamine

• Zoran M. Marković,
• Milica D. Budimir,
• Martin Danko,
• Dušan D. Milivojević,
• Pavel Kubat,
• Danica Z. Zmejkoski,
• Vladimir B. Pavlović,
• Marija M. Mojsin,
• Milena J. Stevanović and
• Biljana M. Todorović Marković

Beilstein J. Nanotechnol. 2023, 14, 165–174, doi:10.3762/bjnano.14.17

• cytotoxic properties of CQDs and CQD/polyurethane composites. Results and Discussion Surface morphology Figure S1 (Supporting Information File 1) presents the surface morphology of the CQD samples. Figure S1a shows a TEM micrograph of CQDs. The average diameter of these dots is 4 ± 1 nm. A top-view AFM

• nm (Figure S1c,d in Supporting Information File 1). Figure 1 shows the surface morphology of neat PU and a CQDs/PU sample. The RMS roughness values of these samples are 4.45 and 14.04 nm, respectively. FTIR, UV–vis, and PL spectra of CQDs and CQDs/PU To study the chemical and optical properties of

Electrical and optical enhancement of ITO/Mo bilayer thin films via laser annealing

• Abdelbaki Hacini,
• Ahmad Hadi Ali,
• Nurul Nadia Adnan and
• Nafarizal Nayan

Beilstein J. Nanotechnol. 2022, 13, 1589–1595, doi:10.3762/bjnano.13.133

• 3.21 × 1014 lines/m2. Figure 2 displays the surface morphology in 3D images of ITO/Mo for the as-deposited and annealed samples. These images were scanned over an area of 1.0 × 1.0 µm using AFM. Figure 2 shows the different morphologies for as-deposited and annealed samples using a laser for different

A TiO₂@MWCNTs nanocomposite photoanode for solar-driven water splitting

• Anh Quynh Huu Le,
• Ngoc Nhu Thi Nguyen,
• Hai Duy Tran,
• Van-Huy Nguyen and
• Le-Hai Tran

Beilstein J. Nanotechnol. 2022, 13, 1520–1530, doi:10.3762/bjnano.13.125

• nanocomposite characterizations The surface morphology of MWCNTs and the TiO2@MWCNTs nanocomposite is characterized by using field-emission scanning electron microscopy (FE-SEM, S4800) and transmission electron microscopy (TEM, JEOL-1400). The crystallization behavior of the catalysts is analyzed by X-ray

Rapid and sensitive detection of box turtles using an electrochemical DNA biosensor based on a gold/graphene nanocomposite

• Abu Hashem,
• M. A. Motalib Hossain,
• Ab Rahman Marlinda,
• Mohammad Al Mamun,
• Khanom Simarani and
• Mohd Rafie Johan

Beilstein J. Nanotechnol. 2022, 13, 1458–1472, doi:10.3762/bjnano.13.120

• modified screen-printed carbon electrode Surface morphology and structural characterisation Field-emission scanning electron microscopy (FESEM) images of nanoparticles and their composites are depicted in Figure 2a–b, where the wrinkled regions represent specific patterns of different materials. In Figure

• Gr/SPCE surface, which was then labelled as AuNPs/Gr/SPCE. Morphological and structural studies of nanomaterials The surface morphology of the nanoparticles and their nanocomposites were analysed using a field-emission scanning electron microscope (model SU8030 Hitachi, Japan), equipped with an

Orally administered docetaxel-loaded chitosan-decorated cationic PLGA nanoparticles for intestinal tumors: formulation, comprehensive in vitro characterization, and release kinetics

• Sedat Ünal,
• Osman Doğan and
• Yeşim Aktaş

Beilstein J. Nanotechnol. 2022, 13, 1393–1407, doi:10.3762/bjnano.13.115

• potential (mV) was stated as the average of three subsequent measurements ± SD. Particle shape and surface morphology The shape and surface morphology of DCX-PLGA NPs and CS/DCX-PLGA NPs were investigated by SEM (Zeiss evo LS-10, Germany). For this purpose, NPs were covered with a 100 Å thick coating of

LED-light-activated photocatalytic performance of metal-free carbon-modified hexagonal boron nitride towards degradation of methylene blue and phenol

• Nirmalendu S. Mishra and
• Pichiah Saravanan

Beilstein J. Nanotechnol. 2022, 13, 1380–1392, doi:10.3762/bjnano.13.114

• turbostratic and poor crystalline nature of the as-synthesized MBN. The characteristic peak shift and widening can be attributed to the surface modification through simultaneous replacement of nitrogen atoms with larger carbon atoms [18][21][22]. The surface morphology of HBN, MBN-25, MBN-50, and MBN-80

