TiO₂ immobilized on 2D mordenite: effect of hydrolysis conditions on structural, textural, and optical characteristics of the nanocomposites

• Marina G. Shelyapina,
• Rosario Isidro Yocupicio-Gaxiola,
• Gleb A. Valkovsky and
• Vitalii Petranovskii

Beilstein J. Nanotechnol. 2025, 16, 128–140, doi:10.3762/bjnano.16.12

• complementary characterization techniques, including XRD, SEM-EDX, TGA, N2 sorption, NMR, XPS and UV–vis spectrometry. It was observed that treatment in 70% ethanol solution preserves the ordered layered structure of 2D mordenite because TEOT hydrolysis is slowed down. This, in turn, leads to higher

• the material. However, as it was shown in [44], the formation of a dense anatase phase has a strong influence on both the value of water adsorption energy and the distribution of water adsorption centers. UV–vis spectrometry To determine the bandgap energy Eg, the Tauc method was applied to the

• , c) and Ti-ENh-C (b, d); (e) t-plot for Ti-E6h-C with a linear fit in the t range from 0.33 to 0.6 nm. TG and DTG profiles for the studied nanocomposites. (a) UV–vis diffuse reflectance spectra and (b) plots of (F(R)hν)1/2 versus photon energy for calculation of bandgap energies of TiO2-loaded

Comparison of organic and inorganic hole transport layers in double perovskite material-based solar cell

• Deepika K and
• Arjun Singh

Beilstein J. Nanotechnol. 2025, 16, 119–127, doi:10.3762/bjnano.16.11

• ETL, and NiO was used as HTL, with La2NiMnO6 as absorber [25]. The DPSC showed promising characteristics. Applications of double perovskite compounds include fuel cells, UV sensors, electrochemical sensors, indoor photovoltaics, and light-emitting diodes [26]. Double perovskite LNMO nanoparticles and

Characterization of ZnO nanoparticles synthesized using probiotic Lactiplantibacillus plantarum GP258

• Prashantkumar Siddappa Chakra,
• Aishwarya Banakar,
• Shriram Narayan Puranik,
• Vishwas Kaveeshwar,
• C. R. Ravikumar and
• Devaraja Gayathri

Beilstein J. Nanotechnol. 2025, 16, 78–89, doi:10.3762/bjnano.16.8

• nanoparticles (ZnO NPs), utilizing lactic acid bacteria isolated from curd as the key biological agent. Bacteria function as agents for both reduction and capping processes, which aids the synthesis of ZnO NPs. Various characterization techniques including XRD, FTIR, UV–vis, TEM, SEM-EDX, and zeta potential

• characterization using UV–vis spectroscopy, Fourier-transform infrared spectroscopy, X-ray diffraction measurements, energy-dispersive X-ray spectroscopy, scanning and transmission electron microscopy, photocatalytic studies, electrochemical analysis, and determination of antibacterial and anticancer activity. The

• + cations. These findings offer information about the structure and chemical interactions within the ZnO NPs (Figure 2b). UV–vis absorption The UV–Vis absorption spectra of ZnO NPs, presented in Figure 2c, establish a distinct absorption peak at 3.16 eV, revealing the characteristic bandgap energy for ZnO

A nanocarrier containing carboxylic and histamine groups with dual action: acetylcholine hydrolysis and antidote atropine delivery

• Elina E. Mansurova,
• Andrey A. Maslennikov,
• Anna P. Lyubina,
• Alexandra D. Voloshina,
• Irek R. Nizameev,
• Marsil K. Kadirov,
• Anzhela A. Mikhailova,
• Polina V. Mikshina,
• Albina Y. Ziganshina and
• Igor S. Antipin

Beilstein J. Nanotechnol. 2025, 16, 11–24, doi:10.3762/bjnano.16.2

• carried out in a manner similar to that of p(Hist-CA). After the reaction, dialysis was carried out using a 12000 Da dialysis bag to remove unencapsulated Fl, resulting in a solution of Fl@p(Hist-CA). The encapsulation efficiency (%EE) was found to be 55%. In the UV spectra of Fl@p(Hist-CA) (PB, pH 7.4

• 1H NMR spectrum of the rest of the dialysis bag, both the signals from the broken-down nanocarrier and the signals of ACh, Ch, and AcOH are present (Figure 7c). The yield of Atr over time and varying concentrations of ACh was analyzed using UV spectroscopy (Figure 8). A 3 mL sample of Atr@p(Hist-CA

