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Search for "mesoporous" in Full Text gives 197 result(s) in Beilstein Journal of Nanotechnology.

Plant growth regulation by seed coating with films of alginate and auxin-intercalated layered double hydroxides

  • Vander A. de Castro,
  • Valber G. O. Duarte,
  • Danúbia A. C. Nobre,
  • Geraldo H. Silva,
  • Vera R. L. Constantino,
  • Frederico G. Pinto,
  • Willian R. Macedo and
  • Jairo Tronto

Beilstein J. Nanotechnol. 2020, 11, 1082–1091, doi:10.3762/bjnano.11.93

Graphical Abstract
  • with indefinitely coherent fragments [28][29]. The volume and average pore diameter values are characteristic of a mesoporous material. Scanning electron microscopy (SEM) images of NAA and ZnAl-NAA-LDH, presented in Figure 4, show the presence of particles with a smooth surface, probably resulting from
  • for the material (19.5 Å) is characteristic of the intercalation of NAA between LDH layers. The auxin intercalated into ZnAl-NAA-LDH was thermally decomposed at temperatures above 270 °C. The hybrid material showed a low specific surface area (29.7 m2·g−1) and a mesoporous volume (0.17 cm3·g−1). The
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Published 24 Jul 2020

A novel dry-blending method to reduce the coefficient of thermal expansion of polymer templates for OTFT electrodes

  • Xiangdong Ye,
  • Bo Tian,
  • Yuxuan Guo,
  • Fan Fan and
  • Anjiang Cai

Beilstein J. Nanotechnol. 2020, 11, 671–677, doi:10.3762/bjnano.11.53

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  • the influence of fullerene (C60) on the CTE of Araldite LY 5052/Aradur HY 5052 cross-linked epoxy resin by molecular dynamics simulations. The CTE was minimized by adding a maximum of 15.9 wt % fullerene to the LY/HY/C60 epoxy system. Liu et al. [14] selected MCM-41 mesoporous silica nanoparticles
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Published 20 Apr 2020

Adsorptive removal of bulky dye molecules from water with mesoporous polyaniline-derived carbon

  • Hyung Jun An,
  • Jong Min Park,
  • Nazmul Abedin Khan and
  • Sung Hwa Jhung

Beilstein J. Nanotechnol. 2020, 11, 597–605, doi:10.3762/bjnano.11.47

Graphical Abstract
  • under different temperatures and applied for the purification of water contaminated with dye molecules of different sizes and charge by adsorption. With increasing pyrolysis temperature, it was found that the hydrophobicity, pore size and mesopore volume increased. A mesoporous PDC sample obtained via
  • because of functional carbon materials (graphene [16] or porous carbon [17]), mesoporous materials [18] and MOFs [19][20][21][22]. For example, MOFs [23][24][25], carbonaceous materials (such as carbon nanotubes, graphene, biochar and activated carbon) [26] and clay [27] have been applied in adsorptive
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Published 08 Apr 2020

Synthesis and enhanced photocatalytic performance of 0D/2D CuO/tourmaline composite photocatalysts

  • Changqiang Yu,
  • Min Wen,
  • Zhen Tong,
  • Shuhua Li,
  • Yanhong Yin,
  • Xianbin Liu,
  • Yesheng Li,
  • Tongxiang Liang,
  • Ziping Wu and
  • Dionysios D. Dionysiou

Beilstein J. Nanotechnol. 2020, 11, 407–416, doi:10.3762/bjnano.11.31

Graphical Abstract
  • photocatalysts was analyzed by their nitrogen adsorption–desorption isotherms. As shown in Figure 4a, CuO, tourmaline, and CuO/tourmaline composite exhibited type-IV adsorption isotherms, which are characteristic of mesoporous materials. As shown in Table 1, the Brunauer–Emmett–Teller (BET) specific surface area
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Published 02 Mar 2020

Interactions at the cell membrane and pathways of internalization of nano-sized materials for nanomedicine