Near-infrared photoactive Ag-Zn-Ga-S-Se quantum dots for high-performance quantum dot-sensitized solar cells

• Roopakala Kottayi,
• Ilangovan Veerappan and
• Ramadasse Sittaramane

Beilstein J. Nanotechnol. 2022, 13, 1337–1344, doi:10.3762/bjnano.13.110

• ]. Studies of Ag-Zn-Ga-S-Se QD-sensitized TiO2 NFs The surface morphology of AZGSSe/TiO2 was examined through HRTEM and EDX analysis. The HRTEM image (Figure 5a) shows the presence of AZGSSe QDs on the TiO2 NFs. The EDX spectrum (Figure 5b) shows the peaks of Ti, O, Ag, Zn, Ga, S, and Se. These analyses

Studies of probe tip materials by atomic force microscopy: a review

• Ke Xu and
• Yuzhe Liu

Beilstein J. Nanotechnol. 2022, 13, 1256–1267, doi:10.3762/bjnano.13.104

• Ke Xu Yuzhe Liu School of Electrical & Control Engineering, Shenyang Jianzhu University, Shenyang 110168, China 10.3762/bjnano.13.104 Abstract As a tool that can test insulators' surface morphology and properties, the performance index of atomic force microscope (AFM) probes is the most critical

Application of nanoarchitectonics in moist-electric generation

• Jia-Cheng Feng and
• Hong Xia

Beilstein J. Nanotechnol. 2022, 13, 1185–1200, doi:10.3762/bjnano.13.99

• content is not subject to CC BY 4.0. (f) Schematic diagram of the liquid flow-induced streaming potential in a natural microchannel. (a) Surface morphology of an Al2O3 layer. Figure 4a was reprinted with permission from [49], Copyright 2021 American Chemical Society. This content is not subject to CC BY

Electrocatalytic oxygen reduction activity of AgCoCu oxides on reduced graphene oxide in alkaline media

• Iyyappan Madakannu,
• Indrajit Patil,
• Bhalchandra Kakade and
• Kasibhatta Kumara Ramanatha Datta

Beilstein J. Nanotechnol. 2022, 13, 1020–1029, doi:10.3762/bjnano.13.89

• slight changes of the peak positions by varying the silver fraction in the trimetallic catalysts (Figure S2a,b, Supporting Information File 1). The surface morphology of rGO-supported bimetallic (Ag-CuO and Ag-Co3O4) and trimetallic (ACC-1, ACC-2 and ACC-3) NPs, as well as the supportless ACC-2*, were

Self-assembly of C₆₀ on a ZnTPP/Fe(001)–p(1 × 1)O substrate: observation of a quasi-freestanding C₆₀ monolayer

• Guglielmo Albani,
• Michele Capra,
• Alessandro Lodesani,
• Alberto Calloni,
• Gianlorenzo Bussetti,
• Marco Finazzi,
• Franco Ciccacci,
• Alberto Brambilla,
• Lamberto Duò and
• Andrea Picone

Beilstein J. Nanotechnol. 2022, 13, 857–864, doi:10.3762/bjnano.13.76

• displayed in Figure 1b, where individual ZnTPP molecules are resolved. Figure 2 focuses on the surface morphology for a sub-monolayer coverage of C60 on the ZnTPP/Fe(001)–p(1 × 1)O substrate. C60 forms a compact film, composed of hexagonal domains extending for hundreds of nanometers. By considering that

Design and characterization of polymeric microneedles containing extracts of Brazilian green propolis

• Camila Felix Vecchi,
• Rafaela Said dos Santos,
• Jéssica Bassi da Silva and
• Marcos Luciano Bruschi

Beilstein J. Nanotechnol. 2022, 13, 503–516, doi:10.3762/bjnano.13.42

• structure of microneedles containing glycolic extract of propolis (G1 to G9); magnification 40×. Arrows represent locations where bubbles are present. Micrographs obtained by scanning electron microscopy (SEM) showing the surface morphology microneedles containing ethanolic extract of propolis (E1 to E9

• ); magnification 150×. Micrograph obtained by scanning electron microscopy (SEM) showing the surface morphology of microneedles containing glycolic extract of propolis (G1 to G9); magnification 150×. Response surface plots for height and base measurements of MNs containing EE or GE. The color scale is indicated in

A non-enzymatic electrochemical hydrogen peroxide sensor based on copper oxide nanostructures

• Irena Mihailova,
• Vjaceslavs Gerbreders,
• Marina Krasovska,
• Eriks Sledevskis,
• Valdis Mizers,
• Andrejs Bulanovs and
• Andrejs Ogurcovs

