TEM sample preparation of lithographically patterned permalloy nanostructures on silicon nitride membranes

• Joshua Williams,
• Michael I. Faley,
• Joseph Vimal Vas,
• Peng-Han Lu and
• Rafal E. Dunin-Borkowski

Beilstein J. Nanotechnol. 2024, 15, 1–12, doi:10.3762/bjnano.15.1

• . Fences and edge roughness from the imperfect lift-off process were reported to influence the magnetic properties of nanostructures [22]. The third method, stencil lithography, makes use of a shadow mask, which was fabricated by milling submicrometer apertures on a conventional TEM grid using a focused

Spatial variations of conductivity of self-assembled monolayers of dodecanethiol on Au/mica and Au/Si substrates

• Julian Skolaut,
• Jędrzej Tepper,
• Federica Galli,
• Wulf Wulfhekel and
• Jan M. van Ruitenbeek

Beilstein J. Nanotechnol. 2023, 14, 1169–1177, doi:10.3762/bjnano.14.97

• rougher and a flatter gold substrate on the lateral variation of the conductivity. We find that the roughness of the substrate crucially defines this variation. We conclude that it is paramount to adequately choose a gold substrate for investigations on molecular layer conductivity. Keywords: Au/mica; Au

• substrates consisting of thin Au layers of different surface roughness. We compare granular Au films deposited on Si wafers with epitaxial (flat) Au films on mica. Experimental Before the experimental results are presented, this section focuses on the preparation of the samples under study and the setup used

• two DDT/Au/mica samples were investigated, yielding consistent results. In Figure 3a, the topography is similar to that obtained for the bare Au/mica surface, that is, relatively large flat areas, only small height differences throughout the image, and small roughness of the surface. By means of

Industrial perspectives for personalized microneedles

• Remmi Danae Baker-Sediako,
• Benjamin Richter,
• Matthias Blaicher,
• Michael Thiel and
• Martin Hermatschweiler

Beilstein J. Nanotechnol. 2023, 14, 857–864, doi:10.3762/bjnano.14.70

• artifact from slicing the computer-aided design (CAD) into layers [47][48]. The staircase effect leads to increased surface roughness of the order of micrometers, and high surface roughness on the microneedles will require substantially more pressure to penetrate the skin. These slicing artifacts

Biomimetics on the micro- and nanoscale – The 25th anniversary of the lotus effect

• Matthias Mail,
• Kerstin Koch,
• Thomas Speck,
• William M. Megill and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2023, 14, 850–856, doi:10.3762/bjnano.14.69

• material through a few steps. In the first step, a molten polypropylene layer is laminated onto a carrier film and run over rollers to cool down. Then the combined laminate is forced through a gap between a hot sandblasted roller and a cold smooth one. The surface roughness and temperature difference

• also reflected in the adhesive forces the animals are able to produce on surfaces of varying roughness. These observations make specific predictions about the behavioural ecology of this species in the wild. They also remind us to keep looking at the archetypes and closely related species for further

Cross-sectional Kelvin probe force microscopy on III–V epitaxial multilayer stacks: challenges and perspectives

• Mattia da Lisca,
• José Alvarez,
• James P. Connolly,
• Nicolas Vaissiere,
• Karim Mekhazni,
• Jean Decobert and
• Jean-Paul Kleider

Beilstein J. Nanotechnol. 2023, 14, 725–737, doi:10.3762/bjnano.14.59

• , that is, the surface of the 2D wafer (e.g., around 3.09 μm in Figure 2). In order to achieve a successful KPFM analysis, a low surface roughness is essential to obtain high-quality images since surface inhomogeneities can cause a topographical image imprint on the surface potential image. With

• sufficiently low surface roughness, the topographic influence on the measurement is minor, and the observed contrast of the VCPD map is dominated by the surface potential such that topographic artefacts can be neglected. A first look at the VCPD image and the extrapolated profile (Figure 2c) allows for a

Investigations on the optical forces from three mainstream optical resonances in all-dielectric nanostructure arrays