  • Valentina Francia,
  • Daphne Montizaan and
  • Anna Salvati

Beilstein J. Nanotechnol. 2020, 11, 338–353, doi:10.3762/bjnano.11.25

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  • required to wrap a lipid membrane around a nanoparticle with high aspect ratio [148]. However, also in relation to this aspect, conflicting results were found in which cross-linked poly(ethylene glycol) hydrogels or mesoporous silica particles with higher aspect ratio were internalized quicker and more
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Published 14 Feb 2020

High-performance asymmetric supercapacitor made of NiMoO4 nanorods@Co3O4 on a cellulose-based carbon aerogel

  • Meixia Wang,
  • Jing Zhang,
  • Xibin Yi,
  • Benxue Liu,
  • Xinfu Zhao and
  • Xiaochan Liu

Beilstein J. Nanotechnol. 2020, 11, 240–251, doi:10.3762/bjnano.11.18

Graphical Abstract
  • considered an ideal supporting material to hybridize with electroactive materials because of its low cost, easy fabrication, large surface area, interconnected porosity and high electrical conductivity [30][31]. Due to its micro/mesoporous 3D morphology with large open pores, it offers more space to grow
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Published 21 Jan 2020

Synthesis of amorphous and graphitized porous nitrogen-doped carbon spheres as oxygen reduction reaction catalysts

  • Maximilian Wassner,
  • Markus Eckardt,
  • Andreas Reyer,
  • Thomas Diemant,
  • Michael S. Elsaesser,
  • R. Jürgen Behm and
  • Nicola Hüsing

Beilstein J. Nanotechnol. 2020, 11, 1–15, doi:10.3762/bjnano.11.1

Graphical Abstract
  • for g-NCS-850 and g-NCS-1000. Amorphous carbon spheres show a smooth surface and distinct microporosity; upon graphitization the surface becomes partially perforated or eroded creating a mesoporous system. For both sample series, NCS and g-NCS, the C content increases while the amount of O and H
  • materials we found a clear ORR activity only after nitriding at 1000 °C. Only the sample TaON@NCS-1000 exhibited a mesoporous shell, thus improving access to the N-doped carbon core. The resulting TaON@NCS-1000 catalyst features a rather similar onset (0.7 V) as the NCS-1000 sample, and similar j–E
  • cases direct comparison of the ORR performance after similar nitriding temperatures is even less possible. Nevertheless, for nitriding temperatures above and below 1000 °C, the TaON layer seems to block the ORR activity of the nitrided carbon cores very likely due to the lack of the permeable mesoporous
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Published 02 Jan 2020

Advanced hybrid nanomaterials

  • Andreas Taubert,
  • Fabrice Leroux,
  • Pierre Rabu and
  • Verónica de Zea Bermudez

Beilstein J. Nanotechnol. 2019, 10, 2563–2567, doi:10.3762/bjnano.10.247

Graphical Abstract
  • the polyol process” [19], the synthetic process was found to be of prime importance to shape the nanoparticles and to optimize their surface/volume ratio in relation to the magnetic behavior. A one-step non-hydrolytic sol–gel synthesis of mesoporous TiO2 phosphonate hybrid materials was applied to
  • (ethylene oxide)-b-poly(acrylic acid) (PEO-b-PAA) and an oligo-chitosan-type polyamine was used as a structure-directing agent to prepare ordered mesoporous silica materials in the work “pH-mediated control over the mesostructure of ordered mesoporous materials templated by polyion complex micelles” [22
  • speciation can be targeted. For example, in the work “New micro/mesoporous nanocomposite material from low-cost sources for the efficient removal of aromatic and pathogenic pollutants from water”, a hybrid kaolinite nanocomposite was assembled via Zn cations upon calcination, resulting in a low-cost porous
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Published 20 Dec 2019

Air oxidation of sulfur mustard gas simulants using a pyrene-based metal–organic framework photocatalyst

  • Ghada Ayoub,
  • Mihails Arhangelskis,
  • Xuan Zhang,
  • Florencia Son,
  • Timur Islamoglu,
  • Tomislav Friščić and
  • Omar K. Farha

