Properties of tin oxide films grown by atomic layer deposition from tin tetraiodide and ozone

• Kristjan Kalam,
• Peeter Ritslaid,
• Tanel Käämbre,
• Aile Tamm and
• Kaupo Kukli

Beilstein J. Nanotechnol. 2023, 14, 1085–1092, doi:10.3762/bjnano.14.89

• film thickness profile along the gas flow direction. Analysis of oxygen and iodine contents in the films revealed that above a substrate temperature of 200 °C, the oxygen content remained stable. At temperatures below 200 °C, the oxygen content was significantly higher than that expected from a

Recognition mechanisms of hemoglobin particles by monocytes – CD163 may just be one

• Jonathan-Gabriel Nimz,
• Pichayut Rerkshanandana,
• Chiraphat Kloypan,
• Ulrich Kalus,
• Saranya Chaiwaree,
• Axel Pruß,
• Radostina Georgieva,
• Yu Xiong and
• Hans Bäumler

Beilstein J. Nanotechnol. 2023, 14, 1028–1040, doi:10.3762/bjnano.14.85

• dependence of HbMP uptake on these receptors. Table 2 gives an overview of the samples of indirect phagocytosis test no. 2; the incubation time with HbMPs was 30 min. All samples were analyzed by flow cytometry. Leucocytes were identified by DNA staining with propidium iodide (PI) or diamidinophenylindole

• for 10 min at 37 °C right away. An MFI value in flow cytometry close to the one of the reference sample showed that neither one of the antibodies we used had an effect on the uptake of FITC-labeled E. coli bacteria (Figure 4). Discussion Indirect phagocytosis assays were carried out with whole blood

Nanoarchitectonics of photothermal materials to enhance the sensitivity of lateral flow assays

• Elangovan Sarathkumar,
• Rajasekharan S. Anjana and
• Ramapurath S. Jayasree

Beilstein J. Nanotechnol. 2023, 14, 988–1003, doi:10.3762/bjnano.14.82

• Elangovan Sarathkumar Rajasekharan S. Anjana Ramapurath S. Jayasree Division of Biophotonics and Imaging, Biomedical Technology Wing, Sree Chitra Tirunal Institute for Medical Sciences and Technology, Poojappura, Thiruvananthapuram-695012, Kerala, India 10.3762/bjnano.14.82 Abstract Lateral flow

• advances in photothermal LFAs and their application in detecting analytes. Keywords: lateral flow assay; nanoarchitectonics; photothermal; photothermal nanomaterials; signal amplification; Introduction Lateral flow assays (LFAs) are a versatile and convenient point-of-care testing (POCT) technique used

• different parts, namely sample pad, conjugate pad, nitrocellulose membrane, and adsorbent pad, maintaining a smooth flow of reagents through the LFA membrane. In the presence of a sample, the analyte initially reacts with affinity molecules, commonly antibodies linked with tracers such as gold nanoparticles

Fragmentation of metal(II) bis(acetylacetonate) complexes induced by slow electrons

• Janina Kopyra and
• Hassan Abdoul-Carime

Beilstein J. Nanotechnol. 2023, 14, 980–987, doi:10.3762/bjnano.14.81

• scale was calibrated using a flow of SF6 gas through the oven that produced the well-known SF6− resonance near 0 eV. The measurements were performed without the presence of the calibration gas, avoiding potentially unwanted reactions such as dissociative electron transfer with the investigated molecules

Upscaling the urea method synthesis of CoAl layered double hydroxides

• Camilo Jaramillo-Hernández,
• Víctor Oestreicher,
• Martín Mizrahi and
• Gonzalo Abellán

Beilstein J. Nanotechnol. 2023, 14, 927–938, doi:10.3762/bjnano.14.76

• co-precipitation, and mechanochemical approaches [27]. Although these methods can produce materials on a large scale, they are very limited in providing materials with controlled morphology, size, or crystallinity [42]. This issue can be partially solved using continuous flow techniques [43][44]. Yet

