Structure and electrochemical performance of electrospun-ordered porous carbon/graphene composite nanofibers

• Yi Wang,
• Yanhua Song,
• Chengwei Ye and
• Lan Xu

Beilstein J. Nanotechnol. 2020, 11, 1280–1290, doi:10.3762/bjnano.11.112

• electron microscopy (SEM) under a field-emission scanning electron microscope (FE-SEM) (Hitachi, S4800, Japan). The structural characteristics of the CNFs were observed via transmission electron microscopy (TEM) (FEI, Tecnai G20, Japan). The diameter values of the CNFs were measured using ImageJ software

• . Afterwards, the tube furnace was cooled to room temperature to obtain CCGNFs, which could be directly used as electrodes. For comparison, disordered CGCNFs were also prepared using electrospinning and carbonization techniques. Material characterization The morphology of the CNFs was investigated via scanning

Ultrasensitive detection of cadmium ions using a microcantilever-based piezoresistive sensor for groundwater

• Dinesh Rotake,
• Anand Darji and
• Nitin Kale

Beilstein J. Nanotechnol. 2020, 11, 1242–1253, doi:10.3762/bjnano.11.108

• ) LOD, which is well below the WHO limit for cadmium ions. The paper describes the methodology, the formation of SAMs and their characterization using field-emission scanning electron microscopy (FESEM), the use of the portable experimental platform with the MEMS-based piezoresistive device to selective

Gas sorption porosimetry for the evaluation of hard carbons as anodes for Li- and Na-ion batteries

• Yuko Matsukawa,
• Fabian Linsenmann,
• Maximilian A. Plass,
• George Hasegawa,
• Katsuro Hayashi and
• Tim-Patrick Fellinger

Beilstein J. Nanotechnol. 2020, 11, 1217–1229, doi:10.3762/bjnano.11.106

• . The morphologies of the HT samples are very similar (Figure 1), but show a different morphology compared to the RF carbons (Supporting Information File 1, Figure S6). Scanning electron microscopy (SEM) imaging reveals spherical particles, morphologically similar to previously reported HCs derived from

• Ventus 532 nm laser using a power of 25 mW at an exposure time of 10 s), respectively. To investigate the morphology of the samples, scanning electron microscopy (SEM) measurements were performed on a scanning electron microscope (NEOSCOPE JCM-6000, JEOL, Japan, equipped with a tungsten filament at 15 kV

High permittivity, breakdown strength, and energy storage density of polythiophene-encapsulated BaTiO₃ nanoparticles

• Adnanullah Khan,
• Amir Habib and
• Adeel Afzal

Beilstein J. Nanotechnol. 2020, 11, 1190–1197, doi:10.3762/bjnano.11.103

• mixture. All materials including BTO, BTO-PTh, and PTh are characterized using Fourier-transform infrared spectroscopy (Nicolet 520 FTIR spectrophotometer) and X-ray diffraction (STOE STADI P X-ray diffractometer). The morphology of BTO and BTO-PTh nanoparticles is studied using scanning electron

• microscopy (JEOL JSM 6490LA SEM) and atomic force microscopy (JSPM-5200 scanning probe microscope). Electrical properties of the bulk materials are measured under ambient conditions with a Wayne Kerr 6505B precision impedance analyzer and a Hipotronics HD103 3kV DC Hipot Tester. Results and Discussion

Revealing the local crystallinity of single silicon core–shell nanowires using tip-enhanced Raman spectroscopy

• Marius van den Berg,
• Ardeshir Moeinian,
• Arne Kobald,
• Yu-Ting Chen,
• Anke Horneber,
• Steffen Strehle,
• Alfred J. Meixner and
• Dai Zhang

Beilstein J. Nanotechnol. 2020, 11, 1147–1156, doi:10.3762/bjnano.11.99

• characterizing the SiNWs using helium-ion microscopy and E. Nadler for characterizing the Au tip using scanning electron microscopy. We also acknowledge the use of the WSXM software, which is used for illustrating the optical and topography images [44].

