Supporting Information
The crystallographic data of the structure are deposited in the Cambridge Crystal Structure Data Bank (CCDC 2: 2237758; CCDC 3: 2481941; CCDC 9a: 2450586; CCDC 9b: 2450587). Statistics on the collection of X-ray diffraction data and refinement of the structure are shown in Table S1 in Supporting Information File 1.
| Supporting Information File 1: General synthetic procedures, characterization data and copies of IR spectra, 1H-13C{1H}, 1H-1H dqfCOSY, 1H-1H NOESY, 1H-13C HMQC, 1H-13C HMBC NMR spectra of all synthesized compounds, and crystallographic data for compounds 2, 3, 9a, and 9b. | ||
| Format: PDF | Size: 4.9 MB | Download |
Cite the Following Article
Highly electrophilic, gem- and spiro-activated trichloromethylnitrocyclopropanes: synthesis and structure
Ilia A. Pilipenko, Mikhail V. Grigoriev, Olga Yu. Ozerova, Igor A. Litvinov, Darya V. Spiridonova, Aleksander V. Vasilyev and Sergey V. Makarenko
Beilstein J. Org. Chem. 2026, 22, 123–130.
https://doi.org/10.3762/bjoc.22.5
How to Cite
Pilipenko, I. A.; Grigoriev, M. V.; Ozerova, O. Y.; Litvinov, I. A.; Spiridonova, D. V.; Vasilyev, A. V.; Makarenko, S. V. Beilstein J. Org. Chem. 2026, 22, 123–130. doi:10.3762/bjoc.22.5
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