• (Table 1). Supporting Information File 1, Table S6 compares the obtained STY values with those ones from other synthesis approaches such as co-precipitation and hydrothermal [39][40][41][65][66][67][68][69], mechanochemistry [27], and continuous flow methods [43][44]. After the limits for the scale-up of

Antibody-conjugated nanoparticles for target-specific drug delivery of chemotherapeutics

• Mamta Kumari,
• Amitabha Acharya and
• Praveen Thaggikuppe Krishnamurthy

Beilstein J. Nanotechnol. 2023, 14, 912–926, doi:10.3762/bjnano.14.75

• antigen binding ability. Improper antibody conjugation influences antigen binding affinity and specificity. Once injected into the body, the ACNPs face both physical and biological barriers (such as diffusion, flow and shear forces, aggregation, protein adsorption, phagocytic sequestration, and clearance

Nanostructured lipid carriers containing benznidazole: physicochemical, biopharmaceutical and cellular in vitro studies

• Giuliana Muraca,
• María Esperanza Ruiz,
• Rocío C. Gambaro,
• Sebastián Scioli-Montoto,
• María Laura Sbaraglini,
• Gisel Padula,
• José Sebastián Cisneros,
• Cecilia Yamil Chain,
• Vera A. Álvarez,
• Cristián Huck-Iriart,
• Guillermo R. Castro,
• María Belén Piñero,
• Matias Ildebrando Marchetto,
• Catalina Alba Soto,
• Germán A. Islan and
• Alan Talevi

Beilstein J. Nanotechnol. 2023, 14, 804–818, doi:10.3762/bjnano.14.66

• the Vero cell line by flow cytometry, where the percentage of dead cells labeled with propidium iodide (PI, Supporting Information File 1, Figure S2) was measured. Neither the drug-loaded or unloaded NLCs elicited significant toxicity in Vero cells. As it is common to parenterally administer

• . A Platinum EPS C8 (150 mm × 4.6 mm, 5 μm, GraceTM, Columbia, MD, USA) column was used; the mobile phase consisted of a mixture of methanol and 0.02% phosphoric acid solution (60:40) for a final pH of 2.5. The system was operated isocratically at a 1.0 mL/min flow rate and the detection was performed

• spectrophotometer, Thermo Fisher Scientific) at 550 nm. The assays were performed in triplicate. Cell toxicity assay on Vero cells Cell viability was analyzed by flow cytometry as described in the “In vitro anti-amastigote effect” section after adding PI to obtain the percentage of dead cells following the

Silver-based SERS substrates fabricated using a 3D printed microfluidic device

• Phommachith Sonexai,
• Minh Van Nguyen,
• Bui The Huy and
• Yong-Ill Lee

Beilstein J. Nanotechnol. 2023, 14, 793–803, doi:10.3762/bjnano.14.65

• [15][16][17]. Two types of microfluidic devices are commonly used, namely droplet-based and continuous devices. Continuous microfluidic devices have several disadvantages when applied for chemical syntheses, such as laminar flow formation due to the low Reynolds number of fluids, which leads to a lack

• reactants in segmented flow and oil in continuous flow. They can control the reaction rates by mass transfer through convection and diffusion [20][21]. Furthermore, droplet-based microfluidic devices are frequently utilized to synthesize complex materials of uniform size, as each droplet can function as a

• method limits the amount of precursor chemicals and enables the sequential flow of droplets, resulting in silver nanoparticles of uniform shape and size. We investigated the effects of different synthesis conditions on the size distribution, dispersity, and LSPR wavelength of the silver nanoparticles

Silver nanoparticles loaded on lactose/alginate: in situ synthesis, catalytic degradation, and pH-dependent antibacterial activity

• Nguyen Thi Thanh Tu,
• T. Lan-Anh Vo,
• T. Thu-Trang Ho,
• Kim-Phuong T. Dang,
• Van-Dung Le,
• Phan Nhat Minh,
• Chi-Hien Dang,
• Vinh-Thien Tran,
• Van-Su Dang,
• Tran Thi Kim Chi,
• Hieu Vu-Quang,
• Radek Fajgar,
• Thi-Lan-Huong Nguyen,
• Van-Dat Doan and
• Thanh-Danh Nguyen