Beilstein J. Nanotechnol. 2022, 13, 424–436, doi:10.3762/bjnano.13.35

• ) shows the surface morphology of a thermally obtained copper oxide film. The resulting film is a homogeneous, polycrystalline oxide layer consisting of grains of arbitrary shape. In practice, this layer exhibits poor adhesion to the surface and can be easily damaged mechanically during post-processing

A chemiresistive sensor array based on polyaniline nanocomposites and machine learning classification

• Jiri Kroutil,
• Alexandr Laposa,
• Ali Ahmad,
• Jan Voves,
• Vojtech Povolny,
• Ladislav Klimsa,
• Marina Davydova and
• Miroslav Husak

Beilstein J. Nanotechnol. 2022, 13, 411–423, doi:10.3762/bjnano.13.34

• analysis. Further, statistical classification analysis was implemented for the evaluation of target gases. Scanning electron microscopy and Raman spectroscopy The surface morphology and uniformity of additives in PANI of the deposited active layers were examined by scanning electron microscopy (TESCAN

Selected properties of Al_xZn_yO thin films prepared by reactive pulsed magnetron sputtering using a two-element Zn/Al target

• Witold Posadowski,
• Artur Wiatrowski,
• Jarosław Domaradzki and
• Michał Mazur

Beilstein J. Nanotechnol. 2022, 13, 344–354, doi:10.3762/bjnano.13.29

• the distance from the target axis is shown in Figure 9b. SEM images of the surface morphology at different distances from the target axis are shown in Figure 10. All films were densely packed, homogeneous, and crack-free. For X ≤ 30 mm, the surface is featureless and no grains are visible. Thin films

The effect of metal surface nanomorphology on the output performance of a TENG

• Yiru Wang,
• Xin Zhao,
• Yang Liu and
• Wenjun Zhou

Beilstein J. Nanotechnol. 2022, 13, 298–312, doi:10.3762/bjnano.13.25

• agglomerate. Results and Discussion The XRD data (Figure 4) were processed using the JADE software to calculate the average particle sizes. SEM micrographs were screened according to the surface morphology size of the nanoparticles and colored according to the nanoscale topography size (Figure 5 and Figure 6

• growth density of the copper nanocrystals. These conclusions may help in improving the output performance of TENGs through the control of the metal surface morphology. Energy band model of the metal–insulator contact electrification. The highest unoccupied intermediate trap state accepts electrons

Relationship between corrosion and nanoscale friction on a metallic glass

• Haoran Ma and
• Roland Bennewitz

Beilstein J. Nanotechnol. 2022, 13, 236–244, doi:10.3762/bjnano.13.18

• , pitting is always distributed along a line. Wang et al. [26] found that pitting occurs preferentially at the shear offsets on a pre-deformed Zr-based MG due to the higher chemical activity of offset sites compared with the surrounding flat region. This influence of surface morphology was also shown for

A comprehensive review on electrospun nanohybrid membranes for wastewater treatment

• Senuri Kumarage,
• Imalka Munaweera and
• Nilwala Kottegoda

Beilstein J. Nanotechnol. 2022, 13, 137–159, doi:10.3762/bjnano.13.10

• dissolved in DMF [44]. They have also reported that the humidity had an effect on the surface morphology of the fibers. The increase of surface roughness of the fibers due to pore formation has been observed with the increase of relative humidity. The increase of fiber diameter with relative humidity can

Biocompatibility and cytotoxicity in vitro of surface-functionalized drug-loaded spinel ferrite nanoparticles

• Sadaf Mushtaq,
• Khuram Shahzad,
• Tariq Saeed,
• Anwar Ul-Hamid,
• Bilal Haider Abbasi,
• Nafees Ahmad,
• Waqas Khalid,
• Muhammad Atif,
• Zulqurnain Ali and
• Rashda Abbasi

Beilstein J. Nanotechnol. 2021, 12, 1339–1364, doi:10.3762/bjnano.12.99

• of the (311) plane [30]: where D is the average crystallite size, K = 0.94, λ = 1.54 Å is the X-ray wavelength, β represents the full width at half maximum (FWHM), and θ represents the Bragg's diffraction angle. The surface morphology and major elemental composition were obtained by high-resolution

Electrical, electrochemical and structural studies of a chlorine-derived ionic liquid-based polymer gel electrolyte

• Ashish Gupta,
• Amrita Jain,
• Manju Kumari and
• Santosh K. Tripathi

Beilstein J. Nanotechnol. 2021, 12, 1252–1261, doi:10.3762/bjnano.12.92

• surface morphology of a pure PVdF-HFP film, {(PVdF-HFP)-[BDiMIM][Cl]} (4:6), and ({(PVdF-HFP)-[BDiMIM][Cl]} (4:6)) (20 wt %) + [PC-Mg(ClO4)2 (0.3 M)] (80 wt %), where PC is the plasticizer propylene carbonate, was characterized using scanning electron microscopy (SEM) and is depicted in Figure 1a–c

