Effect of repeating hydrothermal growth processes and rapid thermal annealing on CuO thin film properties

• Monika Ozga,
• Eunika Zielony,
• Aleksandra Wierzbicka,
• Anna Wolska,
• Marcin Klepka,
• Marek Godlewski,
• Bogdan J. Kowalski and
• Bartłomiej S. Witkowski

Beilstein J. Nanotechnol. 2024, 15, 743–754, doi:10.3762/bjnano.15.62

• thin films can also be grown from liquid phases, employing techniques such as chemical bath deposition [31][32][33], successive ionic layer adsorption and reaction (SILAR) [34][35][36], sol–gel processes (using dip and spin coating) [37][38][39], as well as spray pyrolysis [40][41][42]. This work

Simultaneous electrochemical determination of uric acid and hypoxanthine at a TiO₂/graphene quantum dot-modified electrode

• Vu Ngoc Hoang,
• Dang Thi Ngoc Hoa,
• Nguyen Quang Man,
• Le Vu Truong Son,
• Le Van Thanh Son,
• Vo Thang Nguyen,
• Le Thi Hong Phong,
• Ly Hoang Diem,
• Kieu Chan Ly,
• Ho Sy Thang and
• Dinh Quang Khieu

Beilstein J. Nanotechnol. 2024, 15, 719–732, doi:10.3762/bjnano.15.60

• lithium-ion storage performance of C-GQDs/α-Fe2O3 composites in lithium batteries presented excellent cyclability and rate capability [19]. Among several chemical approaches for the synthesis of titania, sol–gel processes have been commonly used for practical application. In these sol–gel methods

Nanoarchitectonics to entrap living cells in silica-based systems: encapsulations with yolk–shell and sepiolite nanomaterials

• Celia Martín-Morales,
• Jorge Fernández-Méndez,
• Pilar Aranda and
• Eduardo Ruiz-Hitzky

Beilstein J. Nanotechnol. 2023, 14, 522–534, doi:10.3762/bjnano.14.43

• , by inorganic components generated by sol–gel processes from silicon alkoxides is an illustrative example of biohybrids that display the extraordinary functionality inherent to the assembled living components. For instance, bacteria such as Escherichia coli maintain their metabolic activity entrapped

Bismuth-based nanostructured photocatalysts for the remediation of antibiotics and organic dyes

• Akeem Adeyemi Oladipo and
• Faisal Suleiman Mustafa

Beilstein J. Nanotechnol. 2023, 14, 291–321, doi:10.3762/bjnano.14.26

• techniques have been developed to synthesise 3-D Bi-based nanostructures with different morphologies, including solvothermal/hydrothermal and sol–gel processes, mechanical exfoliation, solid-state reactions, chemical vapour deposition, and microwave-assisted techniques [106]. These 3-D photocatalysts have

A review on the green and sustainable synthesis of silver nanoparticles and one-dimensional silver nanostructures

• Sina Kaabipour and
• Shohreh Hemmati

Beilstein J. Nanotechnol. 2021, 12, 102–136, doi:10.3762/bjnano.12.9

• ” synthesis method. These techniques are usually accompanied by the addition of stabilizers to provide stability, prevent aggregation, control morphology, and provide physiologically compatible properties [140][141][142]. Chemical methods were previously used to produce silver nanoparticles including sol–gel

• processes [143][144][145][146], conventional chemical reduction [147][148][149][150][151], reverse micelle [152][153][154], co-precipitation [155], chemical vapor deposition [156][157][158], solvothermal [159][160][161], and electrochemical reduction [162][163][164][165]. Chemical synthesis methods are

Gas sensing properties of individual SnO₂ nanowires and SnO₂ sol–gel nanocomposites

• Alexey V. Shaposhnik,
• Dmitry A. Shaposhnik,
• Sergey Yu. Turishchev,
• Olga A. Chuvenkova,
• Stanislav V. Ryabtsev,
• Alexey A. Vasiliev,
• Xavier Vilanova,
• Francisco Hernandez-Ramirez and
• Joan R. Morante

Beilstein J. Nanotechnol. 2019, 10, 1380–1390, doi:10.3762/bjnano.10.136

• formed material. Sol–gel processes comprise the synthesis of nanopowders, consisting of spherical nanoparticles, the preparation of pastes from these powders, and finally, deposition and annealing. The development of the sol–gel synthesis of small particle semiconductor materials is no longer a

Block copolymers for designing nanostructured porous coatings

• Roberto Nisticò

Beilstein J. Nanotechnol. 2018, 9, 2332–2344, doi:10.3762/bjnano.9.218

• peculiar characteristic can be coupled with sol–gel processes to produce well-ordered oxidic architectures [95][96]. The sol–gel process involves various chemical reactions such as hydrolysis, condensation, and consequently, polymerization involving the monomers (for inorganic systems, either metal

• depending on the templating technique selected. Soft templating, in particular, is the more versatile technique as it allows very complex morphologies to be obtained, which are almost impossible to obtain using nontemplated sol–gel processes [113]. Besides this fundamental advantage, for both templating

Controllable one-pot synthesis of uniform colloidal TiO₂ particles in a mixed solvent solution for photocatalysis

• Jong Tae Moon,
• Seung Ki Lee and
• Ji Bong Joo

Beilstein J. Nanotechnol. 2018, 9, 1715–1727, doi:10.3762/bjnano.9.163

• , large surface area, uniform photocatalytic activity for each particle, and improved accessibility for the reactant molecules. To fabricate the uniform, colloidal TiO2 spheres, several synthetic methods have been reported including hydrothermal, solvothermal, and sol–gel processes [10][26][28][29

