Theranostic potential of self-luminescent branched polyethyleneimine-coated superparamagnetic iron oxide nanoparticles

• Rouhollah Khodadust,
• Ozlem Unal and
• Havva Yagci Acar

Beilstein J. Nanotechnol. 2022, 13, 82–95, doi:10.3762/bjnano.13.6

• synthesized luminescent SPION@bPEI was published by Unal et al. in 2018 [35]. The total organic content of the particles was determined to be 76% by TGA. The average crystal size of SPION@bPEI nanoparticles was measured from transmission electron microscopy (TEM) images to be approx. 6 nm (Figure 1a). The TEM

Sputtering onto liquids: a critical review

• Anastasiya Sergievskaya,
• Adrien Chauvin and
• Stephanos Konstantinidis

Beilstein J. Nanotechnol. 2022, 13, 10–53, doi:10.3762/bjnano.13.2

• be taken regarding the elemental composition of the deposited materials as it might depend on the position where the elemental analysis is made on the substrate, especially if a spatially resolved analysis is carried out by a technique such as scanning (transmission) electron microscopy combined with

• electron microscopy (TEM), it was shown that the Au sol formation process consists of an induction period followed by a rapid increase in the number of particles, followed by a linear increase, followed by a rapid decrease in the growth rate. In other words, the typical kinetic curve has a sigmoidal S

• diluted solutions [77] as shown for the first time by Turkevich in 1951 [92]. Turkevich and co-workers studied the reduction of HAuCl4 by citrate anions (which also plays the role of a stabilizer for the Au NPs) at different temperatures and different reagent concentrations [92]. By means of transmission

Chemical vapor deposition of germanium-rich CrGe_x nanowires

• Vladislav Dřínek,
• Stanislav Tiagulskyi,
• Roman Yatskiv,
• Jan Grym,
• Radek Fajgar,
• Věra Jandová,
• Martin Koštejn and
• Jaroslav Kupčík

Beilstein J. Nanotechnol. 2021, 12, 1365–1371, doi:10.3762/bjnano.12.100

• -resolution transmission electron microscopy, scanning electron microscopy, electron dispersive X-ray analysis, selected area electron diffraction, and X-ray photoelectron spectroscopy, showed that unlike nanoballs and particles composed of crystalline germanium, the layer was made of chromium germanide CrGex

• nanoobjects were studied by transmission electron microscopy (TEM) performed on a Philips CM 120 (LaB6, 120 kV) equipped with a NanoMEGAS precession unit DigiStar, an Olympus SIS CCD camera Veleta (2048 × 2048 px), and a windowless detector Apollo XLTW for EDX measurements. Selected area electron diffraction

Biocompatibility and cytotoxicity in vitro of surface-functionalized drug-loaded spinel ferrite nanoparticles

• Sadaf Mushtaq,
• Khuram Shahzad,
• Tariq Saeed,
• Anwar Ul-Hamid,
• Bilal Haider Abbasi,
• Nafees Ahmad,
• Waqas Khalid,
• Muhammad Atif,
• Zulqurnain Ali and
• Rashda Abbasi

Beilstein J. Nanotechnol. 2021, 12, 1339–1364, doi:10.3762/bjnano.12.99

• phase of the samples is consistent with the XRD results. The formation of spherical NPs was confirmed by transmission electron microscopy (TEM) (Figure 2a). The nanospheres are uniformally distributed throughout the surface of the samples. High-resolution transmission electron microscopy (HR-TEM) images

• transmission electron microscopy (JEM 2100F) and energy dispersive spectroscopy (TESCAN-VEGA3), respectively. The magnetic behavior was determined by using a physical property measurement system (Quantum Design, USA). The colloidal stability and hydrodynamic size of NPs were studied by using a Zetasizer Nano

Morphology-driven gas sensing by fabricated fractals: A review

• Vishal Kamathe and
• Rupali Nagar

Beilstein J. Nanotechnol. 2021, 12, 1187–1208, doi:10.3762/bjnano.12.88

• -assisted chemical etching was used by Qin et al. [79] to prepare a dendritic array of Si/WO3 NW composites, which was tested for the detection of NO2 gas at room temperature. Figure 17a–e SEM and high-resolution transmission electron microscopy (HR-TEM) images of Si/WO3 NWs. Figure 17f shows the XRD

