Nanogenerator-based self-powered sensors for data collection

• Yicheng Shao,
• Maoliang Shen,
• Yuankai Zhou,
• Xin Cui,
• Lijie Li and
• Yan Zhang

Beilstein J. Nanotechnol. 2021, 12, 680–693, doi:10.3762/bjnano.12.54

• (MOS) gas sensors, the PENG/TENG-based self-powered gas sensor has a lower power consumption, requires no heating, and exhibits high stability and high sensitivity. In 2013, Xue et al. proposed a ZnO NWs PENG-based self-powered gas sensor [18]. The response of the unpackaged PENG sensor was studied

A review of defect engineering, ion implantation, and nanofabrication using the helium ion microscope

• Frances I. Allen

Beilstein J. Nanotechnol. 2021, 12, 633–664, doi:10.3762/bjnano.12.52

Properties of graphene deposited on GaN nanowires: influence of nanowire roughness, self-induced nanogating and defects

• Jakub Kierdaszuk,
• Piotr Kaźmierczak,
• Justyna Grzonka,
• Aleksandra Krajewska,
• Aleksandra Przewłoka,
• Wawrzyniec Kaszub,
• Zbigniew R. Zytkiewicz,
• Marta Sobanska,
• Maria Kamińska,
• Andrzej Wysmołek and
• Aneta Drabińska

Beilstein J. Nanotechnol. 2021, 12, 566–577, doi:10.3762/bjnano.12.47

• order to reduce the heating effect. The micro-Raman maps were collected with 100 nm steps with a few square micrometres of mapping area for each sample. The spectra were calibrated by using a reference sample of high-quality silicon. Results and Discussion The morphology of graphene deposited on NWs

Local stiffness and work function variations of hexagonal boron nitride on Cu(111)

• Abhishek Grewal,
• Yuqi Wang,
• Matthias Münks,
• Klaus Kern and
• Markus Ternes

Beilstein J. Nanotechnol. 2021, 12, 559–565, doi:10.3762/bjnano.12.46

• acquisition. Sample preparation: A Cu(111) single crystal (MaTeck GmbH) is cleaned via repeated cycles of Ar-ion sputtering at room temperature followed by annealing to 1020 K in an ultrahigh-vacuum preparation chamber. A partial layer of h-BN is grown by chemical vapour deposition by heating the Cu(111

On the stability of microwave-fabricated SERS substrates – chemical and morphological considerations

• Limin Wang,
• Aisha Adebola Womiloju,
• Christiane Höppener,
• Ulrich S. Schubert and
• Stephanie Hoeppener

Beilstein J. Nanotechnol. 2021, 12, 541–551, doi:10.3762/bjnano.12.44

• typical heating process) which initiates the reduction of the silver salt by ethanol. This triggers a short burst of silver nanoparticle nucleation, which forms reaction seeds on the glass substrate. The strong affinity of the silver ions for the free hydroxyl groups of glass surfaces allows for the

• time was fixed to 2 min, which corresponds to the shortest time to yield a sufficient coverage with Ag nanoparticles with high homogeneity and SERS activity [24]. The chosen time of 2 min includes the heating ramp time and an additional cooling time of 2 min was required. Thus, the total microwave

The preparation temperature influences the physicochemical nature and activity of nanoceria

• Robert A. Yokel,
• Wendel Wohlleben,
• Johannes Georg Keller,
• Matthew L. Hancock,
• Jason M. Unrine,
• D. Allan Butterfield and
• Eric A. Grulke

Beilstein J. Nanotechnol. 2021, 12, 525–540, doi:10.3762/bjnano.12.43

• nanoceria, described in Supporting Information File 1, Table S1, were calcined by heating in porcelain crucibles in a muffle furnace to 900 °C at a ramp rate of ca. 10 °C/min, then held for 3 h. The product was characterized by electron microscopy performed on the Thermo Scientific Talos F200X described

Boosting of photocatalytic hydrogen evolution via chlorine doping of polymeric carbon nitride

• Malgorzata Aleksandrzak,
• Michalina Kijaczko,
• Wojciech Kukulka,
• Daria Baranowska,
• Martyna Baca,
• Beata Zielinska and
• Ewa Mijowska

Beilstein J. Nanotechnol. 2021, 12, 473–484, doi:10.3762/bjnano.12.38

• direct heating of melamine. A given amount of melamine was placed in a covered crucible in a muffle furnace and heated in static air to 550 °C with a ramping rate of 4 °C/min and then was held at 550 °C for 4 h. After the reaction, the furnace was cooled down to room temperature. The obtained PCN was

Rapid controlled synthesis of gold–platinum nanorods with excellent photothermal properties under 808 nm excitation

