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1 article(s) from Akakpo, Christian

Acyclic cucurbit[n]uril bearing alkyl sulfate ionic groups

Christian Akakpo,
Peter Y. Zavalij and
Lyle Isaacs

Beilstein J. Org. Chem. 2025, 21, 717–726, doi:10.3762/bjoc.21.55

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Figure 1: Chemical structures of CB[n] and selected acyclic CB[n]-type molecular containers M1 and M0.

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Scheme 1: Synthesis of C1. Conditions: a) TFA/Ac₂O, 70 °C, 3.5 h, 71%; b) LiOH, 50 °C, 69%; c) dry pyridine, ...

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Figure 2: a) ¹H NMR spectrum (600, D₂O, rt) and b) ¹³C NMR spectrum recorded (150 MHz, D₂O, rt) for C1.

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Figure 3: Chemical structures of guests used in this study along with the complexation induced changes in che...

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Figure 4: ¹H NMR spectra recorded (400 MHz, D₂O, rt) for: a) Me₆PXDA (0.5 mM), b) a mixture of C1 (0.5 mM) an...

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Figure 5: Cross-eyed stereoview of the C1·Me₆CHDA complex in the crystal. Color code: C, gray; H, white; N, b...

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Figure 6: Cross-eyed stereoview of the crystal packing observed in the molecular cell of C1·Me₆CHDA. H-atoms ...

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Figure 7: a) Representative plot of DP (μcal s⁻¹) versus time from the titration of C1 (0.1 mM) in the ITC ce...

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Published 03 Apr 2025

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