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1 article(s) from Burmistrova, Daria A

Synthesis, electrochemical properties, and antioxidant activity of sterically hindered catechols with 1,3,4-oxadiazole, 1,2,4-triazole, thiazole or pyridine fragments

Daria A. Burmistrova,
Andrey Galustyan,
Nadezhda P. Pomortseva,
Kristina D. Pashaeva,
Maxim V. Arsenyev,
Oleg P. Demidov,
Mikhail A. Kiskin,
Andrey I. Poddel’sky,
Nadezhda T. Berberova and
Ivan V. Smolyaninov

Beilstein J. Org. Chem. 2024, 20, 2378–2391, doi:10.3762/bjoc.20.202

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Scheme 1: Synthesis of catechol-containing compounds 1–9.

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Figure 1: The X-ray structure of catechol 5 (the thermal ellipsoids of 50% probability). The hydrogen atoms e...

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Figure 2: The X-ray structures of catechols 6 (a) and 8 (b) (the thermal ellipsoids of 50% probability). The ...

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Figure 3: Fragment of the pack of catechol 5 in crystal (the H-bonds and π–π interactions are shown as dotted...

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Figure 4: The interactions in pair of independent molecules A and B of 6 in crystal 6·0.5CH₃CN (the H-bonds a...

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Figure 5: Fragment of the pack of catechol 8 in crystal (the H-bonds and π–π interactions are shown as dotted...

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Scheme 2: Electrochemical transformations of compounds 1–3.

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Figure 6: The CV curve of 2 at the potential range from −0.50 to 1.60 V (CH₃CN, GC electrode, Ag/AgCl/KCl(sat...

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Figure 7: The CV curves of 3 at the potential ranges from –0.5 to 1.2 V (curve 1); from –0.5 to 2.0 V (curve ...

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Figure 8: The CV curves of 7 at the potential ranges from –0.5 to 1.3 V (curve 1); from –0.5 to 1.8 V (curve ...

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Scheme 3: Proposed mechanism of an electrooxidation of compounds 6–8.

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Figure 9: The level of TBARS in rat liver homogenates in vitro, in the presence of compounds 1–9, Trolox, and...

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Published 19 Sep 2024

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