Self-assembly of amino acids toward functional biomaterials

• Huan Ren,
• Lifang Wu,
• Lina Tan,
• Yanni Bao,
• Yuchen Ma,
• Yong Jin and
• Qianli Zou

Beilstein J. Nanotechnol. 2021, 12, 1140–1150, doi:10.3762/bjnano.12.85

• mechanisms. Scanning electron microscopy and transmission electron microscopy images show that the assembly is layered and has a three-dimensional spherical structure with porous and stacked nanorods (width 50 nm, length 200 nm). During the self-assembly process, tetrakis(4-sulfonatophenyl)porphine and

pH-driven enhancement of anti-tubercular drug loading on iron oxide nanoparticles for drug delivery in macrophages

• Karishma Berta Cotta,
• Sarika Mehra and
• Rajdip Bandyopadhyaya

Beilstein J. Nanotechnol. 2021, 12, 1127–1139, doi:10.3762/bjnano.12.84

• ) measurements using a ZetaSizer (Malvern Instruments, UK). The refractive index and temperature used for the size measurement was 2.34 and 25 °C, respectively. Three replicates were measured for each sample. In addition, the nanoparticle diameter was also measured from transmission electron microscopy (TEM

• nanoparticles. (a) Dynamic light scattering plot of number (%) v/s size (nm) of the nanoparticles in solution at the end of synthesis (n = 3). (b) Transmission electron microscopy image with a 50 nm scale bar. (c) X-ray diffraction plot indicating the Bragg’s 2θ diffraction angles identical to peaks observed

• synthesis (n = 3). (b) Transmission electron microscopy image with a 50 nm scale bar. (c) X-ray diffraction pattern indicating the Bragg’s angle corresponding to those observed in iron oxide. (d) FTIR plot of transmittance v/s wavenumber depicting functional groups of iron oxide. Drug release profile over

First-principles study of the structural, optoelectronic and thermophysical properties of the π-SnSe for thermoelectric applications

• Muhammad Atif Sattar,
• Najwa Al Bouzieh,
• Maamar Benkraouda and
• Noureddine Amrane

Beilstein J. Nanotechnol. 2021, 12, 1101–1114, doi:10.3762/bjnano.12.82

• transmission electron microscopy. As SnS and SnSe share a lot in common, both chemically and structurally, an experimental study verified that the π-SnS prototype exists in the form of π-SnSe. The phase stability of π-SnSe is also confirmed by Golan et al. [47]. By using density functional theory (DFT

Assessment of the optical and electrical properties of light-emitting diodes containing carbon-based nanostructures and plasmonic nanoparticles: a review

• Keshav Nagpal,
• Erwan Rauwel,
• Frédérique Ducroquet and
• Protima Rauwel

Beilstein J. Nanotechnol. 2021, 12, 1078–1092, doi:10.3762/bjnano.12.80

• of 20 mA/cm2. Similarly, the roles of Ag-doped ZnO and pristine ZnO as EIL in the imidazole organic EML-based HyLED were compared [61]. The transmission electron microscopy (TEM) images of Figure 8 illustrate that the pristine ZnO NP are larger (≈50 nm) than the Ag-doped ZnO (≈15 nm). In addition

• AIP Publishing. This content is not subject to CC BY 4.0. Transmission electron microscopy images for (a) pristine ZnO and (b) 2–3% Ag-doped ZnO. Figure 8a and Figure 8b were adapted from [61], J. Photochem. Photobiol. A, vol. 325, by J. Jayabharathi; A. Prabhakaran; V. Thanikachalam; M. Sundharesan

Revealing the formation mechanism and band gap tuning of Sb₂S₃ nanoparticles

• Maximilian Joschko,
• Franck Yvan Fotue Wafo,
• Christina Malsi,
• Danilo Kisić,
• Ivana Validžić and
• Christina Graf

Beilstein J. Nanotechnol. 2021, 12, 1021–1033, doi:10.3762/bjnano.12.76

• different reaction time points were characterized by transmission electron microscopy (TEM, Figure 1a–c) and scanning electron microscopy (SEM, Figure 1d–f). The images show that small nanoparticles (type I) were formed about 2 min (Figure 1a) after injecting the antimony precursor Sb-EHA. The bright orange

