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Beilstein J. Org. Chem. 2024, 20, 1677–1683, doi:10.3762/bjoc.20.149
Graphical Abstract
Figure 1: Overview of common non-iodine-based (left) and iodine-based (right) oxidizing reagents for the gene...
Figure 2: NHIs investigated for the oxidation of benzylic alcohols and the crystal structure (ORTEP drawing) ...
Figure 3: 1H NMR spectra of the time-dependent formation of a) an alkoxy-NHI which is causing a significant d...
Figure 4: Oxidation of 3a to 4a using different iodine(III) reagents with AlCl3 as an additive. Conditions: T...
Figure 5: Substrate scope of aldehydes and ketones synthesized from the corresponding alcohols. Isolated yiel...
Scheme 1: Possible reaction mechanisms via the formation of a) a Cl(I) species and b) the formation of an alk...