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Search for "synthesis methods" in Full Text gives 91 result(s) in Beilstein Journal of Nanotechnology.

In situ SU-8 silver nanocomposites

  • Søren V. Fischer,
  • Basil Uthuppu and
  • Mogens H. Jakobsen

Beilstein J. Nanotechnol. 2015, 6, 1661–1665, doi:10.3762/bjnano.6.168

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  • ]. Furthermore, it is difficult to obtain stable suspensions of preformed NPs in SU-8 without aggregation and phase separation. In situ synthesis methods where the particles are formed directly within the polymeric matrix from a precursor can circumvent this problem. Here, we report a fast and simple method for
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Letter
Published 30 Jul 2015

Using natural language processing techniques to inform research on nanotechnology

  • Nastassja A. Lewinski and
  • Bridget T. McInnes

Beilstein J. Nanotechnol. 2015, 6, 1439–1449, doi:10.3762/bjnano.6.149

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  • available online. TechPerceptor TechPerceptor is a text mining tool to conduct patent analysis and generate a patent map based on a subject–action–object (SAO) approach [26][27][28]. Their training corpus consisted of 136 patents and was initially analyzed for trends in carbon nanotube synthesis methods [26
  • reporting arc-discharge and laser vaporization synthesis methods [26]. Chemical vapor deposition (CVD) methods were also mentioned as being invented frequently. Top patenting companies included NEC, Samsung and Sony. Their dynamic tool revealed a possible patent vacuum of using low temperature or microwave
  • -based synthesis of single-walled carbon nanotubes [27]. Analyzing hot spots revealed changes in the type of synthesis method patented over time, with synthesis methods evolving from arc discharging in 1999–2000 to metal-catalyzed heat-treatment syntheses and CVD in 2003–2004, to arc discharge with
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Review
Published 01 Jul 2015

Growth and morphological analysis of segmented AuAg alloy nanowires created by pulsed electrodeposition in ion-track etched membranes

  • Ina Schubert,
  • Loic Burr,
  • Christina Trautmann and
  • Maria Eugenia Toimil-Molares

Beilstein J. Nanotechnol. 2015, 6, 1272–1280, doi:10.3762/bjnano.6.131

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  • including composition, dimension, and crystallinity. Therefore, to develop synthesis methods that guarantee a precise control of these properties is important. A powerful technique to synthesise nanowires with well-controlled morphological and crystallographic characteristics is the so-called template
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Published 08 Jun 2015

Palladium nanoparticles anchored to anatase TiO2 for enhanced surface plasmon resonance-stimulated, visible-light-driven photocatalytic activity

  • Kah Hon Leong,
  • Hong Ye Chu,
  • Shaliza Ibrahim and
  • Pichiah Saravanan

Beilstein J. Nanotechnol. 2015, 6, 428–437, doi:10.3762/bjnano.6.43

Graphical Abstract
  • photoactivity. There are several synthesis methods available for preparing plasmonic photocatalysts, namely photodeposition [3][30][31], hydrothermal [4][32][33][34], ion exchange [35][36], chemical reduction [25][37][38], physical vapour deposition [27][39][40], and deposition–precipitation [41][42][43]. Among
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Published 11 Feb 2015

Influence of size, shape and core–shell interface on surface plasmon resonance in Ag and Ag@MgO nanoparticle films deposited on Si/SiOx

  • Sergio D’Addato,
  • Daniele Pinotti,
  • Maria Chiara Spadaro,
  • Guido Paolicelli,
  • Vincenzo Grillo,
  • Sergio Valeri,
  • Luca Pasquali,
  • Luca Bergamini and
  • Stefano Corni

Beilstein J. Nanotechnol. 2015, 6, 404–413, doi:10.3762/bjnano.6.40

Graphical Abstract
  • nanoparticles (NPs) with a diameter of d = 3–10 nm were obtained by physical synthesis methods and deposited on Si with its native ultrathin oxide layer SiOx (Si/SiOx). Scanning electron microscopy and transmission electron microscopy (TEM) images of bare Ag NPs revealed the presence of small NP aggregates
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Published 09 Feb 2015

Synthesis of boron nitride nanotubes and their applications

  • Saban Kalay,
  • Zehra Yilmaz,
  • Ozlem Sen,
  • Melis Emanet,
  • Emine Kazanc and
  • Mustafa Çulha

