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Search for "scanning electron microscopy" in Full Text gives 765 result(s) in Beilstein Journal of Nanotechnology. Showing first 200.

Eco-efficient materials for agricultural crops based on a mineral rich in MOR- and HEU-type zeolites

  • Esperanza Yamile de la Nuez-Pantoja,
  • Inocente Rodríguez-Iznaga,
  • Gerardo Rodríguez-Fuentes,
  • Vitalii Petranovskii,
  • Ariel Martínez García,
  • José Juan Calvino Gámez and
  • Daniel Goma Jiménez

Beilstein J. Nanotechnol. 2026, 17, 381–395, doi:10.3762/bjnano.17.26

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  • urea arranged on the surface so that it covers the material and interacts with the zeolitic frameworks, was evidenced by Fourier-transform IR spectroscopy, adsorption measurements, scanning electron microscopy, scanning transmission electron microscopy, and other methods, as well as through culture
  • consequence of the ion exchange processes (Equation 1) occurring during treatment of CLIM with DAP solution, which is in agreement with the data reported in [16][21][42]. Scanning electron microscopy and scanning transmission electron microscopy Microphotography (Figure 5) of natural zeolite (CLIM) revealed
  • , the samples were examined by Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), scanning transmission electron microscopy (STEM), and adsorption measurements based on N2 adsorption isotherms. FTIR spectra were recorded on a Bruker Tensor 27 IR
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Published 26 Feb 2026

Interconnection morphology effects on the radio frequency response of carbon nanotube sponges

  • Manuela Scarselli,
  • Javad Rezvani,
  • Zeno Zuccari,
  • Mattia Scagliotti and
  • Simone Tocci

Beilstein J. Nanotechnol. 2026, 17, 343–351, doi:10.3762/bjnano.17.23

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  • . In particular, we observed that the response of S11 = −22.6 dB around 4.8 GHz from the CNS antenna improved after a mild treatment with ethanol, reaching S11 = −32.6 dB measured after 10 min of waiting. This observed effect is studied in detail with scanning electron microscopy and Raman spectroscopy
  • findings point to a different interpretation related to the morphological effect of ethanol on the CNT mesh [27][29]. A scanning electron microscopy (SEM) study provided insights into the microstructure of the CNT film (Supporting Information File 1, Figure S1) and the sponges (Figure 3). The study
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Published 17 Feb 2026

Beam shaping techniques for pulsed laser ablation in liquids: Unlocking tunable control of nanoparticle synthesis in liquids

  • Sergio Molina-Prados,
  • Nadezhda M. Bulgakova,
  • Alexander V. Bulgakov,
  • Jesus Lancis,
  • Gladys Mínguez Vega and
  • Carlos Doñate-Buendia

Beilstein J. Nanotechnol. 2026, 17, 309–342, doi:10.3762/bjnano.17.22

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Published 16 Feb 2026

Durable antimicrobial activity of fabrics functionalized with zeolite ion-exchanged nanomaterials against Staphylococcus aureus and Escherichia coli

  • Perla Sánchez-López,
  • Kendra Ramirez Acosta,
  • Sergio Fuentes Moyado,
  • Ruben Dario Cadena-Nava and
  • Elena Smolentseva

Beilstein J. Nanotechnol. 2026, 17, 262–274, doi:10.3762/bjnano.17.18

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  • atom % are evaluated regarding their antimicrobial activity against Staphylococcus aureus (Gram-positive) and Escherichia coli (Gram-negative), as well as regarding their physicochemical and mechanical properties. Scanning electron microscopy confirms the uniform distribution and successful
  • ). Scanning electron microscopy confirmed the effective incorporation and uniform distribution of the nanomaterials on the fabric surface, facilitated by a 10% w/w acrylic resin binder. Among the tested materials, silver-based fabrics displayed the highest antibacterial efficacy, followed by copper and zinc
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Published 06 Feb 2026