• ) solution, post-reaction and after 3.5 h of dialysis (C(RA) = 0.4 mM), was placed in a 12000 Da dialysis bag with ACh added at concentrations of 0.4, 4, and 40 mM. The dialysate volume was 50 mL. Yield and concentration of atropine were assessed through UV absorption at 224 nm, revealing that approximately

Attempts to preserve and visualize protein corona on the surface of biological nanoparticles in blood serum using photomodification

• Julia E. Poletaeva,
• Anastasiya V. Tupitsyna,
• Alina E. Grigor’eva,
• Ilya S. Dovydenko and
• Elena I. Ryabchikova

Beilstein J. Nanotechnol. 2024, 15, 1654–1666, doi:10.3762/bjnano.15.130

• , Russia) [23]. PACL (Figure 1) is a molecule carrying two orthogonal reactive groups, namely, (i) a maleimide residue that modifies serum proteins at their thiol groups and (ii) an nitroaryl azide group to form covalent cross-links between proteins and nanoparticles under the influence of UV radiation

• . When incubated in the dark, PACL binds to the thiol groups of serum proteins (i.e., it modifies them). The reaction mixture is then irradiated with UV, under the action of which the nitroaryl azide group covalently fixes the modified proteins on the surface of the NPs. This mechanism has been

• ability of blood serum proteins to bind to each other under the influence of PACL and subsequent UV irradiation. However, if was found that serum proteins bind only to the surface of model NPs and do not cross-link with each other. In other words, in FBS incubated with PACL and irradiated with UV, the

Fabrication of hafnium-based nanoparticles and nanostructures using picosecond laser ablation

• Abhishek Das,
• Mangababu Akkanaboina,
• Jagannath Rathod,
• R. Sai Prasad Goud,
• Kanaka Ravi Kumar,
• Raghu C. Reddy,
• Ratheesh Ravendran,
• Katia Vutova,
• S. V. S. Nageswara Rao and
• Venugopal Rao Soma

Beilstein J. Nanotechnol. 2024, 15, 1639–1653, doi:10.3762/bjnano.15.129

• . All NPs exhibited novel optical reflectance properties. Reflectance measurements revealed that the fabricated NPs had a very high and broad optical absorption throughout the UV–vis–NIR range. The NPs synthesised in toluene exhibited the best absorption. The successful fabrication of Hf NSs with the

• morphology was analysed using field-emission scanning electron microscopy (FESEM); the composition was determined by EDX attached to the FESEM (Carl Zeiss Smart SEM ULTRA 55). Reflectivity was investigated using a UV–vis–NIR spectrometer (PerkinElmer Lambda 750). For photoluminescence (PL) measurements, a

• 60°) taken in the wavelength range from 250 to 1200 nm. The black curve corresponds to the reflectance spectrum of the reference pristine Si sample; the red curve is HfNPs-T, the blue curve is HfNPs-A, and the green curve is HfNPs-D. The values of the reflectance and reduction in the UV (λ = 250 nm

Liver-targeting iron oxide nanoparticles and their complexes with plant extracts for biocompatibility

• Shushanik A. Kazaryan,
• Seda A. Oganian,
• Gayane S. Vardanyan,
• Anatolie S. Sidorenko and
• Ashkhen A. Hovhannisyan

Beilstein J. Nanotechnol. 2024, 15, 1593–1602, doi:10.3762/bjnano.15.125

• colorimetric method using the stable radical 2,2-diphenyl-1-picrylhydrazyl (DPPH, Alfa Aeser, Germany) at 30 °C. Optical density (OD) detection was carried out at 517 nm wavelength (UV-VIS 18, MRC, Israel), and ARA was estimated according to the following equation: where ODc is the optical density of the

• ]. Spectral analysis of sample complexes The analysis of the spectra of the studied samples of 70% ethanol buffer extract of T. polium, rutin, and their complexes with Fe3O4 NPs was carried out at wavelengths from 200 to 800 nm using a UV–vis spectrophotometer UV-VIS 18 (MRC, Israel) [50]. Animal experiment

• ; EC 2.3.2.2), and alkaline phosphatase (ALP; EC 3.1.3.1) in blood plasma, as well as the content of total protein (TP), albumin, total cholesterol (TC), HDL, and LDL, was carried out using standard BioSystems reagent kits (Barcelona, Spain) on a UV–vis spectrophotometer UV-VIS 18 (MRC, Israel

Facile synthesis of size-tunable L-carnosine-capped silver nanoparticles and their role in metal ion sensing and catalytic degradation of p-nitrophenol

