Beilstein J. Nanotechnol.2025,16, 700–710, doi:10.3762/bjnano.16.54
, environmental reliability, and operando capabilities. Scanningphotoelectronspectromicroscopy (SPEM) is one of the characterization tools that combine high spectral resolution X-ray photoelectron spectroscopy with submicron spatial resolution. In particular, the SPEM equipment hosted at the ESCA microscopy
; operando; oxides; scanningphotoelectronspectromicroscopy; semiconductor nanowires; transition metal dichalcogenides; XPS; Introduction
Nanometer or micrometer-sized materials play a key role in modern technologies in the search of new routes for unforeseen performances generating breakthroughs in
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Figure 1:
a) SPEM image of the Cr0.78Ti0.36Se2 single crystal obtained at the area corresponding to the Se 3d...