Beilstein J. Nanotechnol. 2019, 10, 2422–2427, doi:10.3762/bjnano.10.232

Graphical Abstract
  • , 3.4 mg) of the MOF, no conversion of CEES was detected (Figure 2), confirming the role of NU-400 as a photocatalyst. The photocatalytic activity of NU-400 in air, without oxygen presaturation, is significantly higher compared to the previously explored mesoporous NU-1000 MOF, which is based on a
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Published 09 Dec 2019

Coating of upconversion nanoparticles with silica nanoshells of 5–250 nm thickness

  • Cynthia Kembuan,
  • Maysoon Saleh,
  • Bastian Rühle,
  • Ute Resch-Genger and
  • Christina Graf

Beilstein J. Nanotechnol. 2019, 10, 2410–2421, doi:10.3762/bjnano.10.231

Graphical Abstract
  • such as peptides, antibodies or nucleic acids for bioimaging applications or fluorescence assays. The growth of a mesoporous silica shell on a microporous silica shell can also be applied for the subsequent use of these nanomaterials for drug loading and delivery [69]. Experimental All syntheses were
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Published 09 Dec 2019

Semitransparent Sb2S3 thin film solar cells by ultrasonic spray pyrolysis for use in solar windows

  • Jako S. Eensalu,
  • Atanas Katerski,
  • Erki Kärber,
  • Lothar Weinhardt,
  • Monika Blum,
  • Clemens Heske,
  • Wanli Yang,
  • Ilona Oja Acik and
  • Malle Krunks

Beilstein J. Nanotechnol. 2019, 10, 2396–2409, doi:10.3762/bjnano.10.230

Graphical Abstract
  • pioneered by the teams of Nair, Nezu, and Hodes in the mid-2000s [19][23][24]. The record PCE of 7.5%, achieved with solar cells based on Sb2S3 grown by chemical bath deposition (CBD) into mesoporous TiO2, shows the excellent potential of Sb2S3 as a PV absorber, and the suitability of its fabrication by
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Published 06 Dec 2019

Polyvinylpyrrolidone as additive for perovskite solar cells with water and isopropanol as solvents

  • Chen Du,
  • Shuo Wang,
  • Xu Miao,
  • Wenhai Sun,
  • Yu Zhu,
  • Chengyan Wang and
  • Ruixin Ma

Beilstein J. Nanotechnol. 2019, 10, 2374–2382, doi:10.3762/bjnano.10.228

Graphical Abstract
  • remarkable light absorption capacity [5] and the tunable band gap [6] of inorganic–organic lead halide perovskite crystals make them suitable for the production of organic semiconductors [7], photodetectors [8], and photovoltaics [5]. In 2009, Kojima et al. achieved a breakthrough in using mesoporous TiO2 as
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Published 05 Dec 2019

Design and facile synthesis of defect-rich C-MoS2/rGO nanosheets for enhanced lithium–sulfur battery performance

  • Chengxiang Tian,
  • Juwei Wu,
  • Zheng Ma,
  • Bo Li,
  • Pengcheng Li,
  • Xiaotao Zu and
  • Xia Xiang

Beilstein J. Nanotechnol. 2019, 10, 2251–2260, doi:10.3762/bjnano.10.217

Graphical Abstract
  • range of 0.45–1.0 P/P0 suggests the presence of a mesoporous structure, as displayed in Figure 5a. The specific surface area was calculated to be 131.72, 300.64, 539.16 m2·g−1 by using the Brunauer–Emmett–Teller (BET) method. The pore size distribution obtained from the Barrett–Joyner–Halenda (BJH
  • , demonstrating the mesoporous structure C-MoS2/rGO-6. The specific surface area (130.57 m2·g−1) of C-MoS2/rGO-6-S composite is significantly smaller than that of C-MoS2/rGO-6 as shown in Figure S3a (Supporting Information File 1). Additionally, the broad pore size distribution, ranging from 2 to 10 nm
  • , diminished obviously in the C-MoS2/rGO-6-S composite (Figure S3b, Supporting Information File 1) compared to the C-MoS2/rGO-6 composite, which indicates that sulfur can be successfully dispersed into the mesoporous of the C-MoS2/rGO-6 composite. Among all samples, the C-MoS2/rGO-6 composite has the largest
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Published 14 Nov 2019