Gram-scale synthesis of splat-shaped Ag–TiO₂ nanocomposites for enhanced antimicrobial properties

• Mohammad Jaber,
• Asim Mushtaq,
• Kebiao Zhang,
• Jindan Wu,
• Dandan Luo,
• Zihan Yi,
• M. Zubair Iqbal and
• Xiangdong Kong

Beilstein J. Nanotechnol. 2020, 11, 1119–1125, doi:10.3762/bjnano.11.96

• Rigaku D/Max 2500 powder diffractometer with Cu Kα radiation (λ = 1.5406 Å). Scanning electron microscopy (SEM, JSM5610LV, JEOL, Japan) was used to observed the morphology of the Ag–TiO2 NPs. The sample components were examined by energy-dispersive X-ray spectroscopy. Fourier-transform infrared

Plant growth regulation by seed coating with films of alginate and auxin-intercalated layered double hydroxides

• Vander A. de Castro,
• Valber G. O. Duarte,
• Danúbia A. C. Nobre,
• Geraldo H. Silva,
• Vera R. L. Constantino,
• Frederico G. Pinto,
• Willian R. Macedo and
• Jairo Tronto

Beilstein J. Nanotechnol. 2020, 11, 1082–1091, doi:10.3762/bjnano.11.93

• analytical techniques, including powder X-ray diffraction, thermogravimetric analysis coupled to differential scanning calorimetry and mass spectrometry, specific surface area measurement, and scanning electron microscopy. Bioassays were performed with the seeds coated with the composite film to assess the

• with indefinitely coherent fragments [28][29]. The volume and average pore diameter values are characteristic of a mesoporous material. Scanning electron microscopy (SEM) images of NAA and ZnAl-NAA-LDH, presented in Figure 4, show the presence of particles with a smooth surface, probably resulting from

Microwave-induced electric discharges on metal particles for the synthesis of inorganic nanomaterials under solvent-free conditions

• Vijay Tripathi,
• Harit Kumar,
• Anubhav Agarwal and
• Leela S. Panchakarla

Beilstein J. Nanotechnol. 2020, 11, 1019–1025, doi:10.3762/bjnano.11.86

• of Cu2O after acid treatment, while the majority of Cu remains in the metallic form (Figure 1a). Scanning electron microscopy (SEM) images of copper powder before and after acid treatment are shown in Figure 1b and Figure 1c, respectively. The SEM image clearly shows the sharp edges on acid-treated

• supernatant solution is collected for further characterization. Characterization of products The reaction products are characterized by X-ray diffraction (PANanalytical X’pert PRO), field-emission scanning electron microscopy (JEOL JSM 7600F, combined with energy-dispersive spectroscopy (EDS)), transmission

Gas-sensing features of nanostructured tellurium thin films

• Dumitru Tsiulyanu

Beilstein J. Nanotechnol. 2020, 11, 1010–1018, doi:10.3762/bjnano.11.85

• different operating temperatures with respect to scanning electron microscopy and X-ray diffraction analyses. It was shown that both types of films interacted with nitrogen dioxide, which resulted in a decrease of electrical conductivity. The gas sensitivity, as well as the response and recovery times

Wet-spinning of magneto-responsive helical chitosan microfibers

• Dorothea Brüggemann,
• Johanna Michel,
• Naiana Suter,
• Matheus Grande de Aguiar and
• Michael Maas

Beilstein J. Nanotechnol. 2020, 11, 991–999, doi:10.3762/bjnano.11.83

• were prepared by wet-spinning and coagulation in an ethanol bath. Thereby, no toxic components were introduced into the wet-spun chitosan fibers. After drying, the helical fibers had a diameter of approximately 130 µm. Scanning electron microscopy analysis of wet-spun helices revealed that the magnetic

