Electrical, photocatalytic, and sensory properties of graphene oxide and polyimide implanted with low- and medium-energy silver ions

• Josef Novák,
• Eva Štěpanovská,
• Petr Malinský,
• Vlastimil Mazánek,
• Jan Luxa,
• Ulrich Kentsch and
• Zdeněk Sofer

Beilstein J. Nanotechnol. 2025, 16, 1794–1811, doi:10.3762/bjnano.16.123

• atomic force microscopy. Electrical properties as a function of air humidity were evaluated using a two-point method, and photocatalytic activity was tested by monitoring the UV-induced decomposition of rhodamine B. The results demonstrate that ion implantation significantly reduces surface resistivity

• amorphization of the material and probably to the carbonization of the polyimide. Surface morphology studied by AFM Changes in the surface morphology of PI implanted with 20 keV and 1.5 MeV Ag ions at different fluences were examined by atomic force microscopy (AFM). The basic parameters arithmetic average

Prospects of nanotechnology and natural products for cancer and immunotherapy

• Jan Filipe Andrade Santos,
• Marcela Bernardes Brasileiro,
• Pamela Danielle Cavalcante Barreto,
• Ligiane Aranha Rocha and
• José Adão Carvalho Nascimento Júnior

Beilstein J. Nanotechnol. 2025, 16, 1644–1667, doi:10.3762/bjnano.16.116

• aptamer, sorafenib, and ursolic acid as an API at 4 mg·mL−1 in methanol. Physicochemical tests showed that the nanoparticles have a spherical shape, confirmed by atomic force microscopy (AFM), and are stable in ultrapure water and Dulbecco’s modified eagle medium (DMEM) with 10% FBS. Procedures to

Venom-loaded cationic-functionalized poly(lactic acid) nanoparticles for serum production against Tityus serrulatus scorpion

• Philippe de Castro Mesquita,
• Karla Samara Rocha Soares,
• Manoela Torres-Rêgo,
• Emanuell dos Santos-Silva,
• Mariana Farias Alves-Silva,
• Alianda Maira Cornélio,
• Matheus de Freitas Fernandes-Pedrosa and
• Arnóbio Antônio da Silva-Júnior

Beilstein J. Nanotechnol. 2025, 16, 1633–1643, doi:10.3762/bjnano.16.115

• analysis supported small and narrow-sized cationic functionalized nanoparticles. Atomic force microscopy and scanning electron microscopy images showed nanoparticles with a spherical and smooth shape. The stability of tested formulations was accessed for six weeks, and the sustained release of proteins

• corroborates the high encapsulation efficiency obtained by the BCA assay. Field emission gun scanning electron microscopy and atomic force microscopy analyses Field emission gun scanning electron microscopy (FEGSEM) and atomic force microscopy (AFM) analyses were realized to access shape and surface features

• . serrulatus venom protein-loaded PLA nanoparticles at 1.0% (NPs + Tsv 1.0%). MM: molecular mass marker. Gel stained with Coomassie brilliant blue R-250. 2D and 3D atomic force microscopy and field emission gun scanning electron microscopy images, respectively, of formulations of Tityus serrulatus venom-loaded

Bioinspired polypropylene-based functionally graded materials and metamaterials modeling the mistletoe–host interface

• Lina M. Rojas González,
• Naeim Ghavidelnia,
• Christoph Eberl and
• Max D. Mylo

Beilstein J. Nanotechnol. 2025, 16, 1592–1606, doi:10.3762/bjnano.16.113

• − l0)/l0 = Δl/l0) values were calculated from the resulting force and displacement data and specimen geometries. The Young’s modulus (E = σ/ε) of the specimens was calculated within the linear region of the stress–strain curves, and the ultimate tensile strength (UTS) was calculated as the highest

Modeling magnetic properties of cobalt nanofilms used as a component of spin hybrid superconductor–ferromagnetic structures

• Aleksey Fedotov,
• Olesya Severyukhina,
• Anastasia Salomatina and
• Anatolie Sidorenko

Beilstein J. Nanotechnol. 2025, 16, 1557–1566, doi:10.3762/bjnano.16.110

• : where UMEAM(r) is the force potential, the modified embedded atom method (MEAM) potential was used in this work; Hex(r) is the exchange interaction energy of spins; r = {r1,r2,…,rN} is the generalized variable showing the dependence on the whole set of radial vectors of atoms; κ,λ are viscous friction