• Akash Kumar,
• Ridhima Chadha,
• Abhishek Das,
• Nandita Maiti and
• Rayavarapu Raja Gopal

Beilstein J. Nanotechnol. 2024, 15, 1576–1592, doi:10.3762/bjnano.15.124

• ʟ-carnosine in synthesizing tunable plasmonic silver nanoparticles (ʟ-car-AgNPs). The formation of ʟ-car-AgNPs was confirmed via UV–vis optical absorption spectroscopy, showing single and double plasmonic peaks, depending on the synthesis conditions. Physicochemical characterization using TEM, FTIR

• degradation of P-NP and the formation of P-AP were monitored by recording UV–vis spectra in the 300–900 nm range. The disappearance of the yellow color, characteristic of the nitrophenolate ion, was observed upon the addition of the AgNP catalyst, accompanied by a concomitant decrease in the absorbance

• . Detection of Cd2+and Pb+2 using ʟ-car-AgNP1 The ʟ-carnosine-capped AgNPs were evaluated regarding the detection of heavy metals via UV–vis spectrophotometry. A series of metal ions, namely As3+, Al3+, Cd2+, Zn2+, Hg2+, Ni2+, Cu2+, Cr3+, Pb2+, Mo2+, and Fe3+, was used for the sensing experiment. Figure 5

Green synthesis of silver nanoparticles derived from algae and their larvicidal properties to control Aedes aegypti

• Matheus Alves Siqueira de Assunção,
• Douglas Dourado,
• Daiane Rodrigues dos Santos,
• Gabriel Bezerra Faierstein,
• Mara Elga Medeiros Braga,
• Severino Alves Junior,
• Rosângela Maria Rodrigues Barbosa,
• Herminio José Cipriano de Sousa and
• Fábio Rocha Formiga

Beilstein J. Nanotechnol. 2024, 15, 1566–1575, doi:10.3762/bjnano.15.123

• residues in the environment [30]. Physical methods include laser ablation, UV irradiation, evaporation condensation, aerosol methods, and lithography. High cost, high energy consumption, and expensive equipment make these techniques uneconomical [31]. Because of these disadvantages, synthesis methods based

Ultrablack color in velvet ant cuticle

• Vinicius Marques Lopez,
• Wencke Krings,
• Juliana Reis Machado,
• Stanislav Gorb and
• Rhainer Guillermo-Ferreira

Beilstein J. Nanotechnol. 2024, 15, 1554–1565, doi:10.3762/bjnano.15.122

• setup prolongs the light’s exposure to the melanized integument, thereby augmenting light absorption by the pigment [10]. Consequently, ultrablack colors exhibit an extraordinarily low reflectance across ultraviolet and visible (UV–vis) spectrum wavelengths, often falling below 0.5% of the incident

• Spectralon® standard that reflects 99% of light in the UV–vis spectrum. A standard distance of 5 mm was maintained between the fiber probe and both the Spectralon standard and the sample. This distance was determined using the scale provided on the Ocean Insight holder, ensuring consistency across all

• : Salticidae), and the bird-of-paradise Drepanornis bruijnii (Passeriformes: Paradisaeidae). The spectra of these species were obtained from data provided in [10][12], and species with the highest absorbance in the UV–vis spectrum were selected. Thermal images This experimental protocol was adapted from [15

Strain-induced bandgap engineering in 2D ψ-graphene materials: a first-principles study

• Kamal Kumar,
• Nora H. de Leeuw,
• Jost Adam and
• Abhishek Kumar Mishra

Beilstein J. Nanotechnol. 2024, 15, 1440–1452, doi:10.3762/bjnano.15.116

• calculations and concluded that ψ-graphene has the potential to be employed in infrared (IR) sensors, ultraviolet (UV) optomechanical sensors, and visible-light sensors [39]. Li et al. theoretically reported a maximum theoretical storage capacity of 372 mAh·g−1 for Li, showing its capability to be utilized as

Various CVD-grown ZnO nanostructures for nanodevices and interdisciplinary applications

• The-Long Phan,
• Le Viet Cuong,
• Vu Dinh Lam and
• Ngoc Toan Dang

Beilstein J. Nanotechnol. 2024, 15, 1390–1399, doi:10.3762/bjnano.15.112

• . Depending on the morphology and crystal quality, their photoluminescence spectra have only a strong UV emission associated with the exciton radiative recombination, or both UV and defect-related visible emissions with their relative intensity ratio varying with the excitation power density. The obtained