• Guangdong Wang and
• Zhanghua Han

Beilstein J. Nanotechnol. 2023, 14, 674–682, doi:10.3762/bjnano.14.53

• , such as surface roughness, a BIC will turn into a quasi-BIC mode with both the Q-factor and resonant bandwidth becoming limited. Many applications of quasi-BICs have been reported, including ultrasensitive sensing [13], ultra-narrow bandwidth filters [14], and enhanced nonlinear effects [15]. The BICs

Thermal transport in kinked nanowires through simulation

• Alexander N. Robillard,
• Graham W. Gibson and
• Ralf Meyer

Beilstein J. Nanotechnol. 2023, 14, 586–602, doi:10.3762/bjnano.14.49

• systems with high surface roughness. Note the probability of specular reflection is constant here and not a function of the phonon wavelength or incidence angle, so specularities between 0% and 100% should be taken with this in mind. More sophisticated methods for calculating the probability of

SERS performance of GaN/Ag substrates fabricated by Ag coating of GaN platforms

• Magdalena A. Zając,
• Bogusław Budner,
• Malwina Liszewska,
• Bartosz Bartosewicz,
• Łukasz Gutowski,
• Jan L. Weyher and
• Bartłomiej J. Jankiewicz

Beilstein J. Nanotechnol. 2023, 14, 552–564, doi:10.3762/bjnano.14.46

• absorption level for samples in a given series, it can be seen that an increase in the amount of deposited metal causes a decrease in light absorption, which is related to a decrease in surface roughness and the filling of the nanoporous GaN structure with silver. SERS performance of fabricated of GaN/Ag

Observation of multiple bulk bound states in the continuum modes in a photonic crystal cavity

• Rui Chen,
• Yi Zheng,
• Xingyu Huang,
• Qiaoling Lin,
• Chaochao Ye,
• Meng Xiong,
• Martijn Wubs,
• Yungui Ma,
• Minhao Pu and
• Sanshui Xiao

Beilstein J. Nanotechnol. 2023, 14, 544–551, doi:10.3762/bjnano.14.45

• influenced by both the radiative part Qr and a nonradiative part Qnr via 1/Q = 1/Qr + 1/Qnr provided that the material is lossless. Qnr incorporates defects such as structural disorder, surface roughness, and fabrication errors. The simulation of the unit cell was performed by COMSOL Multiphysics with

• nonradiative part of the Q factor mentioned above. Qnr is caused by structural imperfections and disorders, including roughness on the surface, tilted sidewalls, and incomplete etching of the AlGaAs layer, as shown in Figure 3a. Theoretically, resonances of high-order modes have lower Q factors and longer

Conjugated photothermal materials and structure design for solar steam generation

• Chia-Yang Lin and
• Tsuyoshi Michinobu

Beilstein J. Nanotechnol. 2023, 14, 454–466, doi:10.3762/bjnano.14.36

• depends on the number of layers, which was caused by the surface structure of the multilayer PPy nanosheets. The high roughness and sharp local curvature of the multilayer PPy nanosheets were retained and incident light was effectively redistributed. In other words, transmitted light is confined in the

Structural, optical, and bioimaging characterization of carbon quantum dots solvothermally synthesized from o-phenylenediamine

• Zoran M. Marković,
• Milica D. Budimir,
• Martin Danko,
• Dušan D. Milivojević,
• Pavel Kubat,
• Danica Z. Zmejkoski,
• Vladimir B. Pavlović,
• Marija M. Mojsin,
• Milena J. Stevanović and
• Biljana M. Todorović Marković

Beilstein J. Nanotechnol. 2023, 14, 165–174, doi:10.3762/bjnano.14.17

• nm (Figure S1c,d in Supporting Information File 1). Figure 1 shows the surface morphology of neat PU and a CQDs/PU sample. The RMS roughness values of these samples are 4.45 and 14.04 nm, respectively. FTIR, UV–vis, and PL spectra of CQDs and CQDs/PU To study the chemical and optical properties of

Characterisation of a micrometer-scale active plasmonic element by means of complementary computational and experimental methods

• Ciarán Barron,
• Giulia Di Fazio,
• Samuel Kenny,
• Silas O’Toole,
• Robin O’Reilly and
• Dominic Zerulla