• force parameter and damping spin coefficient, respectively; χ(t), η(t) are white noise present in the description of atom motion processes and the behavior of their spins, respectively; and ωi is the multiplication value of the gyromagnetic ratio and the local magnetic field [22]. It has been known for

• properties, are used: where t and t´ are different time points; α and β are components of the random force vector, for the three-dimensional case {α,β} = {x,y,z}; δ(t − t´) is the Dirac delta measure; kB is the Boltzmann constant; is the reduced Planck constant; B is the mobility value of the Brownian

Influence of laser beam profile on morphology and optical properties of silicon nanoparticles formed by laser ablation in liquid

• Natalie Tarasenka,
• Vladislav Kornev,
• Alena Nevar and
• Nikolai Tarasenko

Beilstein J. Nanotechnol. 2025, 16, 1533–1544, doi:10.3762/bjnano.16.108

• directions depending on the material and laser parameters. As shown previously [33], contrary to conventional optical traps using Gaussian beams, Bessel beam traps exhibit significant gradients only in the transverse directions, which leads to particle confinement in two dimensions with a scattering force in

Cross-reactivities in conjugation reactions involving iron oxide nanoparticles

• Shoronia N. Cross,
• Katalin V. Korpany,
• Hanine Zakaria and
• Amy Szuchmacher Blum

Beilstein J. Nanotechnol. 2025, 16, 1504–1521, doi:10.3762/bjnano.16.106

• thermodynamic driving force, use simple reaction conditions, produce no interfering byproducts, produce products that are stable under physiological conditions, and can be purified easily using non-chromatographic means. The copper-catalyzed azide–alkyne cycloaddition (CuAAC) reaction is one of the most

Laser processing in liquids: insights into nanocolloid generation and thin film integration for energy, photonic, and sensing applications

• Akshana Parameswaran Sreekala,
• Pooja Raveendran Nair,
• Jithin Kundalam Kadavath,
• Bindu Krishnan,
• David Avellaneda Avellaneda,
• M. R. Anantharaman and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 1428–1498, doi:10.3762/bjnano.16.104

• photodetectors, and the film surface coverage was improved by multiple layer depositions and condensation of colloidal suspension. Irregular particle shapes and sizes were visible in 3D atomic force microscopy (AFM) images with sizes ranging between 60 and 80 nm. The NPs agglomerated to form submicroparticles

Ferroptosis induction by engineered liposomes for enhanced tumor therapy

• Alireza Ghasempour,
• Mohammad Amin Tokallou,
• Mohammad Reza Naderi Allaf,
• Mohsen Moradi,
• Hamideh Dehghan,
• Mahsa Sedighi,
• Mohammad-Ali Shahbazi and
• Fahimeh Lavi Arab

Beilstein J. Nanotechnol. 2025, 16, 1325–1349, doi:10.3762/bjnano.16.97

• light scattering (DLS) is commonly used to determine liposome size and size distribution. Transmission electron microscopy (TEM) and atomic force microscopy (AFM) can be used to image liposome morphology and determine lamellarity. Zeta potential measurements assess the surface charge of liposomes, which

Chitosan nanocomposite containing rotenoids: an alternative bioinsecticidal approach for the management of Aedes aegypti

• Maria A. A. Bertonceli,
• Vitor D. C. Cristo,
• Ivo J. Vieira,
• Francisco J. A. Lemos,
• Arnoldo R. Façanha,
• Raimundo Braz-Filho,
• Gustavo V. T. Batista,
• Luis G. M. Basso,
• Sérgio H. Seabra,
• Thalya S. R. Nogueira,
• Felipe F. Moreira,
• Arícia L. E. M. Assis,
• Antônia E. A. Oliveira and
• Kátia V. S. Fernandes

Beilstein J. Nanotechnol. 2025, 16, 1197–1208, doi:10.3762/bjnano.16.88

• of 1 cm−1 and an accumulation of 35 scans per spectrum. A compressive force of 15 N was applied to the samples during measurement to ensure proper contact with the ATR crystal surface. Quantification of rotenoids by high-performance liquid chromatography The quantification of rotenoids was performed

Electronic and optical properties of chloropicrin adsorbed ZnS nanotubes: first principle analysis

• Prakash Yadav,
• Boddepalli SanthiBhushan and
• Anurag Srivastava

Beilstein J. Nanotechnol. 2025, 16, 1184–1196, doi:10.3762/bjnano.16.87

• was performed with stringent convergence criteria: a maximum force tolerance of 0.05 eV/Å and a stress tolerance of 0.05 eV/Å3. These parameters ensured the reliability and accuracy of the resulting structural configurations for subsequent electronic and transport property analyses. To study the