Targeted therapeutic effect against the breast cancer cell line MCF-7 with a CuFe2O4/silica/cisplatin nanocomposite formulation

  • B. Rabindran Jermy,
  • Vijaya Ravinayagam,
  • Widyan A. Alamoudi,
  • Dana Almohazey,
  • Hatim Dafalla,
  • Lina Hussain Allehaibi,
  • Abdulhadi Baykal,
  • Muhammet S. Toprak and
  • Thirunavukkarasu Somanathan

Beilstein J. Nanotechnol. 2019, 10, 2217–2228, doi:10.3762/bjnano.10.214

Graphical Abstract
  • (magnetic resonance imaging), tissue repair, and thermal ablation have been gaining considerable attention in recent years. In particular, the use of superparamagnetic iron oxide nanoparticles (SPIONs) is now advantageous as they are FDA-approved for clinical use [2]. Magnetic Fe3O4-based mesoporous silica
  • form aggregates, exert variable oxidation states and result in dose-dependent toxicity. Several supports, including silica and carbon, were used to reduce such aggregation. Notably, different types of nanocomposites were reported based on Co, Ni, Mn and Fe over mesoporous carbon capsules [8]. A carbon
  • surface anisotropy effect [9][10]. Among the ferrites, copper ferrites are interesting due to their superior conductive and magnetic characteristics. A mesoporous Cu1−xZnxFe2O4 system has been reported using a nanocasting technique [11]. Based on the Bertaut analysis, the doping of Zn tends to form mixed
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Published 12 Nov 2019

Ultrathin Ni1−xCoxS2 nanoflakes as high energy density electrode materials for asymmetric supercapacitors

  • Xiaoxiang Wang,
  • Teng Wang,
  • Rusen Zhou,
  • Lijuan Fan,
  • Shengli Zhang,
  • Feng Yu,
  • Tuquabo Tesfamichael,
  • Liwei Su and
  • Hongxia Wang

Beilstein J. Nanotechnol. 2019, 10, 2207–2216, doi:10.3762/bjnano.10.213

Graphical Abstract
  • nanoflakes, the results were compared with previously reported NiCo-based ASCs. The new device outperforms Ni3S2/CoNi2S4/NF//AC [41], NiCo2S4/graphene//AC [39], NiCo2S4/NCF//(OMC = ordered mesoporous carbon)/NCF [31], NiCo2O4//AC [17], NiCo-sulfide//AC [28] and NiCo-hydroxide//AC [42]. The EIS results of the
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Published 11 Nov 2019

Improved adsorption and degradation performance by S-doping of (001)-TiO2

  • Xiao-Yu Sun,
  • Xian Zhang,
  • Xiao Sun,
  • Ni-Xian Qian,
  • Min Wang and
  • Yong-Qing Ma

Beilstein J. Nanotechnol. 2019, 10, 2116–2127, doi:10.3762/bjnano.10.206

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  • performance. Li et al. synthesized composites of mesoporous (001)-TiO2 and C applying a one-pot hydrothermal strategy in the presence of glucose and hydrofluoric acid (HF). The composites an exhibited excellent visible-light-driven photocatalytic performance [14]. Chen et al. synthesized a composite of g-C3N4
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Published 01 Nov 2019

Synthesis of highly active ETS-10-based titanosilicate for heterogeneously catalyzed transesterification of triglycerides

  • Muhammad A. Zaheer,
  • David Poppitz,
  • Khavar Feyzullayeva,
  • Marianne Wenzel,
  • Jörg Matysik,
  • Radomir Ljupkovic,
  • Aleksandra Zarubica,
  • Alexander A. Karavaev,
  • Andreas Pöppl,
  • Roger Gläser and
  • Muslim Dvoyashkin

Beilstein J. Nanotechnol. 2019, 10, 2039–2061, doi:10.3762/bjnano.10.200

Graphical Abstract
  • noting that the appearance of mesopores after treatment has led to the change of the isotherm shape from type I (typical for microporous solids) to a combination of types I and IV, as is expected for micro–mesoporous materials [37]. It was suggested that exposure of the ETS-10 framework to H2O2 solution
  • the possible diffusion exchange with the intercrystalline space during the used diffusion time (20 ms). It is worth mentioning that in both catalysts, microporous Na,K-ETS-10 and micro–mesoporous P-ETS-10/60, the amount of triolein was below the detection limit. While for the microporous
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Published 28 Oct 2019