• microcavities [9]. Additionally, it is a transparent semiconductor with significant piezoelectricity [10]. These noble characteristics suggest ZnO to be a potential material in the fabrication of UV/blue/green LEDs, solid-state random lasers, UV-absorption devices, and nanogenerators [9][11][12][13]. Magnetic

• PL spectra which can be based on to classify the ZnO nanostructures into two sample groups. The first group gives only a UV emission at approx. 384–390 nm, such as P1, T2, M, and S shown in Figure 8a. Here, the UV emission is associated with the exciton radiative recombination [66]. An excitation

Green synthesis of carbon dot structures from Rheum Ribes and Schottky diode fabrication

• Muhammed Taha Durmus and
• Ebru Bozkurt

Beilstein J. Nanotechnol. 2024, 15, 1369–1375, doi:10.3762/bjnano.15.110

• TALOS F200S TEM 200 kV, Malvern Zetasizer Nano ZSP, PANalytical X-ray diffractometer, Bruker VERTEX 70v, Specs‐Flex with a standard Al X‐ray source, WITech alpha 300R, VAKSIS PVD Handy, Zeiss Sigma 300, KEITLEY 2400 picoammeter/voltage source, Shimadzu UV-1800 spectrophotometer, and Agilent Technologies

• electron microscopy (SEM), I–V/C–V measurements, UV–vis spectroscopy, and steady-state fluorescence spectroscopy, respectively. CDs synthesis 2.5 g of the powdered Rheum ribes plant was placed in an autoclave bottle, and 50 mL of pure water was added to the bottle. This aqueous solution was placed in an

• the structure of the coated CDs film (Figure 5); the CDs film thickness was determined as ca. 566 nm. In addition, a UV–vis absorption spectrum of the CDs layer was taken (Figure 6a), and the bandgap value of the layer was determined from the graph of hν versus (αhν)2 using the Tauc equation [23]. The

Nanoarchitectonics with cetrimonium bromide on metal nanoparticles for linker-free detection of toxic metal ions and catalytic degradation of 4-nitrophenol

• Akash Kumar and
• Raja Gopal Rayavarapu

Beilstein J. Nanotechnol. 2024, 15, 1312–1332, doi:10.3762/bjnano.15.106

• CTAB-AuNR2, centrifuged and as-prepared, respectively. The catalytic conversion of 4-NP to 4-AP was measured using a UV–vis spectrophotometer at 300–900 nm. The disappearance of the color upon adding nanoparticles was measured and further, the change in the plasmon band was recorded. As controls, we

• , surface capping, and linker molecules are required to degrade 4-nitrophenol. Therefore, this study analyzed the impact of size, shape, metal type, and nanoparticle concentration on converting 4-nitrophenol to 4-aminophenol. Characterization of CTAB-capped nanoparticles UV–vis, DLS, Zeta, FTIR, XRD, and

Mn-doped ZnO nanopowders prepared by sol–gel and microwave-assisted sol–gel methods and their photocatalytic properties

• Cristina Maria Vlăduț,
• Crina Anastasescu,
• Silviu Preda,
• Oana Catalina Mocioiu,
• Simona Petrescu,
• Jeanina Pandele-Cusu,
• Dana Culita,
• Veronica Bratan,
• Ioan Balint and
• Maria Zaharescu

Beilstein J. Nanotechnol. 2024, 15, 1283–1296, doi:10.3762/bjnano.15.104

• parallel in Figure 7. The insets show a wide pore size distribution reaching 120 nm and pore width maxima located in the mesoporosity area for both samples (40 nm for SG and 35–45 nm for MW). Similar textural features for SG and MW samples are presented in Table 3. UV–vis spectroscopy The recorded UV–vis

• ]. The direct transitions represented in the inset allow one to evaluate the forbidden band energies, Eg(SG) = 2.95 eV and Eg(MW) = 3.05 eV, indicating a slighty higher photoreactivity of the SG sample. Supporting Information File 1, Figure S2 presents comparative UV–vis spectra for the undoped SG ZnO

• photocatalytic properties of SG and MW. Based on these preliminary results, it is fully desirable to develop such engineered materials [57] for the removal of organic pollutants. It is important to expand the activity range of the materials from UV to visible light by tailoring the manganese addition to ZnO and

Enhanced catalytic reduction through in situ synthesized gold nanoparticles embedded in glucosamine/alginate nanocomposites