Beilstein J. Nanotechnol. 2023, 14, 781–792, doi:10.3762/bjnano.14.64

• blank composite and the nanocomposites in an air flow of 20 mL/min at a heating rate of 10 °C/min. The TGA curve of AgNPs@Lac/Alg closely resembles that of the blank composite. Between 37 and 200 °C, the nanocomposite AgNPs@Lac/Alg-0.3 exhibited a significantly higher thermal loss (28%) compared to the

In situ magnesiothermic reduction synthesis of a Ge@C composite for high-performance lithium-ion batterie anodes

• Ha Tran Huu,
• Ngoc Phi Nguyen,
• Vuong Hoang Ngo,
• Huy Hoang Luc,
• Minh Kha Le,
• Minh Thu Nguyen,
• My Loan Phung Le,
• Hye Rim Kim,
• In Young Kim,
• Sung Jin Kim,
• Van Man Tran and
• Vien Vo

Beilstein J. Nanotechnol. 2023, 14, 751–761, doi:10.3762/bjnano.14.62

• , then placed in a ceramic crucible and heated to 800 °C for 5 h under argon gas flow with a heating rate of 10 °C·min−1. The obtained solid was washed with potassium hydroxide solution (KOH 20%) at 70 °C for 2 h, then leached with 2 M HCl at 70 °C for 15 h and washed several times with de-ionized (DI

• mixture of germanium dioxide, magnesium, and activated carbon at a mass ratio of 5:4:10, was ground well and transferred into a ceramic crucible. The solid was heated to 750 °C under Ar gas flow for 3 h. The obtained powder was rinsed with 1 M HCl to remove by-products. The sample, obtained after rinsing

• and transferred to a ceramic crucible. The mixture was heated at 750 °C in argon gas flow for 3 h. The obtained solid was re-ground and denoted as Ge/C-SS750. Material characterization X-ray diffraction measurements (XRD, Bruker D8 Advance with Cu Kα radiation (λ = 1.5406 Å) at 40 kV and 40 mA) were

Control of morphology and crystallinity of CNTs in flame synthesis with one-dimensional reaction zone

• Muhammad Hilmi Ibrahim,
• Norikhwan Hamzah,
• Mohd Zamri Mohd Yusop,
• Ni Luh Wulan Septiani and
• Mohd Fairus Mohd Yasin

Beilstein J. Nanotechnol. 2023, 14, 741–750, doi:10.3762/bjnano.14.61

• Muhammad Hilmi Ibrahim Norikhwan Hamzah Mohd Zamri Mohd Yusop Ni Luh Wulan Septiani Mohd Fairus Mohd Yasin Department of Thermo-Fluids, Faculty of Mechanical Engineering, Universiti Teknologi Malaysia, 81310 Johor Bahru, Malaysia High Speed Reacting Flow Laboratory (HiREF), Universiti Teknologi

• flame is conducted regarding the morphology and crystallinity of the as-grown nanotubes. The premixed burner configuration created a flame that is stabilized through axisymmetric stagnation flow through sintered metal with one-dimensional geometry, different from a conventional co-flow flame. The

• ratio was also shown in another study by Hamzah et al. [13], utilizing a methane diffusion flame with different air flow rates. This study aims to synthesize CNTs on nickel wire through methane combustion in a one-dimensional premixed flat flame. The resulting CNT morphology and crystallinity will be

Nanoarchitectonics for advanced applications in energy, environment and biology: Method for everything in materials science

• Katsuhiko Ariga

Beilstein J. Nanotechnol. 2023, 14, 738–740, doi:10.3762/bjnano.14.60

• instance. Katsuhiko Ariga Tsukuba, June 2023 Historical flow to bridge nanotechnology amd materials science.

