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Search for "TGA" in Full Text gives 133 result(s) in Beilstein Journal of Nanotechnology.
A facile approach to nanoarchitectured three-dimensional graphene-based Li–Mn–O composite as high-power cathodes for Li-ion batteries
Beilstein J. Nanotechnol. 2012, 3, 513–523, doi:10.3762/bjnano.3.59
- precursors. The thermal gravimetric analysis (TGA) results (see Supporting Information File 1, Figure S2a) show that the IMO:G are 0.82, 1.34 and 2.57 for samples prepared with MnSO4 molar concentrations of 0.15, 0.3 and 0.6 M, respectively. For Mn2O3/graphene samples with higher IMO:G values, the shape of
- diffraction peaks using Scherrer’s equation. This grain size is much smaller than that of Mn2O3, which is possibly due to a recrystallization process. No impurity phase is detectable using XRD. After the lithiation process, the TGA results (see Supporting Information File 1, Figure S2b) indicate that the
- JEOL JEM-2100 operating at 200 kV. Raman spectra were obtained on a WITec CRM 200 with a wavelength of 488 nm and a spot size of 0.5 mm. Thermogravimetry analyses were carried out on TGA Q500 from 298–1073 K at a heating rate of 10 K·min−1 in air. The analyses of Li/Mn ratio was performed on
Surface functionalization of aluminosilicate nanotubes with organic molecules
Beilstein J. Nanotechnol. 2012, 3, 82–100, doi:10.3762/bjnano.3.10
- thermogravimetric analysis (TGA) [40]. The subsequent ARGET ATRP was carried out by using ascorbic acid (AA) as the reducing agent and anisole as the solvent. Ascorbic acid is insoluble in anisole, hence, the reduction of the Cu(II) complex takes place at the surface of solid ascorbic acid. The slow reaction rate
Template-assisted formation of microsized nanocrystalline CeO2 tubes and their catalytic performance in the carboxylation of methanol
Beilstein J. Nanotechnol. 2011, 2, 776–784, doi:10.3762/bjnano.2.86
- spectroscopy (PL), as well as thermogravimetric analysis (TGA). Its catalytic performance was studied in the direct carboxylation of methanol with carbon dioxide leading to dimethyl carbonate [(CH3O)2CO, DMC], which is widely employed as a phosgene and dimethyl sulfate substitute, and as well as a fuel
- Kα1) instruments. Thermogravimetric analysis (TGA) was performed on a Netzsch TG 209 F1 instrument coupled with a QMS 403 C mass spectrometer. For BET measurements a NOVA 3000e (Quantachrome) was used. For PLE measurements, Horiba, Fluorog-3 (Xe, excitation wavelength 325 nm) was used. For UV–vis
- nanostructured ceria (obtained with addition of Pluronic P123® to the sol). TGA measurements of bare PMMA fibres (PMMA, solid line), a PMMA/sol without Pluronic P123® (PMMA/sol, dashed-dotted line) and a PMMA/sol containing Pluronic P123® (PMMA/sol + P123, dotted line). PL spectrum of microsized ceria tubes
Investigation on structural, thermal, optical and sensing properties of meta-stable hexagonal MoO3 nanocrystals of one dimensional structure
Beilstein J. Nanotechnol. 2011, 2, 585–592, doi:10.3762/bjnano.2.62
- crystallite size and one dimensional growth. Usually, the α-MoO3 is a stable structure formed at a higher temperature relative to the metastable h-MoO3. Thus, there is a phase transformation from h-MoO3 to α-MoO3 at 400 °C, which is inferred from TGA/DTA studies [14][16]. With an increase in temperature, the
- coordinated water and ammonia molecules from the internal structure of the MoO3 material, which promotes an irreversible phase transformation from the hexagonal to the orthorhombic structure [14][16]. The powder subjected to TGA measurements was subjected to XRD analysis, and the result confirmed that above
Towards multiple readout application of plasmonic arrays
Beilstein J. Nanotechnol. 2011, 2, 501–508, doi:10.3762/bjnano.2.54
- sequence NS151: amino-link-5'-TTT TTT CAG CAT GGG CTC CTT GAT TCT ATG-3'; three mismatch sequence NS153: amino-link-5'-TTT TTT CAG CAT TAT CTC CTT GAT TCT ATG-3'; negative control N7 5'-ACT GAC TGA CTG ACT GAC TGA CTG GGC GGC GAC CT-3'-amino-link) was prepared as a 1 µM solution in 5× phosphate buffered
Dynamics of capillary infiltration of liquids into a highly aligned multi-walled carbon nanotube film
Beilstein J. Nanotechnol. 2011, 2, 311–317, doi:10.3762/bjnano.2.36
- without further treatment. The nanotube density in the HACNT film was measured using ImageJ® on an SEM image (sample with 100 nanotubes). The average diameters of MWCNTs were measured on TEM images of 100 nanotubes. Free volume of the HACNT film was measured via TGA experiment performed on a completely
Studies towards synthesis, evolution and alignment characteristics of dense, millimeter long multiwalled carbon nanotube arrays
Beilstein J. Nanotechnol. 2011, 2, 293–301, doi:10.3762/bjnano.2.34
- -graphitic carbon) in the samples prepared at 1100 °C. Thermogravimetric analysis (TGA) measurements were carried out for the synthesized CNT material grown at 650 and 1100 °C in a dry air atmosphere with a heating rate of 10 °C/min and show the typical temperature behavior of high quality CNTs (Figure 8b
- microscopy TEM, AFM, EDS, TGA and Raman spectroscopy. SEM images of aligned CNTs prepared at different temperatures (a) 650 °C, (b) 750 °C, (c) 850 °C, (d) 950 °C, (e) 1050 °C, and (f) 1100 °C. (a) SEM image of aligned CNTs on a quartz substrate. (b) SEM image of an isolated mat collected from the inner wall
- °C. (a) Raman spectra and (b) TGA curves of aligned CNTs prepared at 650 and 1100 °C.
Pore structure and surface area of silica SBA-15: influence of washing and scale-up
Beilstein J. Nanotechnol. 2011, 2, 110–118, doi:10.3762/bjnano.2.13
- more effective in removing the template from the SBA-15 framework, although the Pluronic 123 cannot be removed completely from the SBA-15 by washing, as shown by thermogravimetric analysis (TGA) [22]. Also the more effective template removal by ethanol is connected with shrinkage of the SBA-15
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