Multilayered hyperbolic Au/TiO2 nanostructures for enhancing the nonlinear response around the epsilon-near-zero point

  • Fernando Arturo Araiza-Sixtos,
  • Mauricio Gomez-Robles,
  • Rafael Salas-Montiel and
  • Raúl Rangel-Rojo

Beilstein J. Nanotechnol. 2026, 17, 251–261, doi:10.3762/bjnano.17.17

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  • oscillator as a starting material for Au, and with TiO2 with Cody–Lorentz oscillators as starting material for TiO2. Scanning electron microscopy (Hitachi SU8030) was used to obtain the cross-sectional image (below in Figure 4a), with the sample oriented to expose the ENZ material edge to the electron beam
  • the deposited layers. In Table 1, we can see that we have widths for every stack that are different from the ones proposed for the simulated ENZ points. This change in thickness was also seen in scanning electron microscopy (SEM). In Figure 4a we present a SEM image of the ML800 structure; we see that
  • dm = 10 nm gold layer measured using spectral ellipsometry compared to the one reported in literature. We observe that the resulting permittivity is almost similar to the one used for the simulations. (a) Scanning electron microscopy image of the ML800 structure. We see that the deposited layers have
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Published 05 Feb 2026

Comparative study on 3D morphologies of delignified, single tracheids and fibers of five wood species

  • Helen Gorges,
  • Felicitas von Usslar,
  • Cordt Zollfrank,
  • Silja Flenner,
  • Imke Greving,
  • Martin Müller,
  • Clemens F. Schaber,
  • Chuchu Li and
  • Stanislav N. Gorb

Beilstein J. Nanotechnol. 2026, 17, 239–250, doi:10.3762/bjnano.17.16

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  • . Scanning electron microscopy was used to compare the morphology between untreated and delignified fibers and tracheids. X-ray tomography enabled us to reconstruct high-resolution 3D models of delignified single tracheids or fibers, providing information on the pit arrangements. Moreover, delignification
  • species in this study by observation of the structural differences after delignification. Using X-ray tomography, we were able to build 3D models of single fibers and tracheids. Additionally, we imaged untreated and delignified samples using scanning electron microscopy for measuring fiber and tracheid
  • nitrogen and subsequent lyophilization overnight (−45 °C, 0.080 mbar, Christ Alpha 2–4 LDplus, Christ, Osterode, Germany). Scanning electron microscopy Air-dried wood samples of each of the five species (untreated and delignified) were glued onto metal (SEM) stubs and sputter-coated with a 10 nm layer of
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Published 04 Feb 2026

Gold nanoparticle-decorated reduced graphene oxide as a highly effective catalyst for the selective α,β-dehydrogenation of N-alkyl-4-piperidones

  • Brenda Flore Kenyim,
  • Mihir Tzalis,
  • Marilyn Kaul,
  • Robert Oestreich,
  • Aysenur Limon,
  • Chancellin Pecheu Nkepdep and
  • Christoph Janiak

Beilstein J. Nanotechnol. 2026, 17, 218–238, doi:10.3762/bjnano.17.15

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  • , scanning electron microscopy (SEM) and nitrogen gas sorption surface area analysis using the Brunauer–Emmett–Teller (BET) theory were employed to evaluate the surface structure, porosity, and overall texture of the materials. The SEM image in Figure 2a reveals the typical structure of AC, characterized by
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Published 30 Jan 2026

Time of flight secondary ion mass spectrometry imaging of contaminant species in chemical vapour deposited graphene on copper

  • Barry Brennan,
  • Vlad-Petru Veigang-Radulescu,
  • Philipp Braeuninger-Weimer,
  • Stephan Hofmann and
  • Andrew J. Pollard

