Electrochemical nanostructured CuBTC/FeBTC MOF composite sensor for enrofloxacin detection

• Thi Kim Ngan Nguyen,
• Tien Dat Doan,
• Huy Hieu Luu,
• Hoang Anh Nguyen,
• Thi Thu Ha Vu,
• Quang Hai Tran,
• Ha Tran Nguyen,
• Thanh Binh Dang,
• Thi Hai Yen Pham and
• Mai Ha Hoang

Beilstein J. Nanotechnol. 2024, 15, 1522–1535, doi:10.3762/bjnano.15.120

• /bjnano.15.120 Abstract A novel electrochemical sensor for the detection of enrofloxacin (ENR) in aqueous solutions has been developed using a carbon paste electrode modified with a mixture of metal-organic frameworks (MOFs) of CuBTC and FeBTC. These MOFs were successfully synthesized via a solvothermal

• analysing tap and lake water samples, with recovery rates ranging from 90.2% to 121.3%. Keywords: CuBTC; electrochemical sensor; enrofloxacin; FeBTC; metal-organic framework; Introduction Enrofloxacin (ENR) is a quinolinemonocarboxylic acid and a third-generation fluoroquinolone. This antibiotic is

• material for electrochemical sensor applications because of their high loading quantity and surface area, defined structures, and chemical stability [19][20]. Since the first report by Yaghi and his group in 1994 [21], MOFs have attracted great attention. The first publication related to a fluorescent

A graphene quantum dots–glassy carbon electrode-based electrochemical sensor for monitoring malathion

• Sanju Tanwar,
• Aditi Sharma and
• Dhirendra Mathur

Beilstein J. Nanotechnol. 2023, 14, 701–710, doi:10.3762/bjnano.14.56

• diffraction were used to characterize the morphological and structural properties of GQDs. An electrochemical sensor was developed by drop casting GQDs on a glassy carbon electrode (GCE). The sensor detects the organophosphate pesticide malathion in a selective and sensitive manner. Using cyclic voltammetry

• spectroscopy; electrochemical sensor; graphene quantum dots; malathion; Introduction Global population growth makes food production more challenging, and pesticides are therefore used in agriculture in greater quantities than in the past to maintain and increase crop yields [1][2]. Pesticides containing

• on a biosensor platform consisting of graphene quantum dots functionalized with acetylcholinesterase and choline oxidase for the detection of the organophosphate pesticide dichlorvos [25]. In 2018, Qian Liu et al. developed a photo-electrochemical sensor with nitrogen-functionalized graphene quantum

Metal-organic framework-based nanomaterials as opto-electrochemical sensors for the detection of antibiotics and hormones: A review

• Akeem Adeyemi Oladipo,
• Saba Derakhshan Oskouei and
• Mustafa Gazi

Beilstein J. Nanotechnol. 2023, 14, 631–673, doi:10.3762/bjnano.14.52

• , high-performance MOFs as commercially viable next-generation opto-electrochemical sensor materials for the detection and monitoring of diverse analytes are discussed. Keywords: antibiotics sensing; endocrinal disorders; fluorescent sensor; hormones sensors; luminescent sensor; MOF nanohybrids

• electrical signals that may be easily identified and shown by electrical equipment. Electrochemical sensor-based techniques can be classified as conductometric, potentiometric, voltammetric, or amperometric, depending on the electrical signal that needs to be measured [56]. Conductivity is measured using

• nanocomposites. Because of their large surface area, ordered structure, tunable physico-chemical properties, and good absorbability, MOFs exhibit high potential among the various materials used for electrochemical sensor electrodes [63]. Strong interactions between the functional groups of MOFs and the target

A nonenzymatic reduced graphene oxide-based nanosensor for parathion

• Sarani Sen,
• Anurag Roy,
• Ambarish Sanyal and
• Parukuttyamma Sujatha Devi

Beilstein J. Nanotechnol. 2022, 13, 730–744, doi:10.3762/bjnano.13.65

• and straightforward responsive nature, high sensitivity, and selectivity leading to real-time detection [7]. A combination of a receptor, an analyte, and a transducer is made up to obtain an electrochemical sensor, in which the surface of the electrode induces redox characteristics via selective

A non-enzymatic electrochemical hydrogen peroxide sensor based on copper oxide nanostructures

• Irena Mihailova,
• Vjaceslavs Gerbreders,
• Marina Krasovska,
• Eriks Sledevskis,
• Valdis Mizers,
• Andrejs Bulanovs and
• Andrejs Ogurcovs

Beilstein J. Nanotechnol. 2022, 13, 424–436, doi:10.3762/bjnano.13.35

• qualitative detection of H2O2 in real samples, as well as for the quantitative determination of its concentration. Keywords: copper oxide; electrochemical sensor; hydrogen peroxide; nanostructures; Introduction Hydrogen peroxide, a strong oxidant and an essential intermediate product in many biomedical

• . 1.1.1.2/16/I/001, research application number 1.1.1.2/VIAA/4/20/743 "Development of nanomaterial-based electrochemical sensor for detection of hydrogen peroxide".

