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Search for "diffuse reflectance" in Full Text gives 82 result(s) in Beilstein Journal of Nanotechnology.

Ar+ implantation-induced tailoring of RF-sputtered ZnO films: structural, morphological, and optical properties

  • Manu Bura,
  • Divya Gupta,
  • Arun Kumar and
  • Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 872–886, doi:10.3762/bjnano.16.66

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  • in grazing incidence angle X-ray diffraction patterns. Atomic force microscopy images show grain size reduction and a fall in the surface roughness value of films after implantation. The implantation-induced structural modifications are further correlated with the variation in diffuse reflectance
  • , Urbach energy, and optical bandgap. The low reflectance values of implanted films assure their suitability as transparent windows and anti-reflective coating in various optoelectronic devices. Keywords: AFM; diffuse reflectance; GXRD; polycrystalline; ZnO films; Introduction Zinc oxide has emerged as a
  • were implanted with 30 keV Ar+ at fluences varying from 1 × 1015 to 2 × 1016 ions·cm−2. Surface variables (roughness and particle size), structural variables (crystallite size and dislocation density), and optical properties (diffuse reflectance, Urbach energy, and optical bandgap) were studied in
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Published 11 Jun 2025

Clays enhanced with niobium: potential in wastewater treatment and reuse as pigment with antibacterial activity

  • Silvia Jaerger,
  • Patricia Appelt,
  • Mario Antônio Alves da Cunha,
  • Fabián Ccahuana Ayma,
  • Ricardo Schneider,
  • Carla Bittencourt and
  • Fauze Jacó Anaissi

Beilstein J. Nanotechnol. 2025, 16, 141–154, doi:10.3762/bjnano.16.13

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  • SHIMADZU) with a 1 cm path length glass cuvette at λmax (maximum absorbance) in nanometers. Samples collected after the adsorption process had the electronic spectra analyzed using an Ocean Optics USB-2000 instrument for solid samples with a tungsten lamp in the range of 200–800 nm in diffuse reflectance
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Published 10 Feb 2025

TiO2 immobilized on 2D mordenite: effect of hydrolysis conditions on structural, textural, and optical characteristics of the nanocomposites

  • Marina G. Shelyapina,
  • Rosario Isidro Yocupicio-Gaxiola,
  • Gleb A. Valkovsky and
  • Vitalii Petranovskii

Beilstein J. Nanotechnol. 2025, 16, 128–140, doi:10.3762/bjnano.16.12

Graphical Abstract
  • diffuse reflectance spectra. In this method, it is assumed that the energy-dependent absorption coefficient α can be written as where h is the Planck constant, hν is the photon energy, and B is a constant. The factor n depends on the nature of the electron transition, that is, n = 1/2 for direct and n = 2
  • (R∞) ∼ α, by combing Equation 4 and Equation 5, one obtains Figure 7a shows the diffuse reflectance spectra of the prepared TiO2/2D mordenite nanocomposite. All samples exhibit absorption edges near 400 nm due to the anatase TiO2 bandgap absorption. Figure 7b shows the reflectance spectra of the
  • determined by diffuse reflectance spectroscopy using a Lambda 1050 spectrophotometer (Perkin Elmer) equipped with an integrating sphere in the spectral range of 200–700 nm. Barium sulfate (BaSO4) was used as a reference. (a) Small-angle powder patterns for the parent compound MOR-L and the samples after TEOT
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Published 10 Feb 2025

Mn-doped ZnO nanopowders prepared by sol–gel and microwave-assisted sol–gel methods and their photocatalytic properties

  • Cristina Maria Vlăduț,
  • Crina Anastasescu,
  • Silviu Preda,
  • Oana Catalina Mocioiu,
  • Simona Petrescu,
  • Jeanina Pandele-Cusu,
  • Dana Culita,
  • Veronica Bratan,
  • Ioan Balint and
  • Maria Zaharescu

Beilstein J. Nanotechnol. 2024, 15, 1283–1296, doi:10.3762/bjnano.15.104

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  • –Halenda) model. Diffuse reflectance UV–vis spectra were recorded with a Perkin Elmer Lambda 35 spectrophotometer equipped with an integrating sphere. The analysis range was 200–1000 nm. Based on the Kubelka–Munk function, the collected reflectance data were transformed into absorption spectra. Eg was
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Published 28 Oct 2024

Photocatalytic methane oxidation over a TiO2/SiNWs p–n junction catalyst at room temperature