Beilstein J. Nanotechnol. 2026, 17, 200–213, doi:10.3762/bjnano.17.13

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  • a Wyko NT1100 White Light Optical Profiling System using a 20× magnification in vertical scanning interferometry (VSI) mode. Scanning electron microscopy (SEM) was carried out with a Carl Zeiss SIGMA VP at an acceleration voltage of 2 kV to ensure sample consistency. Four separate Cu foil samples
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Published 21 Jan 2026

Functional surface engineering for cultural heritage protection: the role of superhydrophobic and superoleophobic coatings – a comprehensive review

  • Giuseppe Cesare Lama,
  • Marino Lavorgna,
  • Letizia Verdolotti,
  • Federica Recupido,
  • Giovanna Giuliana Buonocore and
  • Bharat Bhushan

Beilstein J. Nanotechnol. 2026, 17, 63–96, doi:10.3762/bjnano.17.6

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Published 07 Jan 2026

Subdigital integumentary microstructure in Cyrtodactylus (Squamata: Gekkota): do those lineages with incipiently expressed toepads exclusively exhibit adhesive setae?

  • Philipp Ginal,
  • Yannick Ecker,
  • Timothy Higham,
  • L. Lee Grismer,
  • Benjamin Wipfler,
  • Dennis Rödder,
  • Anthony Russell and
  • Jendrian Riedel

Beilstein J. Nanotechnol. 2026, 17, 38–56, doi:10.3762/bjnano.17.4

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  • variation of digital form within this genus, from species with ancestrally small, round subdigital scales to macroscopically defined incipient toepads (broadened lamella-like subdigital scales). We employed scanning electron microscopy (SEM) and phylogenetic comparative methods to (a) explore the
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Published 06 Jan 2026

Reduced graphene oxide paper electrode for lithium-ion cells – towards optimized thermal reduction

  • Agata Pawłowska,
  • Magdalena Baran,
  • Stefan Marynowicz,
  • Aleksandra Izabela Banasiak,
  • Adrian Racki,
  • Adrian Chlanda,
  • Tymoteusz Ciuk,
  • Marta Wolczko and
  • Andrzej Budziak

Beilstein J. Nanotechnol. 2026, 17, 24–37, doi:10.3762/bjnano.17.3

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  • and thickness were determined with scanning electron microscopy imaging. This paper also reveals electrical and electrochemical properties of the material. The conductivity of the material obtained at 800 °C reached ≈70 S/cm, and the discharge capacity reached ≈160 mAh/g at 100 mA/g current density
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Published 05 Jan 2026

Visualizing nanostructures in supramolecular hydrogels: a correlative study using confocal and cryogenic scanning electron microscopy

  • Shaun M. Smith,
  • Ferdinando Malagreca,
  • Jacqueline Hicks,
  • Giuseppe Mantovani,
  • David B. Amabilino,
  • Christopher Parmenter and
  • Lluïsa Pérez-García

Beilstein J. Nanotechnol. 2025, 16, 2274–2284, doi:10.3762/bjnano.16.156

Graphical Abstract
  • ) fluorophores were imaged using confocal laser scanning microscopy (CLSM) of fully solvated gels and cryogenic scanning electron microscopy (cryo-SEM) was used to observe the corresponding xerogels. The DPP@Gel systems exhibit strong fluorescence and are effectively imaged using CLSM, with fibre morphologies
  • [11]. Cryogenic scanning electron microscopy (cryo-SEM) bypasses many of these resolution limits by preserving the hydrogel through rapid freezing and subsequent fracture, thereby maintaining native-like morphology in the microscope in the form of a xerogel (no solvent) nature [12][13][14]. High
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Published 12 Dec 2025

Chiral plasmonic nanostructures fabricated with circularly polarized light

  • Tian Qiao and
  • Ming Lee Tang

Beilstein J. Nanotechnol. 2025, 16, 2245–2264, doi:10.3762/bjnano.16.154

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Published 08 Dec 2025

Ultrathin water layers on mannosylated gold nanoparticles

  • Maiara A. Iriarte Alonso,
  • Jorge H. Melillo,
  • Silvina Cerveny,
  • Yujin Tong and
  • Alexander M. Bittner