A Au/CuNiCoS₄/p-Si photodiode: electrical and morphological characterization

• Adem Koçyiğit,
• Adem Sarılmaz,
• Teoman Öztürk,
• Faruk Ozel and
• Murat Yıldırım

Beilstein J. Nanotechnol. 2021, 12, 984–994, doi:10.3762/bjnano.12.74

• transmission electron microscopy (HR-TEM), and energy-dispersive X-ray spectroscopy (EDS). The XRD, EDS, and HR-TEM analyses confirmed the successful synthesis of CuNiCoS4. The obtained CuNiCoS4 thiospinel nanocrystals were tested for photodiode and capacitance applications as interfacial layer between Au and

Is the Ne operation of the helium ion microscope suitable for electron backscatter diffraction sample preparation?

• Annalena Wolff

Beilstein J. Nanotechnol. 2021, 12, 965–983, doi:10.3762/bjnano.12.73

• , defects such as interstitials or vacancies can be created [23]. This can induce a significant amount of crystal structure alterations in a sample and thus artefacts. While these artefacts are well recognized for transmission electron microscopy (TEM) lamella preparation, in which the lamella preparation

• transmission electron microscopy (STEM), TEM, TEM selected area electron diffraction (SAED), and TEM dark-field (DF) measurements. The results for each experiment are compared to those of a non-irradiated area of the Cu TEM grid. Monte Carlo simulations of the occurring ion–solid interactions are evaluated to

The role of convolutional neural networks in scanning probe microscopy: a review

• Ido Azuri,
• Irit Rosenhek-Goldian,
• Neta Regev-Rudzki,
• Georg Fantner and
• Sidney R. Cohen

Beilstein J. Nanotechnol. 2021, 12, 878–901, doi:10.3762/bjnano.12.66

• learning was also applied to reduce noise and increase the resolution in scanning electron microscopy images. An approach for creating a training dataset of low- and high-resolution image pairs from a single image, was developed by using deep learning to up-sample scanning transmission electron microscopy

Silver nanoparticles nucleated in NaOH-treated halloysite: a potential antimicrobial material

• Yuri B. Matos,
• Rodrigo S. Romanus,
• Mattheus Torquato,
• Edgar H. de Souza,
• Rodrigo L. Villanova,
• Marlene Soares and
• Emilson R. Viana

Beilstein J. Nanotechnol. 2021, 12, 798–807, doi:10.3762/bjnano.12.63

• studied the nucleation of silver on halloysite substrates modified by chemical treatment with NaOH. The resulting stabilized Ag-NPs were characterized by X-ray diffraction, transmission electron microscopy, and energy-dispersive X-ray spectroscopy. The nucleation was characterized by thermogravimetric

• . Transmission electron microscopy (TEM) was performed in a Jeol JEM-1400 plus (480 keV), energy-dispersive X-ray spectroscopy (EDS) and scanning electron microscopy (SEM) in a Zeiss EVO MA15, and thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) in a simultaneous thermal analyzer

Fate and transformation of silver nanoparticles in different biological conditions

• Barbara Pem,
• Marija Ćurlin,
• Darija Domazet Jurašin,
• Valerije Vrček,
• Rinea Barbir,
• Vedran Micek,
• Raluca M. Fratila,
• Jesus M. de la Fuente and
• Ivana Vinković Vrček

Beilstein J. Nanotechnol. 2021, 12, 665–679, doi:10.3762/bjnano.12.53

• implementing light scattering (dynamic and electrophoretic) techniques, spectroscopy (UV–vis, atomic absorption, nuclear magnetic resonance) and transmission electron microscopy. The obtained results demonstrated that AgNPs may transform very quickly during their journey through different biological conditions

• absorption spectroscopy (GF-AAS), nuclear magnetic resonance (NMR) spectroscopy, and transmission electron microscopy (TEM) experiments. Physicochemical characteristics of freshly prepared AgNPs Freshly prepared AgNPs coated with PVP, sodium bis(2-ethylhexyl)sulfosuccinate (AOT), and poly(ʟ-lysine) (PLL