Mechanical stability of individual bacterial cells under different osmotic pressure conditions: a nanoindentation study of Pseudomonas aeruginosa

• Lizeth García-Torres,
• Idania De Alba Montero,
• Eleazar Samuel Kolosovas-Machuca,
• Facundo Ruiz,
• Sumati Bhatia,
• Jose Luis Cuellar Camacho and
• Jaime Ruiz-García

Beilstein J. Nanotechnol. 2025, 16, 1171–1183, doi:10.3762/bjnano.16.86

• , S.L.P. México 10.3762/bjnano.16.86 Abstract Nanomechanical maps to test the mechanical response of the outer envelope of Pseudomonas aeruginosa were obtained utilizing atomic force microscopy in force–volume mode in the low range of loading forces when exposed to hypotonic (Milli-Q water), isotonic

• (PBS), and hypertonic (0.5 M NaCl) solutions. Imaging and mechanical testing showed that bacteria are highly resilient to deformation and can withstand repetitive indentations in the range of 500 pN. Analysis of force spectra revealed that although there are differences in the mechanical response

• within the first stages of nanoindentation, similar values in the slopes of the curves reflected a stable stiffness of about kB = 20 mN/m and turgor pressures of Pt = 12.1 kPa. Interestingly, a change in the nonlinear regime of the force curves and a gradual increase in maximal deformation by the AFM tip

Deep learning for enhancement of low-resolution and noisy scanning probe microscopy images

• Samuel Gelman,
• Irit Rosenhek-Goldian,
• Nir Kampf,
• Marek Patočka,
• Maricarmen Rios,
• Marcos Penedo,
• Georg Fantner,
• Amir Beker,
• Sidney R. Cohen and
• Ido Azuri

Beilstein J. Nanotechnol. 2025, 16, 1129–1140, doi:10.3762/bjnano.16.83

• shows deep learning models to be superior for super-resolution tasks and enables significant reduction in AFM measurement time, whereby low-pixel-resolution AFM images are enhanced in both resolution and fidelity through deep learning. Keywords: atomic force microscopy; deep learning; fast scanning

• ; low resolution; super resolution; Introduction The capability of atomic force microscopy (AFM) to achieve high resolution at the nanometer level in plane (xy) and at the angstrom level in height (z), on a variety of surfaces, is one of its major advantages. AFM topographical imaging enables high

• scan direction (here, x). However, in some modes, such as peak force and photothermal off-resonance tapping as used here, unless the data is significantly oversampled, decreasing the number of pixels in both x and y scan directions will lower acquisition time proportionately. We therefore sample here

Single-layer graphene oxide film grown on α-Al₂O₃(0001) for use as an adsorbent

• Shiro Entani,
• Mitsunori Honda,
• Masaru Takizawa and
• Makoto Kohda

Beilstein J. Nanotechnol. 2025, 16, 1082–1087, doi:10.3762/bjnano.16.79

• Figure 1 shows an atomic force microscopy (AFM) image of SLG and SLGO on α-Al2O3(0001) substrates. The as-grown SLG film has an atomically flat surface and wrinkles with its height less than 0.4 nm [18]. The single layer of graphene was confirmed through X-ray photoelectron spectroscopy (XPS) peak

• was removed from the SLGO surface by water rinsing and then the Cs-adsorbed SLGO specimen was introduced in the XPS chamber kept at ultra-high vacuum. The surface morphology of SLGO was examined using atomic force microscopy (AFM, SII SAP300). AFM images of (a) SLG/α-Al2O3(0001) and (b) SLGO/α-Al2O3

Piezoelectricity of hexagonal boron nitrides improves bone tissue generation as tested on osteoblasts

• Sevin Adiguzel,
• Nilay Cicek,
• Zehra Cobandede,
• Feray B. Misirlioglu,
• Hulya Yilmaz and
• Mustafa Culha

Beilstein J. Nanotechnol. 2025, 16, 1068–1081, doi:10.3762/bjnano.16.78

• evaluated. The synthesized hBNs and purchased BaTiO3 were used after their full characterization by imaging and spectroscopic techniques. The piezoelectric behavior of both NMs was evaluated using piezoresponse force microscopy (PRFM). During in vitro studies, the piezoelectricity of the NMs was stimulated

• hBN. The materials were characterized using spectroscopic, imaging, and thermal techniques, followed by assessment of their piezoelectric properties via piezoresponse force microscopy (PRFM). In vitro studies on human osteoblasts (HOb) under ultrasound (US) exposure examined proliferation, cellular