Beilstein J. Nanotechnol. 2023, 14, 110–122, doi:10.3762/bjnano.14.12

• SPR curve is slightly broader than the simulated one. This is due to experimental broadening (in particular, the divergence of the laser beam), surface roughness, and further temperature-induced degradation effects that are not taken into account in the simplified simulation setup employed. In order

Antimicrobial and mechanical properties of functionalized textile by nanoarchitectured photoinduced Ag@polymer coating

• Jessica Plé,
• Marine Dabert,
• Helene Lecoq,
• Sophie Hellé,
• Lydie Ploux and
• Lavinia Balan

Beilstein J. Nanotechnol. 2023, 14, 95–109, doi:10.3762/bjnano.14.11

• surface roughness, as can be seen in the SEM images (Figure 7c). Consequently, the diffuse reflectivity drops in favor of the specular reflectance. The particles are no longer simply juxtaposed but form a continuous silver layer, especially after 1000 friction cycles. The characteristic silver plasmon

Electrical and optical enhancement of ITO/Mo bilayer thin films via laser annealing

• Abdelbaki Hacini,
• Ahmad Hadi Ali,
• Nurul Nadia Adnan and
• Nafarizal Nayan

Beilstein J. Nanotechnol. 2022, 13, 1589–1595, doi:10.3762/bjnano.13.133

• AFM analysis shows that grain size and RMS roughness increased from 16.02 to 36.19 nm and 0.4 to 2.6 nm, respectively, when the laser energy was increased to 120 mJ. The as-deposited sample has an optical transmittance of nearly 80% in the 300–800 nm range. The laser annealing yielded a higher

• roughness. In this work, we investigate the effect of laser annealing treatment on ITO/Mo (IM) bilayer thin films as transparent conducting material for solar cell applications. The structural, optical, and electrical properties of the IM structure were examined as functions of the laser energy

• roughness of the bilayer structure were studied utilizing an atomic force microscope (AFM, Bruker Dimension Edge) and the Gwyddion software. The optical transmission was measured using an UV–vis spectrophotometer (UV-3600i Plus, SHIMADZU) in the range of λ = 300–800 nm. Finally, the electrical properties

Induced electric conductivity in organic polymers

• Konstantin Y. Arutyunov,
• Anatoli S. Gurski,
• Vladimir V. Artemov,
• Alexander L. Vasiliev,
• Azat R. Yusupov,
• Danfis D. Karamov and
• Alexei N. Lachinov

Beilstein J. Nanotechnol. 2022, 13, 1551–1557, doi:10.3762/bjnano.13.128

• strip and the whole sandwich itself. (b) Atomic force microscope scan of a PDP film 0.1 wt % on Si substrate. The plot at the bottom illustrates the roughness of the surface along the indicated line. (c) Side view of a Pb–PDP–Pb structure on glass with solitary defect (lead shortcut) obtained by

Bending and punching characteristics of aluminum sheets using the quasi-continuum method

• Man-Ping Chang,
• Shang-Jui Lin and
• Te-Hua Fang

Beilstein J. Nanotechnol. 2022, 13, 1303–1315, doi:10.3762/bjnano.13.108

• strength at a specific structural orientation [51]. Besides, Tran et al. studied the friction and scratch characteristics of pure aluminum by the QC method. The bump width to the bump pitch (W/P) value, scratch depth, surface roughness, and indenter radius were set as variables in order to explore the

Growing up in a rough world: scaling of frictional adhesion and morphology of the Tokay gecko (Gekko gecko)

• Anthony J. Cobos and
• Timothy E. Higham

Beilstein J. Nanotechnol. 2022, 13, 1292–1302, doi:10.3762/bjnano.13.107

• lower values than smooth surfaces. The safety factor went down with body mass and with surface roughness, suggesting that smaller animals may be more likely to occupy rough substrates in their natural habitat. Keywords: allometry; biomechanics; ecology; habitat; ontogeny; substrate; Introduction

• Animals attach to surfaces in numerous ways, including claws, suction, and both wet and dry adhesion. In fact, some animals can utilize multiple attachment mechanisms [1][2], leading to multifunctionality across surfaces of varying roughness. Dry adhesion is found in many invertebrates and squamate