Beilstein J. Nanotechnol. 2025, 16, 2183–2198, doi:10.3762/bjnano.16.151

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  • short oligo(ethylene glycol) chains. The particles were first characterized by dynamic light scattering (DLS) and zeta potential (ZP) measurements in solution, and by scanning electron microscopy (SEM) and scanning transmission electron microscopy (STEM) in vacuum. Samples were adsorbed on flat
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Published 04 Dec 2025

Microplastic pollution in Himalayan lakes: assessment, risks, and sustainable remediation strategies

  • Sameeksha Rawat,
  • S. M. Tauseef and
  • Madhuben Sharma

Beilstein J. Nanotechnol. 2025, 16, 2144–2167, doi:10.3762/bjnano.16.148

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  • polymers that result from local tourist waste and those transported by atmospheric deposition in Himalayan lakes of high elevation [37]. 4.2.2 Microscopy. Microscopic techniques remain crucial for the initial description of MPs, particularly when assessing their physical properties. Scanning electron
  • microscopy (SEM) produces high-resolution images of particle shapes. It also indicates surface wear and tear patterns that reflect how old the MP is and how long it has been in the environment [38]. Ease of operation and minimal cost of optical microscopy make it widely used, despite being less sophisticated
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Published 25 Nov 2025

Molecular and mechanical insights into gecko seta adhesion: multiscale simulations combining molecular dynamics and the finite element method

  • Yash Jain,
  • Saeed Norouzi,
  • Tobias Materzok,
  • Stanislav N. Gorb and
  • Florian Müller-Plathe

Beilstein J. Nanotechnol. 2025, 16, 2055–2076, doi:10.3762/bjnano.16.141

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  • to more spatula–substrate sites is straightforward but would increase runtime. Models Multiscale seta–spatula model A seta branches into spatulae as seen in scanning electron microscopy (SEM) images of gecko setae (Figure 1). A single seta on a gecko’s foot can have dozens of sub-branches, which
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Published 14 Nov 2025

Stereodiscrimination of guests in chiral organosilica aerogels studied by ESR spectroscopy

  • Sebastian Polarz,
  • Yasar Krysiak,
  • Martin Wessig and
  • Florian Kuhlmann

Beilstein J. Nanotechnol. 2025, 16, 2034–2054, doi:10.3762/bjnano.16.140

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  • prepare chiral oSILs by co-condensation of Si(OiPr)4 with a sol–gel precursor that already contains the amino acid. An example is an Ala-modified 1,3-bis(triisopropoxysilyl)aniline [45][49] as shown in Scheme 1. The resulting material was characterized by scanning electron microscopy (SEM; Figure 2a); it
  • using a Bruker AVANCE III spectrometer operating at 400 MHz equipped with a 4 mm PH MAS DVT 400W1 BL4 N-P/H CGR probe head with magic angle gradient. 1H NMR measurements were performed on a Bruker Ascend 400 MHz spectrometer. Scanning electron microscopy and energy-dispersive X-ray spectroscopy were
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Published 13 Nov 2025

Beyond the shell: exploring polymer–lipid interfaces in core–shell nanofibers to carry hyaluronic acid and β-caryophyllene

  • Aline Tavares da Silva Barreto,
  • Francisco Alexandrino-Júnior,
  • Bráulio Soares Arcanjo,
  • Paulo Henrique de Souza Picciani and
  • Kattya Gyselle de Holanda e Silva

