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1 article(s) from Navarro-Santos, Pedro

Divergent role of PIDA and PIFA in the AlX₃ (X = Cl, Br) halogenation of 2-naphthol: a mechanistic study

Kevin A. Juárez-Ornelas,
Manuel Solís-Hernández,
Pedro Navarro-Santos,
J. Oscar C. Jiménez-Halla and
César R. Solorio-Alvarado

Beilstein J. Org. Chem. 2024, 20, 1580–1589, doi:10.3762/bjoc.20.141

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Scheme 1: Representative protocols for the oxidative aromatic chlorination and bromination with iodine(III) r...

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Scheme 2: Chlorination of 2-naphthol using the PIFA/AlCl₃, 1:2 system.

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Scheme 3: Bromination of 2-naphthol using the PIDA/AlBr₃, 1:2 system.

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Scheme 4: Reaction mechanism for the chlorination of 2-naphthol using the PIFA/AlCl₃, 1:2 system.

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Figure 1: Energy profile for the chlorination of 2-naphthol in the presence of PIFA and AlCl₃.

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Scheme 5: Calculated reaction mechanism for the bromination of 2-naphthol using the PIDA/AlBr₃, 1:2 system.

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Figure 2: Calculated mechanism for the bromination of 2-naphthol in the presence of PIDA and AlBr₃.

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Published 15 Jul 2024

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Divergent role of PIDA and PIFA in the AlX3 (X = Cl, Br) halogenation of 2-naphthol: a mechanistic study

Divergent role of PIDA and PIFA in the AlX₃ (X = Cl, Br) halogenation of 2-naphthol: a mechanistic study