  • Qui Thanh Hoai Ta,
  • Luan Minh Nguyen,
  • Ngoc Hoi Nguyen,
  • Phan Khanh Thinh Nguyen and
  • Dai Hai Nguyen

Beilstein J. Nanotechnol. 2024, 15, 1132–1141, doi:10.3762/bjnano.15.92

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  • properties of as-synthesized samples were analyzed using an X-ray diffraction system (XRD, Rigaku, SmartLab) with a 2θ range of 20–80° and a field-emission scanning electron microscope (FE-SEM, Hitachi, S-4700). The absorption properties of the thin films were analyzed using a diffuse reflectance UV–vis
  • images of the TiO2/SiNWs device with a higher-magnification view of the red rectangles on the right-hand side. A thin layer of TiO2 (estimated at 25 nm) was deposited on the SiNWs by using ALD with 500 deposition cycles. The UV–visible diffuse reflectance spectra (a) and I–V curve under light/dark
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Published 02 Sep 2024

A review on the structural characterization of nanomaterials for nano-QSAR models

  • Salvador Moncho,
  • Eva Serrano-Candelas,
  • Jesús Vicente de Julián-Ortiz and
  • Rafael Gozalbes

Beilstein J. Nanotechnol. 2024, 15, 854–866, doi:10.3762/bjnano.15.71

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  • toxicity of metal oxides using two parameters, namely, the experimentally measured concentration of the metal (expressed as a percentage) and the conduction band energy, which was calculated from different physicochemical constants and also from experimental measurements of zeta potential and diffuse
  • reflectance UV–vis spectra). Alternative formulations for valence and conduction band energies, based only on pre-known physicochemical constants and values from reference handbooks, have been reported as well [79][80]. Furthermore, the electric characteristics of the nanoparticle surface can be reported by
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Published 11 Jul 2024

Photocatalytic degradation of methylene blue under visible light by cobalt ferrite nanoparticles/graphene quantum dots

  • Vo Chau Ngoc Anh,
  • Le Thi Thanh Nhi,
  • Le Thi Kim Dung,
  • Dang Thi Ngoc Hoa,
  • Nguyen Truong Son,
  • Nguyen Thi Thao Uyen,
  • Nguyen Ngoc Uyen Thu,
  • Le Van Thanh Son,
  • Le Trung Hieu,
  • Tran Ngoc Tuyen and
  • Dinh Quang Khieu

Beilstein J. Nanotechnol. 2024, 15, 475–489, doi:10.3762/bjnano.15.43

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  • electron microscopy, transmission electron microscopy, ultraviolet–visible diffuse reflectance spectroscopy, Fourier-transform infrared spectroscopy, photoluminescence spectroscopy, vibrating-sample magnetometry, and nitrogen adsorption/desorption isotherms. Cobalt ferrite crystals of around 8–10 nm and
  • ) iron mapping, and (f) cobalt mapping. (a) PL spectra, (b) UV–vis diffuse reflectance spectra with Tauc’s plots in the inset, (c) magnetization curves, and (d) nitrogen adsorption/desorption isotherms of CF/GQDs prepared at different temperatures. (a) MB decolourisation over different catalysts (V = 100
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Published 29 Apr 2024

Titania nanoparticles for photocatalytic degradation of ethanol under simulated solar light

  • Evghenii Goncearenco,
  • Iuliana P. Morjan,
  • Claudiu Teodor Fleaca,
  • Florian Dumitrache,
  • Elena Dutu,
  • Monica Scarisoreanu,
  • Valentin Serban Teodorescu,
  • Alexandra Sandulescu,
  • Crina Anastasescu and
  • Ioan Balint

Beilstein J. Nanotechnol. 2023, 14, 616–630, doi:10.3762/bjnano.14.51

Graphical Abstract
  • lamp at λexc = 260 nm. All samples have been irradiated at room temperature and under the same conditions. Diffuse reflectance UV–vis measurements were performed by using a spectrophotometer Perkin Elmer Lambda 35 with an integrating sphere in the 200–1100 nm range. The measured reflectance data were
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Published 22 May 2023

Conjugated photothermal materials and structure design for solar steam generation