• Chi-Hien Dang,
• Le-Kim-Thuy Nguyen,
• Minh-Trong Tran,
• Van-Dung Le,
• Nguyen Minh Ty,
• T. Ngoc Han Pham,
• Hieu Vu-Quang,
• Tran Thi Kim Chi,
• Tran Thi Huong Giang,
• Nguyen Thi Thanh Tu and
• Thanh-Danh Nguyen

Beilstein J. Nanotechnol. 2024, 15, 1227–1237, doi:10.3762/bjnano.15.99

• synthesizing gold nanoparticles (AuNPs) within a glucosamine/alginate (GluN/Alg) nanocomposite via an ionotropic gelation mechanism in aqueous environment. The resulting nanocomposite, AuNPs@GluN/Alg, underwent thorough characterization using UV–vis, EDX, FTIR, SEM, TEM, SAED, and XRD analyses. The spherical

• g·mL−1). The reduction process was initiated through heating the mixture and visually confirmed by a change in color of the reaction mixture indicating the formation of AuNPs on the GluN/Alg composite. UV–vis spectroscopy within the range of 300 to 600 nm was employed to monitor this process

• tracked over time using a UV–vis spectrophotometer, covering the wavelength range of 200–600 nm at room temperature without delay. We examined the kinetics of catalytic degradation by monitoring changes in absorbance values at specific wavelengths. Given the small quantity of nanocatalyst and the

Synthesis, characterization and anticancer effect of doxorubicin-loaded dual stimuli-responsive smart nanopolymers

• Ömür Acet,
• Pavel Kirsanov,
• Burcu Önal Acet,
• Inessa Halets-Bui,
• Dzmitry Shcharbin,
• Şeyda Ceylan Cömert and
• Mehmet Odabaşı

Beilstein J. Nanotechnol. 2024, 15, 1189–1196, doi:10.3762/bjnano.15.96

• explained in detail in section “DOX loading to SNPs “. Then, the solutions with DOX-loaded SNPs were analyzed by UV–vis spectrophotometry at 495 nm wavelength with pure PBS serving as a control to calculate the amount of unencapsulated DOX. PBS buffer was used to remove both unencapsulated and unreacted DOX

Quantum-to-classical modeling of monolayer Ge₂Se₂ and its application in photovoltaic devices

• Anup Shrivastava,
• Shivani Saini,
• Dolly Kumari,
• Sanjai Singh and
• Jost Adam

Beilstein J. Nanotechnol. 2024, 15, 1153–1169, doi:10.3762/bjnano.15.94

• point. The maximum absorption coefficient is 5 × 105 cm−1 along the XX direction. The highest peak for the ZZ direction is calculated as 5.8 × 105 cm−1, corresponding to the UV region. We attribute this maximum to the transition from VBM to CBM, while the other peaks designate a transition from VBM to

Photocatalytic methane oxidation over a TiO₂/SiNWs p–n junction catalyst at room temperature

• Qui Thanh Hoai Ta,
• Luan Minh Nguyen,
• Ngoc Hoi Nguyen,
• Phan Khanh Thinh Nguyen and
• Dai Hai Nguyen

Beilstein J. Nanotechnol. 2024, 15, 1132–1141, doi:10.3762/bjnano.15.92

• absorption than planar Si wafers because of the specific morphology [45]. The optical absorption of the as-prepared catalyst is shown in Figure 3a. The UV–vis diffuse reflection spectrum of TiO2/SiNWs catalyst is drastically reduced in comparison to the pure SiNWs. The superior antireflection property of the

• crucial in photogenerated charge separation and adsorption enhancement under UV–vis light. In other words, the ethane productivity of TiO2/Si NWs was five times higher (210 µmol/cm2) than that of pure p-Si NWs (20 µmol/cm2) and glass/TiO2 (30 µmol/cm2). Photocatalytic OCM over TiO2/Si NWs catalysts was

• recorded in a batch reactor under different wavelengths of light. As shown in Figure 6b, no products were detected under the visible-light irradiation. The photocatalytic performance under UV illumination was significantly lower than that under full illumination. Figure 7 shows the recyclability of the p–n

Unveiling the potential of alginate-based nanomaterials in sensing technology and smart delivery applications

• Shakhzodjon Uzokboev,
• Khojimukhammad Akhmadbekov,
• Ra’no Nuritdinova,
• Salah M. Tawfik and
• Yong-Ill Lee