Cross-sectional Kelvin probe force microscopy on III–V epitaxial multilayer stacks: challenges and perspectives

• Mattia da Lisca,
• José Alvarez,
• James P. Connolly,
• Nicolas Vaissiere,
• Karim Mekhazni,
• Jean Decobert and
• Jean-Paul Kleider

Beilstein J. Nanotechnol. 2023, 14, 725–737, doi:10.3762/bjnano.14.59

• ), and arsine (AsH3) were the source materials, with hydrogen (H2) as a carrier gas. Diethylzinc (DEZn) was used as a source of Zn for p-type doping the InP:Zn and the phosphorus-based quaternary (GaInAsP:Zn) and GaInAs:Zn layers. The precursor flow was varied to cover a doping level range from 1 × 1018

• ]. As illustrated in Figure 8, in the case of downward surface band bending in an p-type semiconductor, photogenerated holes are repelled from the surface, while photogenerated electrons flow in the direction of the surface, balancing the positive charges corresponding to empty donor-type surface states

• . This results in a reduction of surface band bending and a decrease of surface potential, that is, a negative SPV. Conversely, in the case of upward surface band bending in an n-type semiconductor, photogenerated electrons are repelled from the surface, while photogenerated holes flow towards the

Current-induced mechanical torque in chiral molecular rotors

• Richard Korytár and
• Ferdinand Evers

Beilstein J. Nanotechnol. 2023, 14, 711–721, doi:10.3762/bjnano.14.57

• qualitative description of the current-induced mechanical torque within a toy model framework. We consider a classical model of the molecular rotor where the molecule is modeled as a one-dimensional curve (“molecular wire”) that guides the flow of the charge carriers (see Figure 1 (left) for illustration

• fulfilled. First, the rotor’s velocity must be attenuated for the rotor to settle in the nearest potential minimum. Second, the current must flow in controlled short pulses. The optimal parameter regime can be sought using the EOM (Equation 22 and Equation 23), which is beyond the scope of the present work

Humidity-dependent electrical performance of CuO nanowire networks studied by electrochemical impedance spectroscopy

• Jelena Kosmaca,
• Juris Katkevics,
• Jana Andzane,
• Raitis Sondors,
• Liga Jasulaneca,
• Raimonds Meija,
• Kiryl Niherysh,
• Yelyzaveta Rublova and
• Donats Erts

Beilstein J. Nanotechnol. 2023, 14, 683–691, doi:10.3762/bjnano.14.54

• frequencies below 1 Hz, representing the ability of the sample to impede the flow of current between cathodic and anodic areas, equal to ca. 1 × 1010 Ω. When the RH is higher than 50%, the impedance modules at low f decrease by up to three orders of magnitude, and the log Z curves show a linear dependence on

• electron microscopy (SEM, Hitachi S4800) and atomic force microscopy (AFM, Asylum Research MFP-3D). Electrochemical impedance measurements were performed under various atmospheric conditions in a custom-made system described elsewhere [28]. The main system parameters were RH from 4% to 97%, gas flow from

Investigations on the optical forces from three mainstream optical resonances in all-dielectric nanostructure arrays

• Guangdong Wang and
• Zhanghua Han

Beilstein J. Nanotechnol. 2023, 14, 674–682, doi:10.3762/bjnano.14.53

• continuum (BIC)) which are current in focus nanophotonics research topics, all-dielectric nanostructures have proved themselves to be a good platform for light–matter interactions and an advantageous alternative to their plasmonic counterparts. A TD resonance is produced by the flow of electric currents on

Titania nanoparticles for photocatalytic degradation of ethanol under simulated solar light

• Evghenii Goncearenco,
• Iuliana P. Morjan,
• Claudiu Teodor Fleaca,
• Florian Dumitrache,
• Elena Dutu,
• Monica Scarisoreanu,
• Valentin Serban Teodorescu,
• Alexandra Sandulescu,
• Crina Anastasescu and
• Ioan Balint

Beilstein J. Nanotechnol. 2023, 14, 616–630, doi:10.3762/bjnano.14.51

• productivity, which are in some cases extremely low compared to a continuous flow method such as laser pyrolysis which, in the case of the studied powders, allows for a productivity of 1 g/h with the possibility of upscaling to an industrial level by increasing the reaction area. Another point is to find the