• -Vis-NIR) measured optical properties across the 200–800 nm range, while dynamic light scattering (DLS, Malvern Panalytical) provided data on hydrodynamic size and zeta potential after dispersing 1 mg of material in 1 mL of deionized water and sonicating for 30 min. Finally, piezoresponse force

Soft materials nanoarchitectonics: liquid crystals, polymers, gels, biomaterials, and others

• Katsuhiko Ariga

Beilstein J. Nanotechnol. 2025, 16, 1025–1067, doi:10.3762/bjnano.16.77

Time-resolved probing of laser-induced nanostructuring processes in liquids

• Maximilian Spellauge,
• David Redka,
• Mianzhen Mo,
• Changyong Song,
• Heinz Paul Huber and
• Anton Plech

Beilstein J. Nanotechnol. 2025, 16, 968–1002, doi:10.3762/bjnano.16.74

Shape, membrane morphology, and morphodynamic response of metabolically active human mitochondria revealed by scanning ion conductance microscopy

• Eric Lieberwirth,
• Anja Schaeper,
• Regina Lange,
• Ingo Barke,
• Simone Baltrusch and
• Sylvia Speller

Beilstein J. Nanotechnol. 2025, 16, 951–967, doi:10.3762/bjnano.16.73

• processes and warrants further investigation. Scanning probe microscopy (SPM) methods, such as atomic force microscopy (AFM), have been employed to image mitochondria in liquid, showing features of both the inner and outer membrane [22][23][24]. However, AFM measurements are influenced by the cantilever

• isolated mitochondria. Remarkably, the geometric and mechanical properties of microtubules are comparable to those of the nanopipette. Microtubules are hollow structures with an opening diameter of 18 nm and a total diameter of 25–30 nm [42][43]. Their pushing force, in the range of 3–4 pN [44], is similar

• metabolically active structures, as samples remain immersed in a nutrient medium and are not physically contacted. Unlike AFM, SICM measurements exert no mechanical force directly on the sample, and the ion currents involved are minimal. Although electric fields diminish rapidly over short distances [27][28][51

Tendency in tip polarity changes in non-contact atomic force microscopy imaging on a fluorite surface

• Bob Kyeyune,
• Philipp Rahe and
• Michael Reichling

Beilstein J. Nanotechnol. 2025, 16, 944–950, doi:10.3762/bjnano.16.72

• Bob Kyeyune Philipp Rahe Michael Reichling Institut für Physik, Universität Osnabrück, Barbarastraße 7, 49076 Osnabrück, Germany 10.3762/bjnano.16.72 Abstract We investigate the impact of tip changes on atomic-scale non-contact atomic force microscopy (NC-AFM) contrast formation when imaging a

• . Keywords: atomic resolution imaging; calcium fluoride surface; interaction force; non-contact atomic force microscopy (NC-AFM); tip change; Introduction Non-contact atomic force microscopy (NC-AFM) [1] is a surface science tool that has been used to atomically resolve surfaces of semiconductor and

• ‘dark’. In NC-AFM, the frequency shift Δf is proportional to the weighted average of the tip–sample interaction force gradient [30]. Attractive forces mostly exhibiting a positive force gradient are considered as negative and yield a negative Δf according to a generally accepted convention. When

Focused ion beam-induced platinum deposition with a low-temperature cesium ion source

• Thomas Henning Loeber,
• Bert Laegel,
• Meltem Sezen,
• Feray Bakan Misirlioglu,
• Edgar J. D. Vredenbregt and
• Yang Li

Beilstein J. Nanotechnol. 2025, 16, 910–920, doi:10.3762/bjnano.16.69

• magnetic or superconductive structures can be created [1][2][3][4]. Also, specific mechanical structures on atomic force microscopy (AFM) cantilevers can be made [5][6]. In the literature, four mechanisms are used to explain the complex process of focused ion beam-induced deposition (FIBID) [5][7]; the

Ar⁺ implantation-induced tailoring of RF-sputtered ZnO films: structural, morphological, and optical properties

• Manu Bura,
• Divya Gupta,
• Arun Kumar and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 872–886, doi:10.3762/bjnano.16.66

• in grazing incidence angle X-ray diffraction patterns. Atomic force microscopy images show grain size reduction and a fall in the surface roughness value of films after implantation. The implantation-induced structural modifications are further correlated with the variation in diffuse reflectance

• using a WITec alpha300 RA Raman spectrometer under excitation with a 532 nm solid-state diode laser operated at 10 mW. The topography of the films is examined using atomic force microscopy (AFM) with a Bruker Multimode 8 instrument. The surface morphology of pristine and implanted films is further