• different roughness? Second, how does adhesive performance and morphology vary with body size? Although the former has been the subject of a few studies, the latter has received almost no attention. Surfaces in nature are rarely smooth and geckos are found on all types of surfaces from rough rocks to

Laser-processed antiadhesive bionic combs for handling nanofibers inspired by nanostructures on the legs of cribellate spiders

• Sebastian Lifka,
• Kristóf Harsányi,
• Erich Baumgartner,
• Lukas Pichler,
• Dariya Baiko,
• Karsten Wasmuth,
• Johannes Heitz,
• Marco Meyer,
• Anna-Christin Joel,
• Jörn Bonse and
• Werner Baumgartner

Beilstein J. Nanotechnol. 2022, 13, 1268–1283, doi:10.3762/bjnano.13.105

• arithmetic average roughness (Ra), the quadratic average roughness (Rq) and the maximum height (Ry) were measured; the results are shown in Table 3. The results of the AFM measurements revealed that the LIPSS covering the Al alloy surface are rather flat. Ry, which represents basically double the amplitude a

• value is slightly higher for the LIPSS-covered sample than for polished control sample, which correlates with the behavior described in Figure 5. However, this effect could not be significantly proven. Furthermore, Table 3 shows that an increasing surface roughness does not necessarily entail a

• decreasing peel-off force in the case of nanofibers. For example, the Ra value for all randomly rough surfaces is much higher than that for the LIPSS-covered Ti alloy sample, but the measured peel-off force is much lower for the LIPSS-covered Ti alloy sample. In addition, despite the high roughness of the

Roll-to-roll fabrication of superhydrophobic pads covered with nanofur for the efficient clean-up of oil spills

• Patrick Weiser,
• Robin Kietz,
• Marc Schneider,
• Matthias Worgull and
• Hendrik Hölscher

Beilstein J. Nanotechnol. 2022, 13, 1228–1239, doi:10.3762/bjnano.13.102

• Supporting Information File 2 shows the effects of hair length on roll-off speed and angle. The hair density of the nanofur is indirectly controlled via the sandblasting of the structured roller. The optimal roughness of the roller depends also on the actual polymer type. For polypropylene (PP), polyethylene

Biomimetic chitosan with biocomposite nanomaterials for bone tissue repair and regeneration

• Se-Kwon Kim,
• Sesha Subramanian Murugan,
• Pandurang Appana Dalavi,
• Sebanti Gupta,
• Sukumaran Anil,
• Gi Hun Seong and
• Jayachandran Venkatesan

Beilstein J. Nanotechnol. 2022, 13, 1051–1067, doi:10.3762/bjnano.13.92

• -hydroxybutyrate) composites generates a hydrophilic environment which promotes cell motility, adhesion, and protein adsorption. Furthermore, the mixture enhances the surface roughness of the composites, stimulating bone cells to attach to the surface [108]. The different characteristics of the 3D porous collagen

Temperature and chemical effects on the interfacial energy between a Ga–In–Sn eutectic liquid alloy and nanoscopic asperities

• Yujin Han,
• Pierre-Marie Thebault,
• Corentin Audes,
• Xuelin Wang,
• Haiwoong Park,
• Jian-Zhong Jiang and
• Arnaud Caron

Beilstein J. Nanotechnol. 2022, 13, 817–827, doi:10.3762/bjnano.13.72

• surface of the eutectic Ga–In–Sn melt with three AFM tips of different chemistries, namely SiOx, PtSi, and Au. Figure 2 also indicates the surface roughness Rq value for each topography image. We recorded the presented topography images in contact mode by setting and controlling the normal force to Fn = 2

• nN and the sliding velocity to vs = 4 µm/s. Depending on the tip chemistry, we determined different roughness values ranging from Rq = 4.48 nm with a gold tip to Rq = 10.13 nm with a platinum silicide tip. This dependence on the tip chemistry likely originates from different capillary interactions

Optimizing PMMA solutions to suppress contamination in the transfer of CVD graphene for batch production

• Chun-Da Liao,
• Andrea Capasso,
• Tiago Queirós,
• Telma Domingues,
• Fatima Cerqueira,
• Nicoleta Nicoara,
• Jérôme Borme,
• Paulo Freitas and
• Pedro Alpuim

