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2 article(s) from Sato, Eisuke

Electrocatalytic hydrogenation of cyanoarenes, nitroarenes, quinolines, and pyridines under mild conditions with a proton-exchange membrane reactor

Koichi Mitsudo,
Atsushi Osaki,
Haruka Inoue,
Eisuke Sato,
Naoki Shida,
Mahito Atobe and
Seiji Suga

Beilstein J. Org. Chem. 2024, 20, 1560–1571, doi:10.3762/bjoc.20.139

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Figure 1: Schematic of (a) a PEM reactor and (b) MEA.

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Scheme 1: Plausible mechanism for the reduction of 1a leading to benzylamine 2a and dibenzylamine 3a.

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Scheme 2: Electrochemical reduction of cyanoarenes under optimal conditions. Reaction conditions: anode catal...

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Scheme 3: Scope of the electrochemical reduction of nitroarenes. Reaction conditions: anode catalyst, Pt/C; c...

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Figure 2: Hypothesis of the trap of quinoline on membrane and tetrahydroquinoline and the effect of adding an...

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Figure 3: Recycled use of MEA for the electroreduction of 6a in the presence of PTSA (0.10 equiv). Reaction c...

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Figure 4: Recycled use of MEA for the electroreduction of 6a in the presence of PPTS (0.10 equiv). Reaction c...

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Scheme 4: Scope of the electroreduction of 6 in the presence of PTSA (0.10 equiv). Reaction conditions: anode...

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Scheme 5: a) Large scale synthesis of 7a and b) electoreduction of 6a using H₂SO₄ as a proton source.

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Scheme 6: Scope of the electroreduction of 6 in the presence of PTSA (1 equiv). Reaction conditions: anode ca...

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Published 11 Jul 2024

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Electrochemical hydrogenation of enones using a proton-exchange membrane reactor: selectivity and utility

Koichi Mitsudo,
Haruka Inoue,
Yuta Niki,
Eisuke Sato and
Seiji Suga

Beilstein J. Org. Chem. 2022, 18, 1055–1061, doi:10.3762/bjoc.18.107

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Scheme 1: Designed electrochemical hydrogenation of enones 1 with a PEM reactor.

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Figure 1: Electrochemical setup of the PEM reactor: a) Electrochemical reduction system with the PEM reactor....

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Figure 2: Reaction profile of the electrochemical hydrogenation of 1a with a PEM reactor using a) Pd/C and b)...

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Scheme 2: Electrochemical hydrogenation of several enones 1 with a circulating PEM reactor using a Pd/C catho...

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Scheme 3: Electrochemical hydrogenation of several enones 1 with a circulating PEM reactor using an Ir/C cath...

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Scheme 4: Mechanistic studies.

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Scheme 5: Electroreduction of 1a with the circulating PEM reactor using H₂O as a proton source.

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Published 19 Aug 2022

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