• . The results are presented as % of the dissolved Ag fraction compared to the total Ag content in AgNP suspensions before filtration. Transmission electron microscopy was performed for different AgNPs dispersed in PBS, mCYS, and mGSH media at a concentration of 10 mg Ag/L after 30 min of incubation. The

A review of defect engineering, ion implantation, and nanofabrication using the helium ion microscope

• Frances I. Allen

Beilstein J. Nanotechnol. 2021, 12, 633–664, doi:10.3762/bjnano.12.52

• beam milling that were inspected by transmission electron microscopy (TEM). In this way, the microstructural effect of increasing the helium ion-induced defect density was probed, and threshold doses for a series of structural changes, such as amorphization and subsurface swelling, were established

Stability and activity of platinum nanoparticles in the oxygen electroreduction reaction: is size or uniformity of primary importance?

• Kirill O. Paperzh,
• Anastasia A. Alekseenko,
• Vadim A. Volochaev,
• Ilya V. Pankov,
• Olga A. Safronenko and
• Vladimir E. Guterman

Beilstein J. Nanotechnol. 2021, 12, 593–606, doi:10.3762/bjnano.12.49

• University, "High-Resolution Transmission Electron Microscopy” Shared Use Center, 344090, 194/2 Stachki st., Rostov-on-Don, Russia 10.3762/bjnano.12.49 Abstract Platinum–carbon catalysts are widely used in the manufacturing of proton-exchange membrane fuel cells. Increasing Pt/C activity and stability is an

• distributions were also studied by transmission electron microscopy (TEM). The TEM images were obtained using a JEOL JEM F200 microscope (voltage 200 kV, current 12–15 μA, CFEG). To prepare a sample for measurements, 0.5 mg of the catalyst was placed into 1 mL of isopropanol and dispersed by ultrasound for 10

• assignment in the field of scientific activity No 0852-2020-0019). Acknowledgements The authors are grateful to Mr. Nikulin A.Yu. for assistance in the XRD pattern registration and to the “Shared Use Center High-Resolution Transmission Electron Microscopy” (SFedU) for conducting the TEM studies.

The preparation temperature influences the physicochemical nature and activity of nanoceria

• Robert A. Yokel,
• Wendel Wohlleben,
• Johannes Georg Keller,
• Matthew L. Hancock,
• Jason M. Unrine,
• D. Allan Butterfield and
• Eric A. Grulke

Beilstein J. Nanotechnol. 2021, 12, 525–540, doi:10.3762/bjnano.12.43

• characterizations. Transmission electron microscopy (TEM) and high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) were conducted of NM-212 dispersed in DI water, sonicated for 10 min in a bath, and captured on 300 mesh lacey carbon copper grids dipped into the dispersion for

• nanoceria and their fate and effects. Transmission electron microscopy and high-angle annular dark-field scanning transmission electron microscopy images of NM-212 and its chemical composition determined by energy-dispersive X-ray spectroscopy. (A, B) TEM images, (B) is a part of (A) at higher magnification

• determinations. Non-baseline corrected Fourier-transform infrared spectroscopy of NM-212 with peaks indicated by dashed lines at 1630, 1420, and 1320 cm−1. Transmission electron microscopy image of calcined solvothermally synthesized nanoceria. Electron energy loss spectroscopy of calcined solvothermally

Surface-enhanced Raman scattering of water in aqueous dispersions of silver nanoparticles

• Paulina Filipczak,
• Krzysztof Hałagan,
• Jacek Ulański and
• Marcin Kozanecki

Beilstein J. Nanotechnol. 2021, 12, 497–506, doi:10.3762/bjnano.12.40

• -resolution transmission electron microscopy (TEM) analysis was performed to estimate the size and identify the shape of the nanoparticles (see Figure 1). The nanoparticles in the AgNPs blue sample had a triangular prism shape with an estimated average size of 34 ± 14 nm, while in the AgNPs yellow sample, the

Boosting of photocatalytic hydrogen evolution via chlorine doping of polymeric carbon nitride

• Malgorzata Aleksandrzak,
• Michalina Kijaczko,
• Wojciech Kukulka,
• Daria Baranowska,
• Martyna Baca,
• Beata Zielinska and
• Ewa Mijowska