Review of advanced sensor devices employing nanoarchitectonics concepts

  • Katsuhiko Ariga,
  • Tatsuyuki Makita,
  • Masato Ito,
  • Taizo Mori,
  • Shun Watanabe and
  • Jun Takeya

Beilstein J. Nanotechnol. 2019, 10, 2014–2030, doi:10.3762/bjnano.10.198

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  • particles [122]. Mesoporous carbons were used for sensing of tannins in acidic aqueous environment with highly cooperative adsorption in the mesochannels [123]. The nanoarchitectonic construction of carbon nanocages with high surface mesoporous structures [124] was integrated with electrospun polymer fibers
  • and resulted in a highly sensitive sensing material for aniline vapor [125]. Layer-by-layer structures of mesoporous carbon capsules can work as sensing membranes capable of selectively sensing through the doping of secondary sensing units [126]. As an emerging nanoporous material, metal–organic
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Published 16 Oct 2019

The influence of porosity on nanoparticle formation in hierarchical aluminophosphates

  • Matthew E. Potter,
  • Lauren N. Riley,
  • Alice E. Oakley,
  • Panashe M. Mhembere,
  • June Callison and
  • Robert Raja

Beilstein J. Nanotechnol. 2019, 10, 1952–1957, doi:10.3762/bjnano.10.191

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  • nanoparticles in a catalytic reaction [12]. However, due to the limited pore aperture and channels of these systems, even sub-nanometre particles can block the framework and hinder activity, thereby preventing reagents from accessing the internal active sites. In contrast, mesoporous species (pores greater than
  • hierarchical nature of the sample (Figure S2, Supporting Information File 1), but with a disordered mesoporous region. This is typical of hierarchical materials prepared in this manner [12][14] as they contain a broad range of mesopore sizes. Subsequent pore-distribution plots show no textural features for MP
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Published 25 Sep 2019

Facile synthesis of carbon nanotube-supported NiO//Fe2O3 for all-solid-state supercapacitors

  • Shengming Zhang,
  • Xuhui Wang,
  • Yan Li,
  • Xuemei Mu,
  • Yaxiong Zhang,
  • Jingwei Du,
  • Guo Liu,
  • Xiaohui Hua,
  • Yingzhuo Sheng,
  • Erqing Xie and
  • Zhenxing Zhang

Beilstein J. Nanotechnol. 2019, 10, 1923–1932, doi:10.3762/bjnano.10.188

Graphical Abstract
  • –Halenda (BJH) pore size distribution of CC-CNT@Fe2O3 are shown in Supporting Information File 1, Figure S4. It is a type-IV isotherm, indicating the mesoporous texture of the sample (Figure S4a, Supporting Information File 1). The BET surface area was found to be 24.9 m2·g−1, much larger than that of pure
  • , verifying the mesoporous texture of the sample (Figure S7a, Supporting Information File 1). The BET surface area was 34.4 m2·g−1, much larger than that of pure carbon cloth (0.2 m2·g−1). Pore size distribution (Figure S4b, Supporting Information File 1) shows that numerous pores have a size of about 2 and
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Published 23 Sep 2019

Charge-transfer interactions between fullerenes and a mesoporous tetrathiafulvalene-based metal–organic framework

  • Manuel Souto,
  • Joaquín Calbo,
  • Samuel Mañas-Valero,
  • Aron Walsh and
  • Guillermo Mínguez Espallargas