• collected from the coagulation bath and reeled around a 0.3 mm diameter magnetic needle. Subsequently, a full automatization of this process was achieved by using a Lego Mindstorms NXT setup. Scanning electron microscopy Morphological analysis of the IOP-embedded chitosan fibers was performed under a

Electrochemical nanostructuring of (111) oriented GaAs crystals: from porous structures to nanowires

• Elena I. Monaico,
• Eduard V. Monaico,
• Veaceslav V. Ursaki,
• Shashank Honnali,
• Vitalie Postolache,
• Karin Leistner,
• Kornelius Nielsch and
• Ion M. Tiginyanu

Beilstein J. Nanotechnol. 2020, 11, 966–975, doi:10.3762/bjnano.11.81

• reference electrode and the sample as working electrode. The anodization was performed in galvanostatic as well as potentiostatic regimes at room temperature (T = 23 °C). Analysis of morphology and chemical composition of the anodized GaAs crystals was carried out using scanning electron microscopy (Zeiss

A 3D-polyphenylalanine network inside porous alumina: Synthesis and characterization of an inorganic–organic composite membrane

• Jonathan Stott and
• Jörg J. Schneider

Beilstein J. Nanotechnol. 2020, 11, 938–951, doi:10.3762/bjnano.11.78

• hydrolyzed monomers or an alternative polymerization mechanism [40][41]. The characterization of these composite materials was performed by NIR-spectroscopy (NIR), water contact angle measurements (CA), scanning electron microscopy (SEM) and thermogravimetric (TG) measurements. Mid- and near-infrared

• electron microscopy (SEM), near-infrared spectroscopy (NIR) and contact angle measurements (CA) reveals a change in morphology of the grafted polymer films, which is due to the rearrangement of the secondary structure of the polypeptides. No significant loss of the surface-grafted polypeptides was

• -dimensional fibrillar network with intrinsic porosity was formed in DCM, whereas in THF, a dense and smooth polypeptide film was observed. A post-treatment with a mixture of chloroform and dichloroacetic acid leads to rearrangement of the morphology of the grafted polymer films. The analysis by scanning

Band tail state related photoluminescence and photoresponse of ZnMgO solid solution nanostructured films

• Vadim Morari,
• Aida Pantazi,
• Nicolai Curmei,
• Vitalie Postolache,
• Emil V. Rusu,
• Marius Enachescu,
• Ion M. Tiginyanu and
• Veaceslav V. Ursaki

Beilstein J. Nanotechnol. 2020, 11, 899–910, doi:10.3762/bjnano.11.75

• the composition range x = 0.00–0.40 has been prepared by sol–gel spin coating on Si substrates with a post-deposition thermal treatment in the temperature range of 400–650 °C. The morphology of the films was investigated by scanning electron microscopy and atomic force microscopy while their light

A set of empirical equations describing the observed colours of metal–anodic aluminium oxide–Al nanostructures

• Cristina V. Manzano,
• Jakob J. Schwiedrzik,
• Gerhard Bürki,
• Laszlo Pethö,
• Johann Michler and
• Laetitia Philippe

Beilstein J. Nanotechnol. 2020, 11, 798–806, doi:10.3762/bjnano.11.64

• (yielding to the same porosity), changing only the second anodization time (from 120 to 600 s) to obtain different film thicknesses (from 209 ± 12 nm to 380 ± 15 nm). Focused ion beam (FIB) milling and field-emission scanning electron microscopy (FESEM) imaging were used to accurately determine the

Nickel nanoparticles supported on a covalent triazine framework as electrocatalyst for oxygen evolution reaction and oxygen reduction reactions

• Secil Öztürk,
• Yu-Xuan Xiao,
• Dennis Dietrich,
• Beatriz Giesen,
• Juri Barthel,
• Jie Ying,
• Xiao-Yu Yang and
• Christoph Janiak