Beilstein J. Nanotechnol. 2022, 13, 796–806, doi:10.3762/bjnano.13.70

• ) [28][33]. The crystal morphology appears very smooth and free of identifiable impurities, with an average surface roughness (Ra) of ca. 0.2 nm (Supporting Information File 1, Figure S3d). This value is one order of magnitude lower than that of graphene crystals transferred with C4 PMMA, which showed a

• surface roughness of ca. 2.8 nm. The low roughness obtained with B2 PMMA can be also related to a minimal occurrence of nanometer-scale PMMA residues. XPS was employed to analyze the graphene samples transferred using C4 and B2 PMMA (Figure 4). Figure 4a shows the chemical structure of the PMMA molecule

Effects of substrate stiffness on the viscoelasticity and migration of prostate cancer cells examined by atomic force microscopy

• Xiaoqiong Tang,
• Yan Zhang,
• Jiangbing Mao,
• Yuhua Wang,
• Zhenghong Zhang,
• Zhengchao Wang and
• Hongqin Yang

Beilstein J. Nanotechnol. 2022, 13, 560–569, doi:10.3762/bjnano.13.47

• for cell invasion [25][26]. Our results suggest that stiff substrates promote the protrusion of the leading edge of cancer cell membranes to guide cell motility. The average surface roughness of cells on extracellular environments with different stiffness is shown in Figure 3d. PC-3 cells showed a

• higher average surface roughness (Ra) on stiff substrates than on soft substrates, in contrast to HPV-PZ-7 cells, which did not exhibit this feature. Peak-to-valley ratio roughness (Rt) and root mean square surface roughness (Rq) also showed the same characteristics, see Supporting Information File 1

• , Figure S3c,d. Cell surface roughness is a quantitative measurement of the variability of cellular surface topography and serves as an indicator to assess the state of the cell (i.e., the greater the roughness, the greater the undulation of the cell surface topography [27]). It can be involved in many

Influence of thickness and morphology of MoS₂ on the performance of counter electrodes in dye-sensitized solar cells

• Lam Thuy Thi Mai,
• Hai Viet Le,
• Ngan Kim Thi Nguyen,
• Van La Tran Pham,
• Thu Anh Thi Nguyen,
• Nguyen Thanh Le Huynh and
• Hoang Thai Nguyen

Beilstein J. Nanotechnol. 2022, 13, 528–537, doi:10.3762/bjnano.13.44

• grids with a diameter of around 50 nm (see Figure 3e, insert). The roughness of the films was further studied by AFM. The film with the honeycomb-like structure showed the highest average roughness (Sa) and root mean square roughness (Sq) of 24.179 and 30.443 nm, respectively (see Supporting Information

Micro- and nanotechnology in biomedical engineering for cartilage tissue regeneration in osteoarthritis

• Zahra Nabizadeh,
• Mahmoud Nasrollahzadeh,
• Hamed Daemi,
• Mohamadreza Baghaban Eslaminejad,
• Ali Akbar Shabani,
• Mehdi Dadashpour,
• Majid Mirmohammadkhani and
• Davood Nasrabadi

Beilstein J. Nanotechnol. 2022, 13, 363–389, doi:10.3762/bjnano.13.31

• because they are not biodegradable and provide a more stable matrix in which osteoblasts can proliferate and deposit new ECM. The integration of CNTs into a polymer matrix would increase surface roughness and activate the mitogen-activated protein kinase (MAPK) pathway [128], which is responsible for

• regulating the osteogenic response of cells to surface roughness. In this regard, the fabrication of a CNT-incorporated PLGA nanocomposite has resulted in the enhanced surface roughness and increased attachment and proliferation of MC3T3-E1 osteoblasts [129]. In vitro osteogenesis analysis also showed a

• , and OH) and surface roughness to CNT, Antonioli et al. used oxygen plasma treatment and fabricated novel superhydrophilic VA–CTN films. This treatment could increase the wettability of the nanofilms to acquire appreciable cytocompatibility [134]. The chondrocytes expressed major chondrogenic markers