Beilstein J. Nanotechnol. 2025, 16, 2015–2033, doi:10.3762/bjnano.16.139

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  • fibers without the lipid core. Furthermore, maintaining ambient relative humidity below 45% proved essential for processing stability. Comprehensive morphological characterization via scanning electron microscopy confirmed the uniformity of the fibers. At the same time, confocal microscopy, cross
  • core–shell structure indicates the absence of core material at the surface, and that the shell structure does not possess pores that would allow permeation or direct contact of water molecules with the core, as evidenced by scanning electron microscopy (SEM) images. Electrospun nanofibers organize into
  • average of readings performed in triplicate for each sample analyzed using the ZetaSizer software 7.11. Scanning electron microscopy The morphology of the obtained nanofibers (porosity, average diameter, uniformity, and roughness) was evaluated using a scanning electron microscope under different
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Published 12 Nov 2025

The cement of the tube-dwelling polychaete Sabellaria alveolata: a complex composite adhesive material

  • Emilie Duthoo,
  • Aurélie Lambert,
  • Pierre Becker,
  • Carla Pugliese,
  • Jean-Marc Baele,
  • Arnaud Delfairière,
  • Matthew J. Harrington and
  • Patrick Flammang

Beilstein J. Nanotechnol. 2025, 16, 1998–2014, doi:10.3762/bjnano.16.138

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  • % paraformaldehyde in phosphate-buffered saline, rinsed, and air-dried. Worms were left in the remaining proximal part of the tube and were provided with glass beads (425–600 µm in diameter; Sigma) to reconstruct the missing part [25]. Scanning electron microscopy and elemental composition analyses For secondary
  • composition of cement cell granules, we used energy-dispersive X-ray spectroscopy (EDS) coupled with scanning electron microscopy (SEM). Elemental composition was measured on four secretory granules of both types of cement cells in the parathoracic part of worms embedded in Spurr resin (TEM blocks). Using the
  • the inclusions of the heterogeneous granules occurring through a still unknown process. This swelling was also suggested in P. californica based on the similar bright appearance of heterogeneous granule inclusions and spheroid cortex under scanning electron microscopy using backscattered electrons, as
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Published 11 Nov 2025

Laser ablation in liquids for shape-tailored synthesis of nanomaterials: status and challenges

  • Natalie Tarasenka

Beilstein J. Nanotechnol. 2025, 16, 1963–1997, doi:10.3762/bjnano.16.137

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  • observed the formation of a mixture of nanosheets and spherical NPs for the ablation using the 1064 nm laser wavelength, while at 532 nm only spherical NPs were observed. The authors observed nanosheets only in scanning electron microscopy, while transmission electron microscopy showed only spherical
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Published 10 Nov 2025

Mechanical property measurements enabled by short-term Fourier-transform of atomic force microscopy thermal deflection analysis

  • Thomas Mathias,
  • Roland Bennewitz and
  • Philip Egberts

Beilstein J. Nanotechnol. 2025, 16, 1952–1962, doi:10.3762/bjnano.16.136

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  • glass colloid probe on a HOPG sample (red circles), and (d) a diamond-coated silicon on silicon sample (blue circles). A red dashed line in each figure shows a fit to the experimental data using Equation 7. (a, b) Scanning electron microscopy images of the borosilicate glass colloid glued onto the
  • tipless silicon cantilever. (c, d) Scanning electron microscopy images of the PtSi-coated AFM cantilever with integrated tip. Mechanical properties of the examined samples. Values for silicon, HOPG, and platinum are from [17], [18], and [19], respectively. The values for PEO and PDMS were measured using a
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Published 06 Nov 2025

Evaluating metal-organic precursors for focused ion beam-induced deposition through solid-layer decomposition analysis

  • Benedykt R. Jany,
  • Katarzyna Madajska,
  • Aleksandra Butrymowicz-Kubiak,
  • Franciszek Krok and
  • Iwona B. Szymańska