Beilstein J. Nanotechnol. 2021, 12, 473–484, doi:10.3762/bjnano.12.38

• the morphology of the prepared materials, presented in Figure 1, was performed by transmission electron microscopy (TEM). The images of pristine PCN demonstrate the layered structure with a tendency to fold and aggregate. They also show several stacking layers, indicating the planar graphitic-like

• Ar as a carrier). Each catalyst was tested for 3 h. Every hour, 100 µL of gas was withdrawn from the reactor and injected into the gas chromatograph to measure the amount of H2 evolved. TEM images of PCN (a, b) and Cl-PCN (c, d). Scanning transmission electron microscopy image of Cl-PCN (e) and

Rapid controlled synthesis of gold–platinum nanorods with excellent photothermal properties under 808 nm excitation

• Jialin Wang,
• Qianqian Duan,
• Min Yang,
• Boye Zhang,
• Li Guo,
• Pengcui Li,
• Wendong Zhang and
• Shengbo Sang

Beilstein J. Nanotechnol. 2021, 12, 462–472, doi:10.3762/bjnano.12.37

• in all experiments. Instruments The absorption spectra were measured on a UV–vis–NIR spectrophotometer (UV-8000A, 190–1200 nm, Metash, China). Transmission electron microscopy (TEM) images, morphology, and size of nanoparticles were obtained with a transmission electron microscope (JEOL 2100F, 200 kV

A review on nanostructured silver as a basic ingredient in medicine: physicochemical parameters and characterization

• Gabriel M. Misirli,
• Kishore Sridharan and
• Shirley M. P. Abrantes

Beilstein J. Nanotechnol. 2021, 12, 440–461, doi:10.3762/bjnano.12.36

• experimentally analyzed by UV–vis extinction spectra and transmission electron microscopy (TEM). The rate of photo-oxidation in spherical AgNPs was homogeneous and surprisingly inhomogeneous in the case of cubic AgNPs, which was attributed to the difference in morphology. The noticeable formation of small NPs

• interactions with cells and living organisms. Multidisciplinary teams are essential to pave the way for the future use of AgNPs in living beings. Scanning electron microscope (SEM) with different morphologies: (A) bipyramidal, (B) nanowires, (C) nanocubes and transmission electron microscopy (TEM) micrographs

Solution combustion synthesis of a nanometer-scale Co₃O₄ anode material for Li-ion batteries

• Monika Michalska,
• Huajun Xu,
• Qingmin Shan,
• Shiqiang Zhang,
• Yohan Dall'Agnese,
• Yu Gao,
• Amrita Jain and
• Marcin Krajewski

Beilstein J. Nanotechnol. 2021, 12, 424–431, doi:10.3762/bjnano.12.34

• the Raman spectrometer as well as Mr. Ryszard Strzałkowski from the Institute of Fundamental Technological Research Polish Academy of Sciences for his support in the performance of transmission electron microscopy investigations.

Spontaneous shape transition of Mn_xGe_1−x islands to long nanowires

• S. Javad Rezvani,
• Luc Favre,
• Gabriele Giuli,
• Yiming Wubulikasimu,
• Isabelle Berbezier,
• Augusto Marcelli,
• Luca Boarino and
• Nicola Pinto

Beilstein J. Nanotechnol. 2021, 12, 366–374, doi:10.3762/bjnano.12.30

• (SEM), X-ray diffraction (XRD), and high-resolution transmission electron microscopy (HRTEM). We demonstrate that the thickness of the Mn layer and the annealing conditions finely control the shape transition, resulting in NWs up to ≃1.5 μm length with uniform width and homogeneous composition

Nickel nanoparticle-decorated reduced graphene oxide/WO₃ nanocomposite – a promising candidate for gas sensing

• Ilka Simon,
• Alexandr Savitsky,
• Rolf Mülhaupt,
• Vladimir Pankov and
• Christoph Janiak

Beilstein J. Nanotechnol. 2021, 12, 343–353, doi:10.3762/bjnano.12.28

• diluted 1:100. Transmission electron microscopy, TEM was performed with a FEI Tecnai G2 F20 electron microscope [68] operated at 200 kV accelerating voltage or FEI Titan 80-300 TEM operated at 300 kV accelerating voltage [69]. Conventional TEM images were recorded with a Gatan UltraScan 1000P detector