• Jialin Wang,
• Qianqian Duan,
• Min Yang,
• Boye Zhang,
• Li Guo,
• Pengcui Li,
• Wendong Zhang and
• Shengbo Sang

Beilstein J. Nanotechnol. 2021, 12, 462–472, doi:10.3762/bjnano.12.37

• during heating [15][16]. Pt nanoparticles have better light and thermal stability then Au nanoparticles [17]. Au–Pt bimetal nanoparticles may not only further enrich the functions of nanostructures, but the spatial distribution of both elements also plays an important role in adjusting the properties

• heating. The Au@Pt NRs solution exhibits a stronger thermal response than AuNRs with the same amount of Au. Due to the fact that the LSPR of Au@Pt NRs is closer to 808 nm and has a wider band, it absorbs more photon energy and releases more heat. Next, to explore the influence of laser power on the

• @Pt NRs solution (OD = 0.5) under different laser power densities (10 min). (d) Temperature elevation curves of Au@Pt NRs solution with different OD under 808 nm laser irradiation (2.0 W/cm2, 10 min). Heating and cooling curves of (a) AuNRs and (c) Au@Pt NRs under 808 nm laser irradiation. Linear fit

Nickel nanoparticle-decorated reduced graphene oxide/WO₃ nanocomposite – a promising candidate for gas sensing

• Ilka Simon,
• Alexandr Savitsky,
• Rolf Mülhaupt,
• Vladimir Pankov and
• Christoph Janiak

Beilstein J. Nanotechnol. 2021, 12, 343–353, doi:10.3762/bjnano.12.28

• Ni@rGO composite without heat treatment. The temperature dependence of the magnetization was determined during several heating–cooling cycles. It was noted that with an increase in the number of cycles, the Сurie temperature of the sample increased from 345 to 357 °C. Most likely, the increase in the

The patterning toolbox FIB-o-mat: Exploiting the full potential of focused helium ions for nanofabrication

• Victor Deinhart,
• Lisa-Marie Kern,
• Jan N. Kirchhof,
• Sabrina Juergensen,
• Joris Sturm,
• Enno Krauss,
• Thorsten Feichtner,
• Sviatoslav Kovalchuk,
• Michael Schneider,
• Dieter Engel,
• Bastian Pfau,
• Bert Hecht,
• Kirill I. Bolotin,
• Stephanie Reich and
• Katja Höflich

Beilstein J. Nanotechnol. 2021, 12, 304–318, doi:10.3762/bjnano.12.25

• region exhibits temperatures around 800 K while the bridges stay close to room temperature. The resonance frequency of the fundamental mode is 12.5 MHz (cf. Figure 6b) and exhibits a quality factor of about 300 without laser heating. When suspended graphene is heated by a light source, the built-in

Doxorubicin-loaded gold nanorods: a multifunctional chemo-photothermal nanoplatform for cancer management

• Uzma Azeem Awan,
• Abida Raza,
• Shaukat Ali,
• Rida Fatima Saeed and
• Nosheen Akhtar

Beilstein J. Nanotechnol. 2021, 12, 295–303, doi:10.3762/bjnano.12.24

• DOX release at different pH values. Fluorescence intensity was measured from 0 to 30 h. (b) Heating curves of water, PSS GNRs and PSS-GNRs-DOX (10 µg Au/mL) under NIR (808 nm) laser irradiation. (a) Relative viabilities of HepG2 and 3T3 cells after being incubated with different concentrations of PSS

Gold(I) N-heterocyclic carbene precursors for focused electron beam-induced deposition

• Cristiano Glessi,
• Aya Mahgoub,
• Cornelis W. Hagen and
• Mats Tilset

Beilstein J. Nanotechnol. 2021, 12, 257–269, doi:10.3762/bjnano.12.21

• Sublimation temperatures for compounds 1–7 were obtained by cold finger sublimation. The cold finger sublimation setup was immersed in an oil bath and heated by a heating plate. The temperature was controlled and registered by an immersion thermometer immersed in the oil bath at the same height as the bulk

• material and connected to the heating plate. The pressure measured for each experiment was 1 × 10−3 mbar on a VACUU.VIEW or DCP 3000 Vacuubrand manometer mounted on the Schlenk line used. The cold finger was cooled down with continuous water flow. 20 ± 1.5 mg of bulk material were charged in the

• sublimation apparatus, which was then evacuated and conditioned with Ar or N2 before being evacuated again. The dynamic heating of the sample was carried out at a heating rate of 1 K per 10 min. The sublimation temperature was determined as the point at which the formation of a white film was observed on the

