Structural and magnetic properties of microwave-synthesized reduced graphene oxide/VO₂/Fe₂O₃ nanocomposite

• Sumanta Sahoo,
• Ankur Sood and
• Sung Soo Han

Beilstein J. Nanotechnol. 2025, 16, 921–932, doi:10.3762/bjnano.16.70

• the NCs. The Raman spectra of rGO and the related NCs were recorded through the “XploRA plus HORIBA” instrument with a laser excitation of 532 nm. Additionally, the surface analysis was performed using X-ray photoelectron spectroscopy measurements (XPS, Thermofisher Scientific) functioning at 12 kV

• graphene [33][34][35]. The presence of rGO in the GV and GVF was further confirmed by the Raman spectra (Figure 3c). As shown, the peaks at ≈1350 and ≈1580 cm−1 correspond to the characteristic D and G bands of graphene. Interestingly, minor changes in the peak positions of these two characteristic peaks

• components caused more disorder and defects in the carbon structure [36]. Furthermore, the peak at ≈2700 cm−1 represents the characteristic 2D band of graphene. The Raman pattern of rGO represents such characteristic D band at ≈1343 cm−1, G band at ≈1582.4 cm−1, and 2D band at ≈2690 cm−1, respectively

Heat-induced transformation of nickel-coated polycrystalline diamond film studied in situ by XPS and NEXAFS

• Olga V. Sedelnikova,
• Yuliya V. Fedoseeva,
• Dmitriy V. Gorodetskiy,
• Yuri N. Palyanov,
• Elena V. Shlyakhova,
• Eugene A. Maksimovskiy,
• Anna A. Makarova,
• Lyubov G. Bulusheva and
• Aleksandr V. Okotrub

Beilstein J. Nanotechnol. 2025, 16, 887–898, doi:10.3762/bjnano.16.67

• crystallites; however, the layer defectiveness increased in areas with fine-dispersed crystallites. According to NEXAFS and Raman spectroscopy data, the most ordered atomic structure of graphitic layers was obtained by annealing nickel-coated SCD. The angular dependence of NEXAFS C K-edge spectra of nickel

• . Additionally, angle-resolved NEXAFS spectra of annealed Ni-coated SCD were measured to reveal the orientation of the formed graphitic layers. After synchrotron measurements, the samples were exposed to air and further analyzed using Raman spectroscopy and scanning electron microscopy (SEM). The obtained

• crystallites and the rough PCD film. Various growth defects, including pits, cracks, steps, and protrusions are present on the diamond faces. The secondary nucleation of diamond caused the formation of submicron-sized diamond grains and smoothing of the shape of large crystals. Raman spectroscopy revealed high

Ar⁺ implantation-induced tailoring of RF-sputtered ZnO films: structural, morphological, and optical properties

• Manu Bura,
• Divya Gupta,
• Arun Kumar and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 872–886, doi:10.3762/bjnano.16.66

• . Raman spectra reveal the presence of the E2 (low), E2 (high), and A1 (LO) Raman modes in pristine and implanted ZnO films. A gradual fall and rise in peak intensity of, respectively, the E2 (high) and A1 (LO) Raman modes is observed with increases in ion fluence. However, the E2 (low) mode broadens and

• merges completely with disorder-induced broad band at higher fluences. Moreover, the deconvolution of the A1 (LO) Raman peak affirms the presence of defect-related Raman modes in the implanted samples. A gradual reduction in crystallinity of the implanted ZnO films with increasing ion fluence is observed

• , defects, and interstitials are induced through the interaction between energetic ions and the host material, resulting in structural modification and thus alteration in lattice dynamics of the host material [10]. The implantation-induced disorder can be qualitatively examined using Raman spectroscopy

Synchrotron X-ray photoelectron spectroscopy study of sodium adsorption on vertically arranged MoS₂ layers coated with pyrolytic carbon

• Alexander V. Okotrub,
• Anastasiya D. Fedorenko,
• Anna A. Makarova,
• Veronica S. Sulyaeva,
• Yuliya V. Fedoseeva and
• Lyubov G. Bulusheva

Beilstein J. Nanotechnol. 2025, 16, 847–859, doi:10.3762/bjnano.16.64

• SEM image of PyC transferred onto the SiO2/Si substrate also shows a uniform film surface (Figure 1e). The Raman spectrum of the MoS2 film contains two strong peaks at 382.6 and 408.9 cm−1 (Figure 2a) corresponding to the E12g mode and the A1g mode, respectively, of 2H-MoS2 [33]. The difference

• realized only when they are oriented vertically to the substrate surface. The weak peak at about 280 cm−1 observed in the Raman spectrum corresponds to the E1g mode, which is forbidden when the laser beam is incident perpendicularly on the c axis of MoS2 [36]. The activation of this mode in our case