Nitrogen-doped carbon nanotubes coated with zinc oxide nanoparticles as sulfur encapsulator for high-performance lithium/sulfur batteries

• Yan Zhao,
• Zhengjun Liu,
• Liancheng Sun,
• Yongguang Zhang,
• Yuting Feng,
• Xin Wang,
• Indira Kurmanbayeva and
• Zhumabay Bakenov

Beilstein J. Nanotechnol. 2018, 9, 1677–1685, doi:10.3762/bjnano.9.159

• providing pathways for ion and electron transport. The as-prepared S/ZnO@NCNT composite is a promising cathode material for Li/S batteries. Keywords: batteries; nanocomposites; sol–gel processes; sulfur; zinc oxide (ZnO); Introduction Due to its high theoretical specific capacity of 1672 mAh·g−1 and

Synthesis of graphene–transition metal oxide hybrid nanoparticles and their application in various fields

• Arpita Jana,
• Elke Scheer and
• Sebastian Polarz

Beilstein J. Nanotechnol. 2017, 8, 688–714, doi:10.3762/bjnano.8.74

• thermochromic transition at 257 °C and this material is used as a catalyst for industrial processes, gas sensors and in LIBs [105]. Various nanostructures of V2O5 such as nanotubes, nanowires, nanofibers, nanobelts, and nanorods have been prepared by sol–gel processes, hydrothermal processes [106

Investigation of the photocatalytic efficiency of tantalum alkoxy carboxylate-derived Ta₂O₅ nanoparticles in rhodamine B removal

• Subia Ambreen,
• Mohammad Danish,
• Narendra D. Pandey and
• Ashutosh Pandey

Beilstein J. Nanotechnol. 2017, 8, 604–613, doi:10.3762/bjnano.8.65

• absorption of these materials [9][10][11]. Tantalum(V) alkoxides are important precursors for materials based on tantalum oxide in sol–gel processes. The reactions involved in sol–gel processes can be written as: An inorganic network is formed during hydrolysis the ends of which are occupied either by –OH

Tailoring bifunctional hybrid organic–inorganic nanoadsorbents by the choice of functional layer composition probed by adsorption of Cu²⁺ ions

• Veronika V. Tomina,
• Inna V. Melnyk,
• Yuriy L. Zub,
• Aivaras Kareiva,
• Miroslava Vaclavikova,
• Gulaim A. Seisenbaeva and
• Vadim G. Kessler

Beilstein J. Nanotechnol. 2017, 8, 334–347, doi:10.3762/bjnano.8.36

• was optimized controlling the synthesis conditions, such as concentrations of reactants, basicity of the medium, and the process temperature. Keywords: copper(II) ions; methyl groups; N- and F-containing functional groups; silica nanospheres; sol–gel processes; sorption; surface chemistry

Influence of hydrothermal synthesis parameters on the properties of hydroxyapatite nanoparticles

• Sylwia Kuśnieruk,
• Jacek Wojnarowicz,
• Agnieszka Chodara,
• Tadeusz Chudoba,
• Stanislaw Gierlotka and
• Witold Lojkowski

Beilstein J. Nanotechnol. 2016, 7, 1586–1601, doi:10.3762/bjnano.7.153

• chemistry techniques, such as direct precipitation from aqueous solutions, electrochemical deposition [23], sol–gel processes [24] and hydrothermal synthesis [25][26][27] (Table 1). In the majority of cases, the synthesized powder is a stoichiometric hydroxyapatite, and oftentimes contains additional phases

Synthesis, characterization and in vitro effects of 7 nm alloyed silver–gold nanoparticles

• Simon Ristig,
• Svitlana Chernousova,
• Wolfgang Meyer-Zaika and
• Matthias Epple

Beilstein J. Nanotechnol. 2015, 6, 1212–1220, doi:10.3762/bjnano.6.124

• wet chemical syntheses by co-reduction of gold and silver salts with citrate [18][19], NaBH4 [20] or starch and glucose [21], reduction with hydrazine in water-in-oil emulsions [22], sol–gel processes [23] or UV irradiation [24]. Recently, the generation of alloyed silver–gold nanoparticles by laser

Biopolymer colloids for controlling and templating inorganic synthesis

• Laura C. Preiss,
• Katharina Landfester and
• Rafael Muñoz-Espí

Beilstein J. Nanotechnol. 2014, 5, 2129–2138, doi:10.3762/bjnano.5.222

• gold salts. Like other gel biopolymer templates, gelatin has also been used in silicate sol–gel processes [72][85][86]. Ethirajan et al. [87] used the confinement provided by gelatin particles prepared through a miniemulsion to template the crystallization of hydroxyapatite (Figure 7). A further

Characterization and properties of micro- and nanowires of controlled size, composition, and geometry fabricated by electrodeposition and ion-track technology

• Maria Eugenia Toimil-Molares

Beilstein J. Nanotechnol. 2012, 3, 860–883, doi:10.3762/bjnano.3.97

• photovoltaic applications. CdTe and CdS rods are mostly synthesized by chemical vapour deposition, and sol–gel processes. Electrodeposition of stoichiometric CdTe nanowires with diameters between 80 nm and 1 μm was reported by Enculescu et al. [95]. In addition to SEM, TEM, EDX, and XRD characterization, they