Morphology-driven gas sensing by fabricated fractals: A review

• Vishal Kamathe and
• Rupali Nagar

Beilstein J. Nanotechnol. 2021, 12, 1187–1208, doi:10.3762/bjnano.12.88

• 2–3 µm length) by a hydrothermal method and calcined the fabricated nanostructure precursors in air [84]. Figure 23a–f shows SEM and TEM micrographs with selected-area electron diffraction (SAED) patterns of the Co3O4 nanostructures. Hydrogen peroxide (H2O2) was detected by an electrochemical sensor

Ultrasensitive detection of cadmium ions using a microcantilever-based piezoresistive sensor for groundwater

• Dinesh Rotake,
• Anand Darji and
• Nitin Kale

Beilstein J. Nanotechnol. 2020, 11, 1242–1253, doi:10.3762/bjnano.11.108

• , expensive, and not suitable for on-site determination. The calorimetric approach proposed by [34][35][36][37] is free from these problems but not capable of differentiating between two nearby ranges and the LOD is also on the higher side. The electrochemical sensor described in [38] is a good approach, but

ZnO-nanostructure-based electrochemical sensor: Effect of nanostructure morphology on the sensing of heavy metal ions

• Marina Krasovska,
• Vjaceslavs Gerbreders,
• Irena Mihailova,
• Andrejs Ogurcovs,
• Eriks Sledevskis,
• Andrejs Gerbreders and
• Pavels Sarajevs

Beilstein J. Nanotechnol. 2018, 9, 2421–2431, doi:10.3762/bjnano.9.227

• electrochemical sensor of heavy metal ions. In this work, using the hydrothermal method, nanostructures of ZnO were synthesized in four different morphologies: nanorods (NRs), nanoneedles (NNs), nanotubes (NTs) and nanoplates (NPs). The samples described in this article were obtained using a preparation protocol

• were carried out using these nanostructured ZnO coatings on the working electrodes using aqueous solutions of Pb(NO3)2 and Cd(NO3)2 as analytes with different concentrations. Experimental Design and fabrication of the ZnO nanostructure-based electrochemical sensor Three morphologies of well-aligned one

Synthesis of hafnium nanoparticles and hafnium nanoparticle films by gas condensation and energetic deposition

• Irini Michelakaki,
• Nikos Boukos,
• Dimitrios A. Dragatogiannis,
• Spyros Stathopoulos,
• Costas A. Charitidis and
• Dimitris Tsoukalas

Beilstein J. Nanotechnol. 2018, 9, 1868–1880, doi:10.3762/bjnano.9.179

• demonstrate high catalytic activity during hydrogenation of levulinic acid [17], nickel NPs, which find application as electrochemical sensor [18], and cobalt NPs, which exhibit high magnetic anisotropy [19]. Recently, we have reported that hcp hafnium nanoparticles fabricated by inert-gas condensation, when

Voltammetric determination of polyphenolic content in pomegranate juice using a poly(gallic acid)/multiwalled carbon nanotube modified electrode

• Refat Abdel-Hamid and
• Emad F. Newair

Beilstein J. Nanotechnol. 2016, 7, 1104–1112, doi:10.3762/bjnano.7.103

• /MWCNT/GCE) electrochemical sensor was prepared for direct determination of the total phenolic content (TPC) as gallic acid equivalent. The GCE working electrode was electrochemically modified and characterized using scanning electron microscope (SEM), cyclic voltammetry (CV), chronoamperometry and

• pomegranate juice without interference of ascorbic acid, fructose, potassium nitrate and barbituric acid. The obtained data were compared with the standard Folin–Ciocalteu spectrophotometric results. Keywords: electrochemical sensor; gallic acid; multiwalled carbon nanotubes; pomegranate juice; total

• optimal test conditions of GA were carefully investigated on a sensor based on chitosan/fFe2O3/reduced graphene oxide/GCE. Under optimal conditions, the detection limit was estimated to be 1.5 × 10−7 M [4]. An electrochemical sensor coupled with an effective flow-injection amperometric system was

Electrochemical behavior of polypyrrol/AuNP composites deposited by different electrochemical methods: sensing properties towards catechol

• Celia García-Hernández,
• Cristina García-Cabezón,
• Cristina Medina-Plaza,
• Fernando Martín-Pedrosa,
• Yolanda Blanco,
• José Antonio de Saja and
• María Luz Rodríguez-Méndez

Beilstein J. Nanotechnol. 2015, 6, 2052–2061, doi:10.3762/bjnano.6.209

• electrochemical sensor, the Ppy/AuNp deposited on platinum exhibited a strong electrocatalytic activity towards the oxidation of catechol. The effect was higher in films obtained by CP than in films obtained by chronoamperometry (CA). The influence of the method used to introduce the AuNPs (trapping or

• stainless steel, caused by pitting process can be avoided by using phosphate buffer as supporting electrolyte. As an electrochemical sensor, the Ppy/AuNP deposited on platinum exhibited important electrocatalytic activity towards the oxidation of catechol. The effect was higher in films obtained by CP than