• Raman spectrum of the PyC-MoS2 sample, so the coating with PyC film does not destroy the structure of the MoS2 film. The Raman spectra of PyC and PyC-MoS2 show a peak at 1600 cm−1 corresponding to the in-plane stretching of C=C bonds (G mode) and a peak at 1355 cm−1 caused by the disorder in the

Facile one-step radio frequency magnetron sputtering of Ni/NiO on stainless steel for an efficient electrode for hydrogen evolution reaction

• Ha Huu Do,
• Khac Binh Nguyen,
• Phuong N. Nguyen and
• Hoai Phuong Pham

Beilstein J. Nanotechnol. 2025, 16, 837–846, doi:10.3762/bjnano.16.63

• exhibited a moderate O2 content (11.96 wt %), which could bring the highest HER efficiency. The Ni/NiO ratio is the most crucial parameter in the Ni/NiO catalyst system, influencing the electrode’s HER efficiency, which Yan and coworkers proved [18]. The Raman spectrum of the Ni/NiO/SS-10 electrode

• displayed the prominent peaks shown in Figure 3. The bands at 200 to 600 cm−1 represent one phonon (1P), whereas the bands at 650 to 1100 cm−1 could be assigned to two phonons (2P) of NiO species in the electrode. In particular, the Raman peak at 552 cm−1 was indexed into the 1P longitudinal optical (LO

• distribution in materials were studied using EDX. The Raman spectra were studied using a LabRAM-HR Evolution Raman microscope with a laser wavelength of 532 nm. The composition of the thin films was investigated using XPS on a Thermo Scientific K-Alpha XPS system. Electrochemical measurements The HER catalytic

Changes of structural, magnetic and spectroscopic properties of microencapsulated iron sucrose nanoparticles in saline

• Sabina Lewińska,
• Pavlo Aleshkevych,
• Roman Minikayev,
• Anna Bajorek,
• Mateusz Dulski,
• Krystian Prusik,
• Tomasz Wojciechowski and
• Anna Ślawska-Waniewska

Beilstein J. Nanotechnol. 2025, 16, 762–784, doi:10.3762/bjnano.16.59

• AC) performed on the undissolved sample revealed the presence of a low temperature blocking process ( ≈ 10 K), and confirmed its superparamagnetic state between 70– 250 K. X-ray photoelectron spectroscopy and Raman studies showed a varied composition of the undissolved sample in which organic

• transmission electron microscopy (TEM). Composition studies using XRD, magnetic properties using dc and ac magnetometry, and extensive spectral analysis using Fourier-transform infrared spectroscopy (FTIR), Raman, and electron paramagnetic resonance (EPR) were also performed. Considering that the AB-Fortis

• proved that most likely the cores of the nanoparticles are composed of FeO(OH). However, the results of the magnetic measurements do not allow resolving the issues related to the type of FeO(OH) polymorph. Therefore, additional studies such as FTIR, Raman, and XPS were performed, and their results will

Nanostructured materials characterized by scanning photoelectron spectromicroscopy

• Matteo Amati,
• Alexey S. Shkvarin,
• Alexander I. Merentsov,
• Alexander N. Titov,
• María Taeño,
• David Maestre,
• Sarah R. McKibbin,
• Zygmunt Milosz,
• Ana Cremades,
• Rainer Timm and
• Luca Gregoratti

Beilstein J. Nanotechnol. 2025, 16, 700–710, doi:10.3762/bjnano.16.54

• , were considered to occur during the growth process, leading to NiO samples with variable properties. Raman spectroscopy indicated changes between the relative intensity of first order modes and the 2M mode due to the variable lattice disorder induced in the samples during the growth process

Colloidal few layered graphene–tannic acid preserves the biocompatibility of periodontal ligament cells

• Teissir Ben Ammar,
• Naji Kharouf,
• Dominique Vautier,
• Housseinou Ba,
• Nivedita Sudheer,
• Philippe Lavalle and
• Vincent Ball

Beilstein J. Nanotechnol. 2025, 16, 664–677, doi:10.3762/bjnano.16.51

• S1B, Supporting Information File 1) shows that they are spherical and that they remodel into clusters on the surface. Raman spectra recorded for the initial graphite and the synthesized FLG–TA exhibits typical D, G, and 2D vibration bands centered at 1355, 1583, and 2720 cm−1, respectively. It is

• FLG–TA has a low defect content, evidenced by its weak D peak. Although the absorption of carbonyl functions in TA molecules might influence the defect ratio for FLG–TA because of the increase in the G peak (Figure S2, Supporting Information File 1, shows the Raman spectrum of TA powder), it remains

• provided DPPH (Figure S4B0–B2 of Supporting Information File 1). These findings indicate significant oxygen enrichment due to TA adsorption on FLG sheets, supporting earlier Raman spectroscopy results and colloidal stability observations (Figure S3A1, Supporting Information File 1). Both free and adsorbed