  • Chia-Yang Lin and
  • Tsuyoshi Michinobu

Beilstein J. Nanotechnol. 2023, 14, 454–466, doi:10.3762/bjnano.14.36

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  • formed by sequential polymerization on paper substrates, to enhance their light capturing capability (Figure 6a) [32]. Transmission and diffuse reflectance measurements of the PPy nanosheets confirmed that the multilayer PPy nanosheets on the paper substrate exhibited a distinct broadband absorption in
  • process of multilayer PPy nanosheets. (b)Transmittance and (c) diffuse reflectance spectra of the air-laid paper substrate coated with different layer numbers of PPy nanosheets. The inset figure in (b) is the enlarged view of the 500–1500 nm wavelength range. The solar spectral irradiance (AM1.5G) is
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Published 04 Apr 2023

Antimicrobial and mechanical properties of functionalized textile by nanoarchitectured photoinduced Ag@polymer coating

  • Jessica Plé,
  • Marine Dabert,
  • Helene Lecoq,
  • Sophie Hellé,
  • Lydie Ploux and
  • Lavinia Balan

Beilstein J. Nanotechnol. 2023, 14, 95–109, doi:10.3762/bjnano.14.11

Graphical Abstract
  • total reflectance increased significantly between 400 and 580 nm, while dropping slightly (10%) in the 580–1000 nm range. The diffuse reflectance effectively decreased from 52 to 20% at 700 nm. Indeed, friction causes a localized rise in temperature between particles, which promotes a reduction in
  • the surface of an Ag@PEG600DA coating (a) and on the total and diffuse reflectance (b). Associated SEM surface images (c). Influence of 500 and 1000 abrasion cycles on the surface of an Ag@PEG600DA/PETIA coating (1:1) (a) and on the total and diffuse reflectance (b). Associated SEM surface images (c
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Published 12 Jan 2023

Photoelectrochemical water oxidation over TiO2 nanotubes modified with MoS2 and g-C3N4

  • Phuong Hoang Nguyen,
  • Thi Minh Cao,
  • Tho Truong Nguyen,
  • Hien Duy Tong and
  • Viet Van Pham

Beilstein J. Nanotechnol. 2022, 13, 1541–1550, doi:10.3762/bjnano.13.127

Graphical Abstract
  • of materials The morphology, the phase, and the vibrational characteristics of the surface functional groups of the materials were observed by field-emission scanning electron microscopy (FESEM), X-ray diffraction (XRD), and Fourier-transform infrared spectroscopy (FTIR). Diffuse reflectance
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Published 16 Dec 2022

A TiO2@MWCNTs nanocomposite photoanode for solar-driven water splitting

  • Anh Quynh Huu Le,
  • Ngoc Nhu Thi Nguyen,
  • Hai Duy Tran,
  • Van-Huy Nguyen and
  • Le-Hai Tran

Beilstein J. Nanotechnol. 2022, 13, 1520–1530, doi:10.3762/bjnano.13.125

Graphical Abstract
  • diffraction (XRD, D2 PHASER). The chemical structure of the samples is characterized using Fourier-transform infrared spectroscopy (FTIR, Brucker 27). The electrochemical measurements are carried out on a MPG2 Biologic system with a three-electrode cell controlled by ECLab® software. Diffuse reflectance
  • at 621 cm−1 is assigned to the Ti–O and Ti–O–Ti stretching of TiO2 [24]. In addition, the spectrum of TiO2@MWCNTs shows the characteristic peak at 972 cm−1 of the vibration of Ti–O–C groups, indicating the formation of a covalent bond between TiO2 and MWCNTs [24]. The UV–vis diffuse reflectance
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Published 14 Dec 2022

Spindle-like MIL101(Fe) decorated with Bi2O3 nanoparticles for enhanced degradation of chlortetracycline under visible-light irradiation

  • Chen-chen Hao,
  • Fang-yan Chen,
  • Kun Bian,
  • Yu-bin Tang and
  • Wei-long Shi

Beilstein J. Nanotechnol. 2022, 13, 1038–1050, doi:10.3762/bjnano.13.91

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  • -DLD, England). The Brunauer–Emmett–Teller (BET) surface area and pore size were determined using N2 adsorption–desorption isotherms (Microfor TriStar II Plus 2.02 system, USA). The UV–vis diffuse reflectance spectra (UV–vis DRS) were recorded by UV–vis spectrophotometry (FTS-165, PerkinElmer, USA
  • investigate the optical response and bandgap of the prepared samples, UV–vis diffuse reflectance (UV–vis DRS) spectra were recorded and given in Figure 5. As seen from Figure 5a, both Bi2O3 and MIL101(Fe) show strong visible-light response with absorption edge of 460 nm and 510 nm, respectively. Compared with
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Published 28 Sep 2022