Beilstein J. Nanotechnol. 2025, 16, 1942–1951, doi:10.3762/bjnano.16.135

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  • create a new precursor, extensive testing using specialized gas injection systems is required along with time-consuming and costly chemical analysis typically conducted using scanning electron microscopy (SEM). This process can be quite challenging due to its complexity and expense. Here, the response of
  • -dispersive X-ray spectroscopy (EDX); focused ion beam (FIB); focused ion beam-induced deposition (FIBID); machine learning; scanning electron microscopy (SEM); Introduction A variety of nanomanufacturing techniques, such as optical and electron-beam lithography, nanoimprint lithography, atomic layer
  • studies. Here, we present a pathway for unraveling how the chemical composition of metal-organic precursors affects their decomposition when irradiated with FIB in the form of supported layers. A decomposition process of the studied layer was quantitatively monitored by scanning electron microscopy
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Published 04 Nov 2025

Beyond the bilayer: multilayered hygroscopic actuation in pine cone scales

  • Kim Ulrich,
  • Max David Mylo,
  • Tom Masselter,
  • Fabian Scheckenbach,
  • Sophia Fischerbauer,
  • Martin Nopens,
  • Silja Flenner,
  • Imke Greving,
  • Linnea Hesse and
  • Thomas Speck

Beilstein J. Nanotechnol. 2025, 16, 1695–1710, doi:10.3762/bjnano.16.119

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  • electron microscopy (abaxial: 9%, adaxial: 1%, [18]). Although their exact values of measured longitudinal expansion may differ from ours due to differences in methodology and pine species studied, our results do support the ability of individual fibers to bend independently in response to moisture changes
  • abaxial side exhibiting about 70% greater median shrinkage (Table 1). This gradient is consistent with spiral secondary cell wall thickenings only being observed on the abaxial side, leading to a differential longitudinal extension rate within the sclerenchyma fibers measured using environmental scanning
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Published 29 Sep 2025

Prospects of nanotechnology and natural products for cancer and immunotherapy

  • Jan Filipe Andrade Santos,
  • Marcela Bernardes Brasileiro,
  • Pamela Danielle Cavalcante Barreto,
  • Ligiane Aranha Rocha and
  • José Adão Carvalho Nascimento Júnior

Beilstein J. Nanotechnol. 2025, 16, 1644–1667, doi:10.3762/bjnano.16.116

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  • CXCL9/10 expression in Schwann cells [114]. Particle size and stability of the formulation in the patent were characterized using scanning electron microscopy (SEM). The nanoparticles demonstrated enhanced uptake in HepG2 cells, as confirmed by flow cytometry and confocal microscopy, and achieved a
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Published 22 Sep 2025

Venom-loaded cationic-functionalized poly(lactic acid) nanoparticles for serum production against Tityus serrulatus scorpion

  • Philippe de Castro Mesquita,
  • Karla Samara Rocha Soares,
  • Manoela Torres-Rêgo,
  • Emanuell dos Santos-Silva,
  • Mariana Farias Alves-Silva,
  • Alianda Maira Cornélio,
  • Matheus de Freitas Fernandes-Pedrosa and
  • Arnóbio Antônio da Silva-Júnior

Beilstein J. Nanotechnol. 2025, 16, 1633–1643, doi:10.3762/bjnano.16.115

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  • analysis supported small and narrow-sized cationic functionalized nanoparticles. Atomic force microscopy and scanning electron microscopy images showed nanoparticles with a spherical and smooth shape. The stability of tested formulations was accessed for six weeks, and the sustained release of proteins
  • corroborates the high encapsulation efficiency obtained by the BCA assay. Field emission gun scanning electron microscopy and atomic force microscopy analyses Field emission gun scanning electron microscopy (FEGSEM) and atomic force microscopy (AFM) analyses were realized to access shape and surface features
  • . serrulatus venom protein-loaded PLA nanoparticles at 1.0% (NPs + Tsv 1.0%). MM: molecular mass marker. Gel stained with Coomassie brilliant blue R-250. 2D and 3D atomic force microscopy and field emission gun scanning electron microscopy images, respectively, of formulations of Tityus serrulatus venom-loaded
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Published 17 Sep 2025
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