Beilstein J. Nanotechnol. 2019, 10, 1883–1893, doi:10.3762/bjnano.10.183

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  • (CT) process between the framework and the guest molecules is a crucial step towards the design of new electroactive MOFs. Herein, we present the encapsulation of fullerenes (C60) in a mesoporous tetrathiafulvalene (TTF)-based MOF. The CT process between the electron-acceptor C60 guest and the
  • is based on the 6-connected trimeric cluster [Fe3(μ3O)(COO)6] as secondary building unit (SBU) and tetratopic tetrathiafulvalene-tetrabenzoate (TTFTB4−) ligands. This MOF shows a hierarchical structure with mesoporous channels of ≈3 nm and orthogonal microporous channels of ≈1 nm. In addition, it
  • along the c-axis), which could prevent the charge delocalisation along the framework. Conclusion In summary, we have reported for the first time the encapsulation of C60 in a mesoporous TTF-based MOF (MUV-2). Charge-transfer interactions between C60 and TTF ligands from the framework in C60@MUV-2 were
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Published 18 Sep 2019

Layered double hydroxide/sepiolite hybrid nanoarchitectures for the controlled release of herbicides

  • Ediana Paula Rebitski,
  • Margarita Darder and
  • Pilar Aranda

Beilstein J. Nanotechnol. 2019, 10, 1679–1690, doi:10.3762/bjnano.10.163

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  • , iii) field-induced material control, iv) new manipulations of atoms and molecules, and v) theoretical modeling and design [1][2]. Based on these premises a large number of nanoarchitectonic materials have been prepared including mesoporous solids, self-organized block-copolymers, supramolecular
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Published 09 Aug 2019

Nanoporous smartPearls for dermal application – Identification of optimal silica types and a scalable production process as prerequisites for marketed products

  • David Hespeler,
  • Sanaa El Nomeiri,
  • Jonas Kaltenbach and
  • Rainer H. Müller

Beilstein J. Nanotechnol. 2019, 10, 1666–1678, doi:10.3762/bjnano.10.162

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  • parameters (e.g., particle size, pore diameter, pore volume) in order to identify particles which are most easy to process. Materials and Methods Materials Rutin with a purity of 95% was purchased from Denk Ingredients (Munich, Germany). Various mesoporous silica particles (Table 1) with pore diameter of 3
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Published 08 Aug 2019

Materials nanoarchitectonics at two-dimensional liquid interfaces

  • Katsuhiko Ariga,
  • Michio Matsumoto,
  • Taizo Mori and
  • Lok Kumar Shrestha

Beilstein J. Nanotechnol. 2019, 10, 1559–1587, doi:10.3762/bjnano.10.153

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  • -dimensional fullerene objects, Ji, Shrestha, and co-workers reported the synthesis of two-dimensional mesoporous carbon microbelts and demonstrated their usage as electrode material for electrochemical supercapacitors (Figure 19) [251]. Two-dimensional belt-like mesoporous structures can be fabricated from
  • C60 molecules by liquid–liquid interfacial precipitation using a carbon disulfide solution of C60 and isopropyl alcohol. Under optimized conditions, these mesoporous C60 microbelts extended to lengths of the order of centimetres. Heat treatment of the obtained C60 microbelts converts them into two
  • -dimensional amorphous carbon microbelts at 900 °C and their dense graphitic versions at 2000 °C. Especially the former carbon material exhibited excellent electrochemical supercapacitive performance due to the enhanced surface area and the robust mesoporous framework motifs. The hierarchical bimodal pore
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Published 30 Jul 2019

BiOCl/TiO2/diatomite composites with enhanced visible-light photocatalytic activity for the degradation of rhodamine B

  • Minlin Ao,
  • Kun Liu,
  • Xuekun Tang,
  • Zishun Li,
  • Qian Peng and
  • Jing Huang

Beilstein J. Nanotechnol. 2019, 10, 1412–1422, doi:10.3762/bjnano.10.139

Graphical Abstract
  • diatomite, TiO2/diatomite and BTD have an H4-type hysteresis loop, indicating that all samples have a mesoporous structure. At the same time, the pore size distribution and average pore size also confirm that the samples have mesoporous structure. Figure 2b shows that the pore size distribution of BTD has a
  • wide size distribution, although most are mesoporous, and the rest are macroporous. The specific surface area of BTD is slightly lower than that of diatomite due to the surface loading of BiOCl and TiO2. The pore volume of the BTD composite is larger than that of BiOCl and TiO2/diatomite, which
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Published 16 Jul 2019
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