Beilstein J. Org. Chem.2025,21, 10–38, doi:10.3762/bjoc.21.3
laboratory (ASL) was designed and built by Eli Lilly [33]. This state-of-the-art facility allowed for heating, cryogenic conditions, microwaving, high-pressurereactions, evaporation, and workup, empowering researchers to conduct an extensive array of chemical reactions. The ASL comprises of three bench
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Graphical Abstract
Figure 1:
A high-level representation of the workflow and framework used for the optimization of organic reac...
Beilstein J. Org. Chem.2015,11, 576–582, doi:10.3762/bjoc.11.63
sulfones.
Keywords: dimethyl acetylenedicarboxylate (DMAD); hetero-Diels–Alder reactions; highpressurereactions; methyl propiolate; thioketones; thiopyrans; Introduction
A series of recent publications evidence that, in contrast to earlier opinions, thioketones are useful building blocks for the
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Graphical Abstract
Scheme 1:
Hetero-Diels–Alder reaction of thiobenzophenone (1a) with dimethyl acetylenedicarboxylate (2a) [10].