• . Figure 1a shows the surface morphology of a pure PVdF-HFP film, indicating an uneven and rough surface of the crystalline polymer. Upon the addition of the ionic liquid [BDiMIM][Cl] on PVdF-HFP, the sizes of the grains start decreasing and the membrane becomes flexible and appears as a swollen structure

• Cu Kα radiation. The scan rate was fixed to 5°·min−1. The surface morphology of the synthesized polymer electrolyte films was recorded by using a scanning electron microscope (JEOL JXA - 8100 EPMA). The ionic conductivity of any polymer gel electrolyte film plays an important role, especially at the

Morphology-driven gas sensing by fabricated fractals: A review

• Vishal Kamathe and
• Rupali Nagar

Beilstein J. Nanotechnol. 2021, 12, 1187–1208, doi:10.3762/bjnano.12.88

• number L also characterizes fractal textures and quantifies the fractal-to-fractal gaps; the higher the lacunarity, the lower is the homogeneity [49]. In fractal studies, surface morphology, geometrical features, and degree of self-organization of materials are determined through these dimensionless

Progress and innovation of nanostructured sulfur cathodes and metal-free anodes for room-temperature Na–S batteries

• Marina Tabuyo-Martínez,
• Bernd Wicklein and
• Pilar Aranda

Beilstein J. Nanotechnol. 2021, 12, 995–1020, doi:10.3762/bjnano.12.75

A Au/CuNiCoS₄/p-Si photodiode: electrical and morphological characterization

• Adem Koçyiğit,
• Adem Sarılmaz,
• Teoman Öztürk,
• Faruk Ozel and
• Murat Yıldırım

Beilstein J. Nanotechnol. 2021, 12, 984–994, doi:10.3762/bjnano.12.74

• understand the structural and morphological characteristics of the nanocrystals. A Zeiss-Evo SEM-EDX was employed to determine surface morphology and EDS patterns of the nanocrystals. I–V measurements were carried out on a Fytronix FY-7000 in the dark and under illumination of 20 to 100 mW in 20 mW intervals

9.1% efficient zinc oxide/silicon solar cells on a 50 μm thick Si absorber

• Rafal Pietruszka,
• Bartlomiej S. Witkowski,
• Monika Ozga,
• Katarzyna Gwozdz,
• Ewa Placzek-Popko and
• Marek Godlewski

Beilstein J. Nanotechnol. 2021, 12, 766–774, doi:10.3762/bjnano.12.60

• (ZnONR) were grown via a hydrothermal method (HT) to create a rough surface morphology. Sample B was placed into the ALD growth chamber without modification of the surface morphology. During HT growth, sample B was kept under nitrogen atmosphere. After the HT process, both samples were transferred to the

• calculated for the MZO/ZnONR system, which equals to 1150 ± 50 nm. The estimated thickness of the AZO top electrode was 270 ± 20 nm. In the case of the sample B, the thickness of the deposited films equals to 320 ± 30 nm and 260 ± 10 nm for MZO and AZO, respectively. Figure 4 shows the surface morphology of

• to a non-uniform surface morphology, as intended by us. The average root mean square (RMS) roughness of sample A equals 60 nm. As a result, light reflection is reduced for the cell. This effect was published previously [14] for PV structures prepared on a thicker Si absorber. This feature enhances

Electromigration-induced formation of percolating adsorbate islands during condensation from the gaseous phase: a computational study

• Alina V. Dvornichenko,
• Vasyl O. Kharchenko and
• Dmitrii O. Kharchenko

Beilstein J. Nanotechnol. 2021, 12, 694–703, doi:10.3762/bjnano.12.55

• surface pattern formation at elevated temperatures are the result of the self-organization of adsorbed atoms. They are usually governed by kinetic factors, that is, the rates of processes realized on the growing surface. One of the interesting phenomena influencing the formation of surface morphology at

• observed on silicon substrates [12][13]. Strong effects of EM were manifested in the processes of evolution of vanadium surface morphology [14], and in the epitaxial growth of semiconductor heterostructures [15]. It was found that at low deposition temperatures the growth of surface structures occurs

• include the formation of surface steps [28][29][30][31], faceting of the surface [32][33][34][35][36][37], elimination of instability of surface morphology caused by stress and wetting of the substrate [38][39][40][41], the evolution of contact irregularities in switches of microelectromechanical systems