Solar-light-driven LaFexNi1−xO3 perovskite oxides for photocatalytic Fenton-like reaction to degrade organic pollutants

  • Chao-Wei Huang,
  • Shu-Yu Hsu,
  • Jun-Han Lin,
  • Yun Jhou,
  • Wei-Yu Chen,
  • Kun-Yi Andrew Lin,
  • Yu-Tang Lin and
  • Van-Huy Nguyen

Beilstein J. Nanotechnol. 2022, 13, 882–895, doi:10.3762/bjnano.13.79

Graphical Abstract
  • . The UV–vis absorption capability with diffuse reflectance spectroscopy (DRS) and photographs of various LaFexNi1−xO3 perovskite oxides with different proportions were shown in Figure 5a and 5b. Except for LaFeO3, which was brown, the rest of the perovskite oxides doped with Ni became black. Since
  • microscopy (FESEM). The light absorption spectra of the perovskite oxides were inspected using V-670 (Jasco, Japan) to examine the UV–vis absorption capability with diffuse reflectance spectroscopy (DRS) from 200 to 800 nm. The nitrogen adsorption–desorption analyzer, ASAP 2020 PLUS (ASAP, USA), was applied
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Published 05 Sep 2022

Hierarchical Bi2WO6/TiO2-nanotube composites derived from natural cellulose for visible-light photocatalytic treatment of pollutants

  • Zehao Lin,
  • Zhan Yang and
  • Jianguo Huang

Beilstein J. Nanotechnol. 2022, 13, 745–762, doi:10.3762/bjnano.13.66

Graphical Abstract
  • determined according to the Brunauer−Emmett−Teller (BET) model and the Barrett−Joyner−Halenda (BJH) method. The UV–visible diffuse reflectance spectra (UV–vis DRS) were acquired on a Shimadzu UV-2450 spectrophotometer in the diffuse reflectance mode, equipped with an integrating sphere and using BaSO4 as the
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Published 04 Aug 2022

Sodium doping in brookite TiO2 enhances its photocatalytic activity

  • Boxiang Zhuang,
  • Honglong Shi,
  • Honglei Zhang and
  • Zeqian Zhang

Beilstein J. Nanotechnol. 2022, 13, 599–609, doi:10.3762/bjnano.13.52

Graphical Abstract
  • understand the photocatalytic behavior of a given material. The bandgap values were determined from the diffuse reflectance spectra using the Tauc plot method [26]: where A in Equation 1 is a proportional constant, α is the absorption coefficient, and n depends on the type of electron transition. The bandgap
  • Eg is the x-axis interception when linear fitting the absorption edge of the Tauc plot. As both the direct and the indirect electron transition in the brookite were reported, two transitions were considered in this work. Figure 2 shows the Tauc plot derived from the diffuse reflectance spectra of
  • of the MB (≈665 nm) acquired by a UV–vis spectrophotometer. The diffuse reflectance spectra were measured in the wavelength range of 300–800 nm using a UV–vis spectrophotometer. The bandgap was determined by linear fitting the absorption edge of the Tauc plot of the absorption spectra. Structure
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Published 05 Jul 2022

A photonic crystal material for the online detection of nonpolar hydrocarbon vapors

  • Evgenii S. Bolshakov,
  • Aleksander V. Ivanov,
  • Andrei A. Kozlov,
  • Anton S. Aksenov,
  • Elena V. Isanbaeva,
  • Sergei E. Kushnir,
  • Aleksei D. Yapryntsev,
  • Aleksander E. Baranchikov and
  • Yury A. Zolotov

Beilstein J. Nanotechnol. 2022, 13, 127–136, doi:10.3762/bjnano.13.9

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  • qualitative detection of saturated vapors of volatile organic compounds due to configuration changes of the photonic bandgap, recorded by diffuse reflectance spectroscopy. The exposure of the sensor to aromatic (benzene, toluene and p-xylene) and aliphatic (n-pentane, n-heptane, n-octane and n-decane
  • ) hydrocarbons has been analyzed. The reconstitution of spectral parameters of the sensor during the periodic detection of saturated vapors of toluene has been evaluated. Keywords: diffuse reflectance spectroscopy; photonic crystal sensor; stimuli-responsive materials; Introduction Photonic crystals (PhCs
  • are a CCA of polystyrene submicrometer particles embedded in a polydimethylsiloxane (PDMS) layer. The matrix interaction was responsible for the main mechanism, which was monitored by configuration changes of the photonic bandgap using diffuse reflectance spectroscopy. Results and Discussion
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Published 25 Jan 2022