Beilstein J. Nanotechnol. 2015, 6, 84–102, doi:10.3762/bjnano.6.9

Graphical Abstract
  • neutron capture therapy. In this review, BNNT synthesis methods and the surface modification strategies are first discussed, and then their toxicity and application studies are summarized. Finally, a perspective for the future use of these novel materials is discussed. Keywords: boron nitride nanotubes
  • ; chemical modifications; medical applications; synthesis methods; toxicity; Review Introduction Boron nitride nanotubes (BNNTs) are known as structural analogs of carbon nanotubes (CNTs) but with superior properties [1][2][3]. Although they have structural similarities, they significantly differ in their
  • ][29], ball milling [30][31][32][33][34][35], laser ablation [36][37][38], and low temperature methods [39][40][41] were reported. The CVD and ball milling methods are currently the two most widely used methods for the synthesis of BNNTs. In this review, the most important BNNT synthesis methods are
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Review
Published 08 Jan 2015

Hybrid spin-crossover nanostructures

  • Carlos M. Quintero,
  • Gautier Félix,
  • Iurii Suleimanov,
  • José Sánchez Costa,
  • Gábor Molnár,
  • Lionel Salmon,
  • William Nicolazzi and
  • Azzedine Bousseksou

Beilstein J. Nanotechnol. 2014, 5, 2230–2239, doi:10.3762/bjnano.5.232

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  • probe lies in the fact that the speed and temperature range (where the spin transition takes place) can be tuned by well-known chemical synthesis methods and without necessarily modifying the luminescent agent. This can be translated into a flexible design when it comes to sensitivity and working range
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Published 25 Nov 2014

Silica nanoparticles are less toxic to human lung cells when deposited at the air–liquid interface compared to conventional submerged exposure

  • Alicja Panas,
  • Andreas Comouth,
  • Harald Saathoff,
  • Thomas Leisner,
  • Marco Al-Rawi,
  • Michael Simon,
  • Gunnar Seemann,
  • Olaf Dössel,
  • Sonja Mülhopt,
  • Hanns-Rudolf Paur,
  • Susanne Fritsch-Decker,
  • Carsten Weiss and
  • Silvia Diabaté

Beilstein J. Nanotechnol. 2014, 5, 1590–1602, doi:10.3762/bjnano.5.171

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  • specific surface area is well known and has already been shown for many types of particles including amorphous silica particles [36]. Conclusion In this study two silica NPs produced by different synthesis methods were intensively characterized with regard to their properties in aerosols, deposition from
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Published 19 Sep 2014

Current state of laser synthesis of metal and alloy nanoparticles as ligand-free reference materials for nano-toxicological assays

  • Christoph Rehbock,
  • Jurij Jakobi,
  • Lisa Gamrad,
  • Selina van der Meer,
  • Daniela Tiedemann,
  • Ulrike Taylor,
  • Wilfried Kues,
  • Detlef Rath and
  • Stephan Barcikowski

Beilstein J. Nanotechnol. 2014, 5, 1523–1541, doi:10.3762/bjnano.5.165

Graphical Abstract
  • controlled independently while their uniquely high purity is retained. Hence, this article will highlight totally surfactant-free size control strategies for laser-fabricated nanoparticles and will comment on the stability of these particles in biological fluids. Additionally, laser-based synthesis methods
  • . This often favors element segregation and the formation of core shell structures in the resulting nanoparticles [137][138]. Laser-based synthesis methods have proven to be a veritable alternative to generate AuAg alloy nanoparticles with homogeneous elemental distributions even on a single particle
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Review
Published 12 Sep 2014

Nanoporous composites prepared by a combination of SBA-15 with Mg–Al mixed oxides. Water vapor sorption properties

  • Amaury Pérez-Verdejo,
  • Alvaro Sampieri,
  • Heriberto Pfeiffer,
  • Mayra Ruiz-Reyes,
  • Juana-Deisy Santamaría and
  • Geolar Fetter

Beilstein J. Nanotechnol. 2014, 5, 1226–1234, doi:10.3762/bjnano.5.136

Graphical Abstract
  • 2.03 (Table 1). This value is in agreement with its nominal composition (Mg/Al = 2). The composites prepared in post-synthesis methods showed a molar ratio of Mg/Al = 1.85 and 1.95, respectively. Such ratios are very close to the nominal composition of the calcined composites. Still, the (Mg–Al)/SBA
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Published 07 Aug 2014

Growth and characterization of CNT–TiO2 heterostructures

  • Yucheng Zhang,
  • Ivo Utke,
  • Johann Michler,
  • Gabriele Ilari,
  • Marta D. Rossell and
  • Rolf Erni