Beilstein J. Nanotechnol. 2020, 11, 770–781, doi:10.3762/bjnano.11.62

• for CTF-1-600 (see Table S2, Supporting Information File 1, for details). Elemental analyses, thermogravimetric analyses (TGA) and scanning electron microscopy (SEM) characterization data of the materials can be found in Table S1 and Figures S3–S5 in Supporting Information File 1. Synthesis and

• suppressed conductivity detection. Karl-Fischer titration (KFT) was carried out with an ECH/ANALYTIK JENA AQUA 40:00 Karl Fischer titrator. A Carbolite Gero tube furnace has been used for the CTF synthesis. Scanning electron microscopy (SEM) images were recorded with a Jeol JSM-65 10 LV QSEM advanced

Structural optical and electrical properties of a transparent conductive ITO/Al–Ag/ITO multilayer contact

• Aliyu Kabiru Isiyaku,
• Ahmad Hadi Ali and
• Nafarizal Nayan

Beilstein J. Nanotechnol. 2020, 11, 695–702, doi:10.3762/bjnano.11.57

• IAAI and ITO films was further analyzed by field-emission scanning electron microscopy (FESEM, 5.0 kV, 100000× magnification). Figure 4 shows FESEM images of the as-deposited and annealed IAAI and ITO films. The as-deposited IAAI and ITO films show a smooth and continuous surface with small grains and

• carried out using the Nanoscope Analysis software. All films were scanned over an area of 1 μm × 1 μm. Field-emission scanning electron microscopic analyses The surface morphology of the prepared thin films was further studied using field-emission scanning electron microscopy (FESEM). A FESEM JEOL JSM

A novel dry-blending method to reduce the coefficient of thermal expansion of polymer templates for OTFT electrodes

• Xiangdong Ye,
• Bo Tian,
• Yuxuan Guo,
• Fan Fan and
• Anjiang Cai

Beilstein J. Nanotechnol. 2020, 11, 671–677, doi:10.3762/bjnano.11.53

• the silicon template. Characterization The surface morphology of the PDMS/SiO2 composite template and the OTFT electrodes was investigated via scanning electron microscopy (SEM, JSM-6390a, Japan). The thermal expansion of the PDMS/SiO2 composite template was examined using a thermomechanical analyzer

Exfoliation in a low boiling point solvent and electrochemical applications of MoO₃

• Matangi Sricharan,
• Bikesh Gupta,
• Sreejesh Moolayadukkam and
• H. S. S. Ramakrishna Matte

Beilstein J. Nanotechnol. 2020, 11, 662–670, doi:10.3762/bjnano.11.52

• preheated oven. The remaining MoO3 powder in the beaker was weighed to determine the concentration. The morphology of MoO3 flakes was characterized using field-emission scanning electron microscopy (FESEM; Tescan Mira3), transmission electron microscopy (TEM; FEI Talos, 200 kV) and atomic force microsopy

Preparation, characterization and photocatalytic performance of heterostructured CuO–ZnO-loaded composite nanofiber membranes

• Wei Fang,
• Liang Yu and
• Lan Xu

Beilstein J. Nanotechnol. 2020, 11, 631–650, doi:10.3762/bjnano.11.50

• investigated using scanning electron microscopy (SEM, Hitachi S-4800, Japan). The matrix morphology and fiber diameter distribution were determined using the Image J software (National Institute of Mental Health, Bethesda, Maryland, USA). The diameter of 100 randomly selected fibers in each sample were chosen

Silver-decorated gel-shell nanobeads: physicochemical characterization and evaluation of antibacterial properties

• Marta Bartel,
• Katarzyna Markowska,
• Marcin Strawski,
• Krystyna Wolska and
• Maciej Mazur

Beilstein J. Nanotechnol. 2020, 11, 620–630, doi:10.3762/bjnano.11.49

• –Hinton broth (MH; Biocorp Poland). The medium was supplemented with glucose when required (Chempur, Poland). For the analysis of bacterial viability the LIVE/DEAD BacLight bacterial viability kit (Promega) was used. Instrumentation Microscopy Scanning electron microscopy and electron microprobe (EDS