Tin dioxide nanomaterial-based photocatalysts for nitrogen oxide oxidation: a review

  • Viet Van Pham,
  • Hong-Huy Tran,
  • Thao Kim Truong and
  • Thi Minh Cao

Beilstein J. Nanotechnol. 2022, 13, 96–113, doi:10.3762/bjnano.13.7

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  • photoinduced electrons from the CB of BiOBr to that of SnO2, thus prolonging the lifetime of photogenerated electron–hole pairs (Figure 8). The NO-to-NO2 conversion and intermediates and products were confirmed via in situ diffuse reflectance infrared Fourier transform spectroscopy during NO oxidation [70
  • –210, Copyright (2017), with permission from Elsevier. This content is not subject to CC BY 4.0. (a) Diffuse reflectance spectra of SnO2 and SnO2/GQDs composites. Inset is the absorption spectrum of GQDs dispersed in water. (b) PL spectra of SnO2 and SnO2/GQDs composites. Excitation wavelength: 260 nm
  • reports still proposed its photocatalytic behaviors partly based on •O2− species via the combination of experimental physicochemical analyses, such as electron spin resonance (ESR) spectroscopy, active species trapping experiments, valence band X-ray photoelectron spectroscopy (XPS), and diffuse
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Published 21 Jan 2022

A Au/CuNiCoS4/p-Si photodiode: electrical and morphological characterization

  • Adem Koçyiğit,
  • Adem Sarılmaz,
  • Teoman Öztürk,
  • Faruk Ozel and
  • Murat Yıldırım

Beilstein J. Nanotechnol. 2021, 12, 984–994, doi:10.3762/bjnano.12.74

Graphical Abstract
  • results of the CuNiCoS4 nanocrystals confirmed that the nanocrystals are suitable for interfacial layers of photodiodes. Optical properties The optical properties of CuNiCoS4 nanocrystals were investigated by absorbance and diffuse reflectance spectroscopy (Figure 3). As can be seen in Figure 3a, the
  • synthesized nanocrystals exhibit strong absorption over a broad spectrum including the ultraviolet and the near-infrared region. Furthermore, the graph of the diffuse reflectance spectroscopy is given as an inset in Figure 3a. The obtained result show that the absorption of CuNiCoS4 nanocrystals increases
  • illustration and (b) band diagram of the fabricated Au/CuNiCoS4/p-Si photodiode. (a) XRD pattern and crystal structure model, (b) TEM image, (c) HR-TEM interplanar spacing image, (d) FE-SEM image and (e) EDS pattern of the CuNiCoS4 nanocrystals. (a) Absorbance spectroscopy graph (inset figure: diffuse
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Published 02 Sep 2021

Boosting of photocatalytic hydrogen evolution via chlorine doping of polymeric carbon nitride

  • Malgorzata Aleksandrzak,
  • Michalina Kijaczko,
  • Wojciech Kukulka,
  • Daria Baranowska,
  • Martyna Baca,
  • Beata Zielinska and
  • Ewa Mijowska

Beilstein J. Nanotechnol. 2021, 12, 473–484, doi:10.3762/bjnano.12.38

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  • -PCN were investigated via UV–vis diffuse reflectance spectroscopy (DRS) and photoluminescence (PL) emission spectroscopy. Figure 8a shows the Kubelka–Munk function curves of the fabricated materials. The bandgap is 2.78 and 2.77 eV for PCN and Cl-PCN, respectively, indicating that the Cl-doping had no
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Published 19 May 2021

Unravelling the interfacial interaction in mesoporous SiO2@nickel phyllosilicate/TiO2 core–shell nanostructures for photocatalytic activity

  • Bridget K. Mutuma,
  • Xiluva Mathebula,
  • Isaac Nongwe,
  • Bonakele P. Mtolo,
  • Boitumelo J. Matsoso,
  • Rudolph Erasmus,
  • Zikhona Tetana and
  • Neil J. Coville