Scanning transmission helium ion microscopy on carbon nanomembranes

• Daniel Emmrich,
• Annalena Wolff,
• Nikolaus Meyerbröker,
• Jörg K. N. Lindner,
• André Beyer and
• Armin Gölzhäuser

Beilstein J. Nanotechnol. 2021, 12, 222–231, doi:10.3762/bjnano.12.18

• nanocrystalline graphene upon heating [25]. It was observed that this comes with a loss of atoms, which is also apparent in this experiment by the decreasing membrane thickness (see Figure 7a). The results from both methods, XPS and EFTEM, confirm the thickness measurement by STIM. While XPS and STIM are close

Paper-based triboelectric nanogenerators and their applications: a review

• Jing Han,
• Nuo Xu,
• Yuchen Liang,
• Mei Ding,
• Junyi Zhai,
• Qijun Sun and
• Zhong Lin Wang

Beilstein J. Nanotechnol. 2021, 12, 151–171, doi:10.3762/bjnano.12.12

• conductivity. VF is a simple and rapid method to cast functional materials onto solution-processable substrates without the need to implement any time-consuming and high-cost processes (e.g., evacuation, thermal/e-beam heating, and radio-frequency sputtering). The conductivity is also easily adjustable by

A review on the green and sustainable synthesis of silver nanoparticles and one-dimensional silver nanostructures

• Sina Kaabipour and
• Shohreh Hemmati

Beilstein J. Nanotechnol. 2021, 12, 102–136, doi:10.3762/bjnano.12.9

• [143][231]. In most cases, AgNPs are synthesized in metal oxide thin films such as TiO2, SiO2, and ZrO2 where the average particle size is almost 10 nm when the heating temperature is 600 °C in the case of SiO2 thin films, and 500 °C in the case of TiO2 and ZrO2 [231]. Arun Kumar et al. [145

• the gas phase to the reactor chamber. Second, adsorption of the vapor on the substrate surface and establishment of medium compounds followed by formation of a layer. Third, nucleation and growth of the layer through heating [241]. The important factors that control the process and size of synthesized

The role of gold atom concentration in the formation of Cu–Au nanoparticles from the gas phase

• Yuri Ya. Gafner,
• Svetlana L. Gafner,
• Darya A. Ryzkova and
• Andrey V. Nomoev

Beilstein J. Nanotechnol. 2021, 12, 72–81, doi:10.3762/bjnano.12.6

• heating of Cu3Au nanoclusters, typical changes called “order–disorder transition” occur in the nanocluster structure, leading to the decomposition of the initial L12 crystal structure. This leads to a transition to the FCC structure with a random atomic distribution in the long-range coordination spheres

Effect of different silica coatings on the toxicity of upconversion nanoparticles on RAW 264.7 macrophage cells

• Cynthia Kembuan,
• Helena Oliveira and
• Christina Graf

Beilstein J. Nanotechnol. 2021, 12, 35–48, doi:10.3762/bjnano.12.3

• (30% v/v) were added, respectively. The mixture was stirred overnight under argon atmosphere, followed by heating under reflux for 1 h. For the particles with thicker silica coating, 1.5 mL (c = 20 g/L in ethanol, particle mass = 30 mg) of the dispersion was diluted to c = 1 g/L and reacted with 25 µL

Free and partially encapsulated manganese ferrite nanoparticles in multiwall carbon nanotubes

• Saja Al-Khabouri,
• Salim Al-Harthi,
• Toru Maekawa,
• Mohamed E. Elzain,
• Ashraf Al-Hinai,
• Ahmed D. Al-Rawas,
• Abbsher M. Gismelseed,
• Ali A. Yousif and
• Myo Tay Zar Myint

Beilstein J. Nanotechnol. 2020, 11, 1891–1904, doi:10.3762/bjnano.11.170

• analyzer transmission energy of 50 eV, while the individual elemental peaks were recorded at an analyzer pass energy of 20 eV. All XPS measurements were carried out at room temperature and no heating was performed prior to the XPS measurement. The obtained XPS spectra were deconvoluted using the CasaXPS

Nanocasting synthesis of BiFeO₃ nanoparticles with enhanced visible-light photocatalytic activity

• Thomas Cadenbach,
• Maria J. Benitez,
• A. Lucia Morales,
• Cesar Costa Vera,
• Luis Lascano,
• Francisco Quiroz,
• Alexis Debut and
• Karla Vizuete

Beilstein J. Nanotechnol. 2020, 11, 1822–1833, doi:10.3762/bjnano.11.164

• -methoxyethanol as a solvent, the effect of different molar ratios between the Bi/Fe metal precursors was then analyzed, since significant bismuth loss can be observed during calcination as bismuth is volatile at high temperatures. Thus, it is necessary to compensate for this loss during the heating step by