Beilstein J. Nanotechnol. 2024, 15, 1077–1104, doi:10.3762/bjnano.15.88

• sensor. Another fluorescence-based smart sensor from alginate nanofilms was prepared [122]. Scientists proved that relative humidity could be detected using a guar gum–sodium alginate (GGSA) nanocomposite film. The study found that the fluorescence of biocomposite films under UV light varies at various

Effect of wavelength and liquid on formation of Ag, Au, Ag/Au nanoparticles via picosecond laser ablation and SERS-based detection of DMMP

• Sree Satya Bharati Moram,
• Chandu Byram and
• Venugopal Rao Soma

Beilstein J. Nanotechnol. 2024, 15, 1054–1069, doi:10.3762/bjnano.15.86

• was meticulously evaluated by analyzing the ablation rates, surface plasmon resonance peak positions, and particle size distributions of the obtained colloids. The nanoparticles (NPs) were characterized using the techniques of UV–visible absorption, transmission electron microscopy, and energy

• . This process took approximately 20 minutes. Characterization techniques The absorption studies were conducted by placing 3 mL of the colloidal solution in a 1 cm quartz cuvette and using a UV–visible absorption spectrometer (PerkinElmer, LAMBDA 750) within the 300–800 nm wavelength range. The

• detection of DMMP (1.2 ppm V) in the vapor phase using Glass_Ag_Au NPs, 3D fractal microstructure substrates developed by corner lithography and anisotropic wet etching of silicon using the 785 nm as the Raman excitation. When UV excitation was utilized during the measurements, the Raman peak intensities

Bolometric IR photoresponse based on a 3D micro-nano integrated CNT architecture

• Yasameen Al-Mafrachi,
• Sandeep Yadav,
• Sascha Preu,
• Jörg J. Schneider and
• Oktay Yilmazoglu

Beilstein J. Nanotechnol. 2024, 15, 1030–1040, doi:10.3762/bjnano.15.84

• numerous advantages at room temperature operation. New thermally isolated micro-nano architectures equipped with integrated temperature sensors should outperform their predecessors regarding various critical aspects, such as ultra-broadband detection from ultraviolet (UV) to terahertz radiation [1

• VACNTs (water-assisted CVD on silicon substrates with ethylene as the carbon source) has been investigated by [3]. They showed that vertically aligned SWCNTs can absorb light almost perfectly with a reflectance of 0.01–0.02 over a very wide spectral range (0.2–200 μm). The UV-to-mid-IR absorption

Beyond biomimicry – next generation applications of bioinspired adhesives from microfluidics to composites

• Dan Sameoto

Beilstein J. Nanotechnol. 2024, 15, 965–976, doi:10.3762/bjnano.15.79

• ) and (B) used silicone rubbers as the structural material for adhesives, and were capable of isotropic (A) or directional (B) adhesive performance depending on the symmetry of the cap. A more durable and useful system used deep-UV exposure of acrylic to form master molds, followed by a negative mold in

A review on the structural characterization of nanomaterials for nano-QSAR models

• Salvador Moncho,
• Eva Serrano-Candelas,
• Jesús Vicente de Julián-Ortiz and
• Rafael Gozalbes

Beilstein J. Nanotechnol. 2024, 15, 854–866, doi:10.3762/bjnano.15.71

• reflectance UV–vis spectra). Alternative formulations for valence and conduction band energies, based only on pre-known physicochemical constants and values from reference handbooks, have been reported as well [79][80]. Furthermore, the electric characteristics of the nanoparticle surface can be reported by

Intermixing of MoS₂ and WS₂ photocatalysts toward methylene blue photodegradation

• Maryam Al Qaydi,
• Nitul S. Rajput,
• Michael Lejeune,
• Abdellatif Bouchalkha,
• Mimoun El Marssi,
• Steevy Cordette,
• Chaouki Kasmi and
• Mustapha Jouiad

Beilstein J. Nanotechnol. 2024, 15, 817–829, doi:10.3762/bjnano.15.68

• properties and photodegradation experiments were conducted on a UV–vis–near IR spectrometer (JASCO V-670) and using solar simulator excitation for the PD monitoring using 10 mL of MB dye solution with a concentration of 5 mg/L (10−5 M) and 1 mg of exfoliated photocatalyst. The intensity of the optical

• intensity of the 631 nm peak and the MB concentration. For all experiments, a first run was conducted in the dark for 30 min, followed by PD tests, and maintained for 180 min while monitored by a UV–vis spectrometer every 30 min. Raman spectroscopy for a) MoS2, b) WS2, and c) MoS2/WS2 composite. XRD