• is TO-250-a, that is, the sample synthesized at the lowest pressure and in the presence of the highest C2H4 sensitizer flow (120 sccm). Here, the rutile crystal structure is the main constituent. The crystallite size increases for both phases from 14 nm and 11 nm to 22 nm for anatase and rutile

• crystalline phase and rutile being a minor fraction. An exception to this is the sample synthesized at the lowest pressure without supplementary air flow. Two series of samples were tested in ethanol photodegradation experiments, observing that all samples from series “a” have a higher photocatalytic activity

Suspension feeding in Copepoda (Crustacea) – a numerical model of setae acting in concert

• Alexander E. Filippov,
• Wencke Krings and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2023, 14, 603–615, doi:10.3762/bjnano.14.50

• described as filtering or sieving with, for example, setae, cilia, or mucous nets, and is present in form of passive or active suspension feeding. Passive feeders rely on external water currents that bring food particles to the filtering structures and active feeders create a feeding flow by pumping systems

• . The second mechanism involves structures manipulating the water flow (e.g., setae and tentacles) that redirect the food particles and lead them to specialized structures that contact and capture them. A good example for the latter mechanism are the filtering setae of crustaceans (for in-depth reviews

• adhesive forces to retain particles. In contrast to organisms, which collect particles at the nano- to millimeter scale, most industrial cross-flow filtration systems can capture material only in more limited size ranges, highlighting the necessity to investigate particle retention in biological systems

Thermal transport in kinked nanowires through simulation

• Alexander N. Robillard,
• Graham W. Gibson and
• Ralf Meyer

Beilstein J. Nanotechnol. 2023, 14, 586–602, doi:10.3762/bjnano.14.49

• phonon reflection specularity on the heat flux is also examined. It is found that, in general, the flow of heat through systems simulated through phonon Monte Carlo methods is concentrated into a channel smaller than the wire dimensions, while this is not the case in the classical solutions of the

• increase with increasing kink angle. With the scattering rate becoming large, and consequently the mean free path of phonons becoming short, the effect of scattering off surfaces becomes negligible, and the heat flow becomes more diffusive (it is also reduced in magnitude due to overall reduced transport

• small “shortcuts” that the heat flow can use to reduce its effective path length, much like a race-car driver taking the inside corners of a series of curves. This corner cutting has been seen and discussed previously in the context of right-angled serpentine nanowires [20][22][30]. To reiterate a point

Carbon nanotube-cellulose ink for rapid solvent identification

• Tiago Amarante,
• Thiago H. R. Cunha,
• Claudio Laudares,
• Ana P. M. Barboza,
• Ana Carolina dos Santos,
• Cíntia L. Pereira,
• Vinicius Ornelas,
• Bernardo R. A. Neves,
• André S. Ferlauto and
• Rodrigo G. Lacerda

Beilstein J. Nanotechnol. 2023, 14, 535–543, doi:10.3762/bjnano.14.44

• two important properties of the liquids, namely dielectric constant and vapor pressure, on the transduction of the MFC-MWCNT sensors. These results were corroborated by independent heat flow measurements (thermogravimetric analysis). The proposed MFC-MWCNT sensor platform may help paving the way to

• contact mode. AC160TS silicon cantilevers from Olympus with a typical spring constant of k ≈ 46 N/m, a nominal radius of curvature of r ≈ 7 nm, and a resonant frequency of ω0 ≈ 300 kHz were employed. Heat flow and weight changes of selected solvents were determined by thermogravimetric analysis (TGA

• produced by the impinging liquid drops over the heated surface of the transducer. The temperature change and the heat flow produced by the liquid as it gets in contact with the heated surface were estimated by dripping a liquid (of about 6.5 µL) into an empty crucible kept at 55 °C inside a

Nanoarchitectonics to entrap living cells in silica-based systems: encapsulations with yolk–shell and sepiolite nanomaterials

• Celia Martín-Morales,
• Jorge Fernández-Méndez,
• Pilar Aranda and
• Eduardo Ruiz-Hitzky