Beilstein J. Nanotechnol. 2014, 5, 946–955, doi:10.3762/bjnano.5.108

Graphical Abstract
  • the recent progress achieved in these areas is reviewed here. ALD growth of CNT–TiO2 Many methods have been developed to fabricate CNT–metal/metal oxide nanocomposites. For CNT–TiO2, the methods that are mostly adopted are sol–gel and hydrothermal deposition. A good summary of the synthesis methods
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Published 02 Jul 2014

Injection of ligand-free gold and silver nanoparticles into murine embryos does not impact pre-implantation development

  • Ulrike Taylor,
  • Wiebke Garrels,
  • Annette Barchanski,
  • Svea Peterson,
  • Laszlo Sajti,
  • Andrea Lucas-Hahn,
  • Lisa Gamrad,
  • Ulrich Baulain,
  • Sabine Klein,
  • Wilfried A. Kues,
  • Stephan Barcikowski and
  • Detlef Rath

Beilstein J. Nanotechnol. 2014, 5, 677–688, doi:10.3762/bjnano.5.80

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  • ions, which imply that their toxicity can be reduced by either adapting surface properties or choosing alternative synthesis methods, so that their use could be rendered more safely in a plethora of applications. Experimental Nanoparticle production and characterization The applied laser-based approach
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Published 21 May 2014

Encapsulation of nanoparticles into single-crystal ZnO nanorods and microrods

  • Jinzhang Liu,
  • Marco Notarianni,
  • Llew Rintoul and
  • Nunzio Motta

Beilstein J. Nanotechnol. 2014, 5, 485–493, doi:10.3762/bjnano.5.56

Graphical Abstract
  • synthesis methods and applications. ZnO is a multifunctional material with semiconducting, photonic, and piezoelectric properties. Potential applications of ZnO 1D nanostructures include gas sensor [1], transistor [2], light-emitting device [3], optical waveguide [4], nanolaser [5], and piezoelectric power
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Published 16 Apr 2014

Extracellular biosynthesis of gadolinium oxide (Gd2O3) nanoparticles, their biodistribution and bioconjugation with the chemically modified anticancer drug taxol

  • Shadab Ali Khan,
  • Sanjay Gambhir and
  • Absar Ahmad

Beilstein J. Nanotechnol. 2014, 5, 249–257, doi:10.3762/bjnano.5.27

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  • responsible for the tumor killing efficiency of Gd-NCT [8]. Gd-157 not only requires shorter neutron irradiation time but also has a large neutron capture cross section area than boron-10, so that it is an ideal substitute for boron-10. As far as synthesis methods for Gd2O3 nanoparticles are concerned, the
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Published 07 Mar 2014

Synthesis and catalytic applications of combined zeolitic/mesoporous materials

  • Jarian Vernimmen,
  • Vera Meynen and
  • Pegie Cool

Beilstein J. Nanotechnol. 2011, 2, 785–801, doi:10.3762/bjnano.2.87

Graphical Abstract
  • section, the synthesis methods and formation mechanisms of the combined zeolitic/mesoporous materials are described. In addition, a thorough evaluation of the different synthesis strategies leading towards combined zeolitic/mesoporous materials is carried out, in which their advantages and disadvantages
  • , such as nuclear track imprinting [63], but since their use is not very widespread, they will not be dealt with here. The synthesis methods can be roughly divided into three different classes, namely postsynthetic, templating and nontemplating approaches. In the postsynthetic approach, a zeolite or
  • with organosilane surfactants and postsynthetic routes). All synthesis methods have their advantages and disadvantages, meaning that there is no obviously superior synthesis strategy. Therefore, the applied synthesis approach should depend on the final application, the desired properties of the
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Published 30 Nov 2011

Review and outlook: from single nanoparticles to self-assembled monolayers and granular GMR sensors

  • Alexander Weddemann,
  • Inga Ennen,
  • Anna Regtmeier,
  • Camelia Albon,
  • Annalena Wolff,
  • Katrin Eckstädt,
  • Nadine Mill,
  • Michael K.-H. Peter,
  • Jochen Mattay,
  • Carolin Plattner,
  • Norbert Sewald and
  • Andreas Hütten

Beilstein J. Nanotechnol. 2010, 1, 75–93, doi:10.3762/bjnano.1.10

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  • mentioned in the preliminary section, bottom-up synthesis methods are well suited for these requirements. In addition, particle size distributions can be further refined via sedimentation or by magnetic separation subsequent to chemical synthesis [15]. 2.1 Driving forces to self-assemblies The organization
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Published 22 Nov 2010
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