Comparison of fresh and aged lithium iron phosphate cathodes using a tailored electrochemical strain microscopy technique

• Matthias Simolka,
• Hanno Kaess and
• Kaspar Andreas Friedrich

Beilstein J. Nanotechnol. 2020, 11, 583–596, doi:10.3762/bjnano.11.46

• category of destructive and post-mortem methods, scanning electron microscopy (SEM) is widely applied, due to the deep insights into the material that it can provide, e.g., insights related to structural changes and generated surface layers. In combination with X-ray techniques like energy dispersive

Identification of physicochemical properties that modulate nanoparticle aggregation in blood

• Ludovica Soddu,
• Duong N. Trinh,
• Eimear Dunne,
• Dermot Kenny,
• Giorgia Bernardini,
• Ida Kokalari,
• Arianna Marucco,
• Marco P. Monopoli and
• Ivana Fenoglio

Beilstein J. Nanotechnol. 2020, 11, 550–567, doi:10.3762/bjnano.11.44

• particles re-suspended in ethanol once, centrifuged, and re-suspended in ultrapure water. The procedure was repeated three times. The purified NPs were suspended in ultrapure water and stored at 4 °C until use. Scanning electron microscopy (SEM) The NPs morphology was characterised using scanning electron

• microscopy (SEM), using a Zeiss Evo 50XVP (Assing) instrument. CNPs and SNPs suspensions were diluted up to 0.05 mg/mL in ultrapure water. A volume of 20 μL of the diluted suspensions was mounted on aluminium stubs using double-sided adhesive carbon tape and silicon wafers. The samples were dried overnight

Multilayer capsules made of weak polyelectrolytes: a review on the preparation, functionalization and applications in drug delivery

• Varsha Sharma and
• Anandhakumar Sundaramurthy

Beilstein J. Nanotechnol. 2020, 11, 508–532, doi:10.3762/bjnano.11.41

• applied to a variety of PEs. Multilayer capsules formed on such a variety of cores can reveal specific characteristics and are mostly studied using microscopy techniques such as scanning electron microscopy (SEM) and transmission electron microscopy (TEM) to observe their morphological changes. Moreover

Evolution of Ag nanostructures created from thin films: UV–vis absorption and its theoretical predictions

• Robert Kozioł,
• Marcin Łapiński,
• Paweł Syty,
• Damian Koszelow,
• Wojciech Sadowski,
• Józef E. Sienkiewicz and
• Barbara Kościelska

Beilstein J. Nanotechnol. 2020, 11, 494–507, doi:10.3762/bjnano.11.40

• Narutowicza 11/12, 80-233 Gdansk, Poland 10.3762/bjnano.11.40 Abstract Ag-based plasmonic nanostructures were manufactured by thermal annealing of thin metallic films. Structure and morphology were studied using scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution

Interfacial charge transfer processes in 2D and 3D semiconducting hybrid perovskites: azobenzene as photoswitchable ligand

• Nicole Fillafer,
• Tobias Seewald,
• Lukas Schmidt-Mende and
• Sebastian Polarz

Beilstein J. Nanotechnol. 2020, 11, 466–479, doi:10.3762/bjnano.11.38

• headgroup provides not enough space for the molecule to fit into the structure. The materials were examined by using a combination of methods to study their structure and electronic properties. In Figure 2D the powder X-ray diffraction (PXRD) patterns and the associated scanning electron microscopy (SEM

• silicon substrates were obtained using an X-ray diffractometer (Bruker D8 Discover). Small-angle X-ray scattering (SAXS) patterns were obtained using a Bruker Nanostar. Scanning electron microscopy (SEM) images of drop-cast particles on silicon substrates were obtained using a Zeiss Auriga Crossbeam and a