• heating. In addition, the presence of Bi3+ in acidic aqueous solutions leads to the formation of polynuclear cationic species. Once a thermal treatment at 500 °C is applied, those clusters decompose into α- and β-Bi2O3 by-products, which are not observed when an intermediate heating step is carried out

Self-standing heterostructured NiC_x-NiFe-NC/biochar as a highly efficient cathode for lithium–oxygen batteries

• Shengyu Jing,
• Xu Gong,
• Shan Ji,
• Linhui Jia,
• Bruno G. Pollet,
• Sheng Yan and
• Huagen Liang

Beilstein J. Nanotechnol. 2020, 11, 1809–1821, doi:10.3762/bjnano.11.163

• were washed with ethanol and water alternatively and calcined at a certain temperature for 2 h with a heating ramp of 5 °C·min−1 in a tube furnace in nitrogen atmosphere. The calcined samples were labeled as NiFe-PBA/PP-T. Physical characterization X-ray diffraction (XRD) patterns were recorded using a

Electron beam-induced deposition of platinum from Pt(CO)₂Cl₂ and Pt(CO)₂Br₂

• Aya Mahgoub,
• Hang Lu,
• Rachel M. Thorman,
• Konstantin Preradovic,
• Titel Jurca,
• Lisa McElwee-White,
• Howard Fairbrother and
• Cornelis W. Hagen

Beilstein J. Nanotechnol. 2020, 11, 1789–1800, doi:10.3762/bjnano.11.161

• likely indicative that prolonged heating at 90 °C will result in precursor decomposition (Figure 2a,b). Conversely, for Pt(CO)2Br2, prolonged heating at 90 °C facilitated a greater degree of sublimation vs decomposition whereupon approximately 29% of the original mass remained (Figure 2b,c). This is

• reasonably below the initial Pt content of 47.5%. The TGA studies indicate that Pt(CO)2Br2 is more stable under prolonged heating, leading to increased volatility, but Pt(CO)2Cl2 is more efficient under a faster ramped-temperature process (10 °C/min). Precursor gas properties Precursor crucible temperature

Direct observation of the Si(110)-(16×2) surface reconstruction by atomic force microscopy

• Tatsuya Yamamoto,
• Ryo Izumi,
• Kazushi Miki,
• Takahiro Yamasaki,
• Yasuhiro Sugawara and
• Yan Jun Li

Beilstein J. Nanotechnol. 2020, 11, 1750–1756, doi:10.3762/bjnano.11.157

• zig-zag chains extend) was not related to the direction of current during sample heating, which is consistent with previous studies [12][22]. In the step area, two types of typical facets were observed: (17 15 1) and (15 17 1) [12][16] extending in the directions of and , respectively, which are

Seebeck coefficient of silicon nanowire forests doped by thermal diffusion

• Shaimaa Elyamny,
• Elisabetta Dimaggio and
• Giovanni Pennelli

Beilstein J. Nanotechnol. 2020, 11, 1707–1713, doi:10.3762/bjnano.11.153

• electrical power needed to heat TH through Joule heating is the thermal power = V × I that crosses the sample in the absence of heat losses. The system is in vacuum and the irradiation loss is limited by a thermal shield maintained at TH. Hence, the thermal resistance ℜ can be evaluated as ℜ = (TH − TC

• of the contact thermal resistance ℜCA, together with the value of the heat flux through the sample = V × I, can be used for a correct evaluation of ΔTNW: For each sample, several Seebeck voltage values Vseebeck have been recorded for different heating power values , that is, for different values of

Out-of-plane surface patterning by subsurface processing of polymer substrates with focused ion beams

• Serguei Chiriaev,
• Luciana Tavares,
• Vadzim Adashkevich,
• Arkadiusz J. Goszczak and
• Horst-Günter Rubahn

Beilstein J. Nanotechnol. 2020, 11, 1693–1703, doi:10.3762/bjnano.11.151

• ions and materials, such as structural damage and chemical modification that affect functional properties of the near-surface layers, are substantially reduced in comparison to FIB milling. Another advantage of the subsurface processing is that the local heating is negligible in comparison to ion

The influence of an interfacial hBN layer on the fluorescence of an organic molecule

• Christine Brülke,
• Oliver Bauer and
• Moritz M. Sokolowski

Beilstein J. Nanotechnol. 2020, 11, 1663–1684, doi:10.3762/bjnano.11.149

• . The sample was annealed in iterative steps of heating, holding at a constant temperature for 3 min, and cooling down again to 20 K for a measurement. The annealing temperatures were in the range of 100–400 K and are specified below. In the following, one monolayer (ML) of PTCDA refers to a single