• ) mode both at the Γ and K–M points of the Brillouin zone shows softening and broadening with increasing argon ion fluence. Also, enhancement in peak intensity of both the peaks reveals the increases in lattice defects with increasing ion fluence. Morphological analysis Atomic force microscopy The

Supramolecular hydration structure of graphene-based hydrogels: density functional theory, green chemistry and interface application

• Hon Nhien Le,
• Duy Khanh Nguyen,
• Minh Triet Dang,
• Huyen Trinh Nguyen,
• Thi Bang Tam Dao,
• Trung Do Nguyen,
• Chi Nhan Ha Thuc and
• Van Hieu Le

Beilstein J. Nanotechnol. 2025, 16, 806–822, doi:10.3762/bjnano.16.61

• supramolecular hydration structures that preserve graphene nanosheets from the restacking through hydrophobic force, van der Waals force, and π–π interaction. In this manuscript, density functional theory and high-performance computing (HPC) are used for modeling and calculating van der Waals force between

• graphene nanosheets in water-intercalated AB bilayer graphene structures. A layer of water molecules significantly decreases the intersheet van der Waals force. A novel hydrogel of graphene oxide–silica gel–zinc hydroxide (GO-SG-ZH) is experimentally synthesized to demonstrate the advantages of hydrated

• interactions, a type of van der Waals force, for supramolecular attraction [9]. Particularly, graphene sheets with a large surface area and π-conjugated network are likely to stack together through hydrophobic agglomeration and π–π interaction. Although π–π interactions are generally weaker than hydrogen

Morphology and properties of pyrite nanoparticles obtained by pulsed laser ablation in liquid and thin films for photodetection

• Akshana Parameswaran Sreekala,
• Bindu Krishnan,
• Rene Fabian Cienfuegos Pelaes,
• David Avellaneda Avellaneda,
• Josué Amílcar Aguilar-Martínez and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 785–805, doi:10.3762/bjnano.16.60

• nanoparticle synthesis by PLAL. For instance, it has been reported that the density and viscosity of the surrounding liquid influence the expansion of the plasma plume. The expansion dynamics of the plume differ due to the larger opposing force induced by the increased viscosity of the solvent, which in turn

Thickness dependent oxidation in CrCl₃: a scanning X-ray photoemission and Kelvin probe microscopies study

• Shafaq Kazim,
• Rahul Parmar,
• Maryam Azizinia,
• Matteo Amati,
• Muhammad Rauf,
• Andrea Di Cicco,
• Seyed Javid Rezvani,
• Dario Mastrippolito,
• Luca Ottaviano,
• Tomasz Klimczuk,
• Luca Gregoratti and
• Roberto Gunnella

Beilstein J. Nanotechnol. 2025, 16, 749–761, doi:10.3762/bjnano.16.58

• particular technological interest, even more in the case of chromium trihalides (CrX3, X = Cl, Br, and I), whose longer lifetime under ambient conditions is particularly intriguing. By using synchrotron-based scanning photoelectron microscopy with a resolution of 0.1 μm and Kelvin probe force microscopy, we

• oxidation or the introduction of surface vacancies, a novel and versatile approach is unveiled for the development of low-dimensional multifunctional nanodevices. Keywords: chemical mapping; CrX3; Kelvin probe force microscopy; mechanical exfoliation; scanning photoelectron microscopy (SPEM); two

• correlation between the microscopic results and the surface potential of CrCl3 flakes at the nanoscale level using Kelvin probe force microscopy (KPFM) [28]. KPFM is mainly employed to measure the local contact potential difference between the conductive AFM tip and the sample, allowing for high-resolution

Nanostructured materials characterized by scanning photoelectron spectromicroscopy

• Matteo Amati,
• Alexey S. Shkvarin,
• Alexander I. Merentsov,
• Alexander N. Titov,
• María Taeño,
• David Maestre,
• Sarah R. McKibbin,
• Zygmunt Milosz,
• Ana Cremades,
• Rainer Timm and
• Luca Gregoratti

Beilstein J. Nanotechnol. 2025, 16, 700–710, doi:10.3762/bjnano.16.54

• suitable substrates for characterization by scanning probe microscopy and SPEM. An atomic force microscopy (AFM) image of a typical InP p–n junction nanowire is shown in Figure 2a, confirming a homogeneous shape with a nanowire length of about 2.5 µm and a diameter of about 200 nm, fluctuating only by a