Beilstein J. Nanotechnol. 2023, 14, 522–534, doi:10.3762/bjnano.14.43

• , fresh yeast). All employed materials and equipment have been sterilized by heating to 120 °C for 25 min and subsequent cool down to room temperature within the autoclave chamber. All culture handling operations have been performed within a sterile laminar flow hood, which before and after its usage had

A mid-infrared focusing grating coupler with a single circular arc element based on germanium on silicon

• Xiaojun Zhu,
• Shuai Li,
• Ang Sun,
• Yongquan Pan,
• Wen Liu,
• Yue Wu,
• Guoan Zhang and
• Yuechun Shi

Beilstein J. Nanotechnol. 2023, 14, 478–484, doi:10.3762/bjnano.14.38

• membrane Ge waveguide [1]. The maximum coupling efficiency was −11 dB at the focusing SWG’s center wavelength of 2.37 μm. The high coupling efficiency was obtained experimentally. However, the fabrication flow of the suspended membrane Ge waveguide with focusing SWGs greatly increased the complexity of the

The steep road to nonviral nanomedicines: Frequent challenges and culprits in designing nanoparticles for gene therapy

• Yao Yao,
• Yeongun Ko,
• Grant Grasman,
• Jeffery E. Raymond and
• Joerg Lahann

Beilstein J. Nanotechnol. 2023, 14, 351–361, doi:10.3762/bjnano.14.30

• are assessed with the use of fluorescent-labeling carriers and the expression of fluorescent proteins (e.g., enhanced green fluorescent protein). Both of which are typically assessed by widefield fluorescent microscopy/confocal microscopy (referred to as “imaging”) and/or flow cytometry (Table 1

• after image capture (26%, Figure 1a2). Flow cytometry, also a fluorescence-based method, is an alternate assessment of uptake and transfection. It is commonly used for high-throughput cell studies and is known for both rapid data acquisition and large data sets [17]. Flow cytometry can generate large

• papers, Figure 1b). Despite the robust data it can provide, flow cytometry counts the total number of cells associated with NPs and cannot distinguish internalized cargo from surface-bound NPs [1][17]. To precisely quantify internalization, a secondary method is required that can differentiate between

Overview of mechanism and consequences of endothelial leakiness caused by metal and polymeric nanoparticles

• Magdalena Lasak and
• Karol Ciepluch

Beilstein J. Nanotechnol. 2023, 14, 329–338, doi:10.3762/bjnano.14.28

• vasoconstrictions factors (e.g., thromboxane, prostaglandin, and endothelin-1), regulating vessel tension and, thus, blood flow and pressure [4][5][6][7][8]. The endothelium also produces mediators involved in angiogenic processes (e.g., vascular endothelial growth factor (VEGF) and fibroblast growth factor (FGF

• nutrient molecules to NPs could change the toxicity of NPs (NP protein corona), and the physiological conditions, such as blood flow and physiological stretch, will also play a role [37][38][39]. NanoEL mechanism Adherens junctions between endothelial cells are maintained by a complex set of proteins

• EPR effect, but transport strictly depends on the stage of the tumor. Hence, the use of the EPR effect may be justified only in the case of mature tumors. Moreover, leaky vessels and heterogeneous blood flow limit its use for therapeutic purposes. By contrast, NanoEL is a mechanism completely

Biocatalytic synthesis and ordered self-assembly of silica nanoparticles via a silica-binding peptide

• Mustafa Gungormus

Beilstein J. Nanotechnol. 2023, 14, 280–290, doi:10.3762/bjnano.14.25

• molecular crowding-like effects, preventing efficient assembly of the particles. Therefore, tailoring intermolecular interactions between nanoparticles by modifying the particle surfaces or through external influences such as temperature, pH value, templates, and magnetic or flow fields, is important to

• –MS analyses were done with a fused silica capillary column a (Restek 14623, Thermo Fischer Scientific Inc, Waltham, MA, USA), 150 °C injection temperature, 250 °C detection temperature, 1 µL injection volume, and 1 mL/min He flow rate. Dionex Chromeleon 7.2 software (Thermo Fischer Scientific Inc