Beilstein J. Nanotechnol. 2020, 11, 1834–1846, doi:10.3762/bjnano.11.165

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  • . Therefore, in this study we report on the growth of mesoporous SiO2@NiPS and titania-coated mSiO2@NiPS (mSiO2@NiPS/TiO2) core–shell nanostructures using a simple deposition-precipitation method. Transmission electron microscopy (TEM), N2 physisorption analysis, diffuse reflectance UV–visible spectroscopy
  • functionality of nanomaterials greatly influence their photoactivity. UV–vis diffuse reflectance spectroscopy is a useful technique for probing the optoelectronic properties, band structure and molecular energy levels of semiconductors. It gives relevant information on the optical activity of nanomaterials as
  • support for TiO2 creating a photocatalyst with improved photoactivity due to the presence of more active sites for the adsorption of the MV dye molecules. Additionally, from the diffuse reflectance UV–vis data, an optical bandgap of approximately 2.05 eV was obtained for mSiO2@NiPS while that of mSiO2
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Published 09 Dec 2020

Nanocasting synthesis of BiFeO3 nanoparticles with enhanced visible-light photocatalytic activity

  • Thomas Cadenbach,
  • Maria J. Benitez,
  • A. Lucia Morales,
  • Cesar Costa Vera,
  • Luis Lascano,
  • Francisco Quiroz,
  • Alexis Debut and
  • Karla Vizuete

Beilstein J. Nanotechnol. 2020, 11, 1822–1833, doi:10.3762/bjnano.11.164

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  • -fabricated metal carboxylates as metal precursors. To the best of our knowledge, the synthesized particles are the smallest BiFeO3 particles ever prepared by any method. The samples were characterized by X-ray powder diffraction, transmission electron microscopy and UV–vis diffuse reflectance spectroscopy
  • non-agglomerated nanoparticles. We would like to point out that, to the best of our knowledge, the present pure-phase 5.5 nm BiFeO3 nanoparticles are the smallest nanoparticles of that material so far. In order to investigate the optical properties of the nanocast BiFeO3 powder, diffuse reflectance UV
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Published 07 Dec 2020

A 3D-polyphenylalanine network inside porous alumina: Synthesis and characterization of an inorganic–organic composite membrane

  • Jonathan Stott and
  • Jörg J. Schneider

Beilstein J. Nanotechnol. 2020, 11, 938–951, doi:10.3762/bjnano.11.78

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  • ALOX surface and the crystal of the ATR module could not be achieved, therefore we employed diffuse reflectance infrared Fourier transform spectroscopy (DRIFT) to analyze surface-grafted polymers. Figure 7 shows the NIR spectra of the outer surface of the pPA-functionalized ALOX-membranes. All observed
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Published 17 Jun 2020

Effect of Ag loading position on the photocatalytic performance of TiO2 nanocolumn arrays

  • Jinghan Xu,
  • Yanqi Liu and
  • Yan Zhao

Beilstein J. Nanotechnol. 2020, 11, 717–728, doi:10.3762/bjnano.11.59

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  • the array was measured using a laser of 325 nm excitation wavelength and a grating spectrometer (Horiba, JY iHR550). The diffuse reflectance absorption spectrum of the array was measured using an ultraviolet–visible spectrophotometer (UV–vis, Shimadzu, UV-3600). Photocatalytic experiments. The
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Published 05 May 2020

Synthesis and enhanced photocatalytic performance of 0D/2D CuO/tourmaline composite photocatalysts

  • Changqiang Yu,
  • Min Wen,
  • Zhen Tong,
  • Shuhua Li,
  • Yanhong Yin,
  • Xianbin Liu,
  • Yesheng Li,
  • Tongxiang Liang,
  • Ziping Wu and
  • Dionysios D. Dionysiou

Beilstein J. Nanotechnol. 2020, 11, 407–416, doi:10.3762/bjnano.11.31

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  • ) spectra. UV–visible diffuse reflectance spectra were measured using a Lambda 750S UV–vis spectrophotometer (Perkin-Elmer, USA) calibrated using barium sulfate. Photoluminescence (PL) spectra were measured with a F-4600 fluorescence spectrophotometer (Hitachi, Japan) with an excitation wavelength of 400 nm
  • (15.219 nm, 0.049 cm3 g−1) were analyzed according to the Barrett–Joyner–Halenda (BJH) method (Figure 4b). The larger pore volume and BET specific surface area confirmed that the CuO/tourmaline composite with 0D/2D CuO structure possessed an increased number of active sites. UV–vis diffuse reflectance
  • ) BJH pore size distribution of the CuO, tourmaline, and CuO/tourmaline composite. (a) UV–vis diffuse reflectance spectra, (b) plots of (Ahν)2 vs hν, (c) transient photocurrent, and (d) time-resolved PL spectra of the CuO and CuO/tourmaline composite. (a) MB degradation, (b) the apparent pseudo-first
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Published 02 Mar 2020
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