Beilstein J. Nanotechnol.2011,2, 593–606, doi:10.3762/bjnano.2.63
transmission electron microscopy images and XRD results characterizing the structure and morphology of these films and the distribution and particle size of the Au nanoparticles. The chemicalstate of the materials was characterized by XPS, and finally the catalytic activity of these model systems was
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Figure 1:
Schematic drawing of the end of the SMS capillary and the sample in the scanning mass spectrometer....
Beilstein J. Nanotechnol.2010,1, 24–47, doi:10.3762/bjnano.1.5
) the structure of the particles and (ii) to the chemicalstate. Advanced analytical tools such as aberration-corrected high-resolution transmission electron microscopy (HRTEM) and related techniques as well as X-ray photoelectron spectroscopy (XPS) give important additional information on the atomic
with literature data the main peak can be assigned to the Fe3+ oxidation state [69]. Interestingly, Pt-4f levels reveal no significant indication of oxide formation, proving the chemicalstate of the Pt atoms remains practically unchanged during oxidation of the FePt particles. This finding is
magnetic circular dichroism (XMCD) which provides information on (i) the chemicalstate of sample, (ii) element-specific magnetic moments and (iii) element-specific hysteresis loops. The results presented below were measured at beamline PM-3 of the BESSY II synchrotron facility in Berlin, Germany. The
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Scheme 1:
Preparation of NPs by a reverse micelle technique. PS-b-P2VP or PS-b-P4VP is dispersed in anhydrous...