Feasibility analysis of carbon nanofiber synthesis and morphology control using a LPG premixed flame

• Iftikhar Rahman Bishal,
• Muhammad Hilmi Ibrahim,
• Norikhwan Hamzah,
• Mohd Zamri Mohd Yusop,
• Faizuan Bin Abdullah,
• I Putu Tedy Indrayana and
• Mohd Fairus Mohd Yasin

Beilstein J. Nanotechnol. 2025, 16, 581–590, doi:10.3762/bjnano.16.45

• nucleation rate, which in turn increases the catalyst particle size and the amount of free carbon atoms, producing CNFs with larger diameters and amorphous carbon. According to Raman analysis, the grown CNFs have a high number of defects, which may be good for applications where defective nanomaterials are

• room temperature, the product was purified with 1% HCl solution, distilled water, and ethanol, then vacuum-dried at 50 °C for about 4 h. The final product was nearly pure CNFs, as shown by FESEM images. TEM images indicated an average CNF diameter of 100 nm. Raman spectra showed a strong, narrow peak

• revealed nanofiber morphology, and Raman spectroscopy showed the characteristic IG and ID bands of CNFs [18]. Catalytic chemical vapor deposition was conducted by Hammel et al. to synthesize CNFs using a tube furnace. The experiment used a nickel-based catalyst and diluted acetylene as the source of carbon

Retrieval of B1 phase from high-pressure B2 phase for CdO nanoparticles by electronic excitations in Cd_xZn_1−xO composite thin films

• Arkaprava Das,
• Marcin Zając and
• Carla Bittencourt

Beilstein J. Nanotechnol. 2025, 16, 551–560, doi:10.3762/bjnano.16.43

• irradiated thin films was performed with X-ray diffraction and Raman spectroscopy. Additionally, X-ray absorption near-edge structure (XANES) spectroscopy was conducted at the Zn L3,2 and O K edges for all the thin films. X-ray photoelectron spectroscopy (XPS) on Si 2p and O 1s core levels provided direct

• film prior to further irradiation. The characterization of the thin films was performed using X-ray diffraction (XRD) on a Bruker high-resolution X-ray diffractometer, employing a Cu Kα beam over a 2θ range of 30–50°. Raman spectroscopic measurements were conducted at room temperature with a SENTERRA

• mode. Table 1 summarizes the irradiation ion energies and fluences for each thin film, along with their corresponding labels. Results and Discussion Influence of Ag and O ion irradiation on crystallographic phase by X-ray diffraction and Raman spectroscopy Figure 1a shows the XRD patterns illustrating

Functionalized gold nanoflowers on carbon screen-printed electrodes: an electrochemical platform for biosensing hemagglutinin protein of influenza A H1N1 virus

• Carlos Enrique Torres-Méndez,
• Sharmilee Nandi,
• Klara Martinovic,
• Patrizia Kühne,
• Yifan Liu,
• Sam Taylor,
• Maria Lysandrou,
• Maria Ines Berrojo Romeyro Mascarenhas,
• Viktoria Langwallner,
• Javier Enrique Sebastián Alonso,
• Ivana Jovanovic,
• Maike Lüftner,
• Georgia-Vasiliki Gkountana,
• David Bern,
• Abdul-Raouf Atif,
• Ehsan Manouchehri Doulabi,
• Gemma Mestres and
• Masood Kamali-Moghaddam

Beilstein J. Nanotechnol. 2025, 16, 540–550, doi:10.3762/bjnano.16.42

• nanohybrids of MoSe2−CsPbBr3 with a size range between 60 and 80 nm [38]. This effect has been relevant to enhance the Raman scattering vibrational modes in surface-enhanced Raman spectroscopy measurements. It has also been noticed that the shape of the nanostructure can be used to tune the magnitude of the

Quantification of lead through rod-shaped silver-doped zinc oxide nanoparticles using an electrochemical approach

• Ravinder Lamba,
• Gaurav Bhanjana,
• Neeraj Dilbaghi,
• Vivek Gupta and
• Sandeep Kumar

Beilstein J. Nanotechnol. 2025, 16, 422–434, doi:10.3762/bjnano.16.33

• . Raman spectroscopy of Ag@ZnO nanorods The influence of Ag doping in ZnO nanorods were investigated by Raman scattering. Raman scattering of Ag@ZnO NRs were recorded using a 532 nm laser at room temperature in the spectra range varying from 0 to 2000 cm−1. ZnO has four atoms in each primitive cell, which

• results in 12 degrees of freedom (three acoustic phonon modes and nine optical phonon modes). Figure 6 demonstrates the Raman spectra of Ag@ZnO NRs; when doping is done in ZnO, there is a significant change in the optical and non-optical modes of ZnO. The collapse of the translational crystal symmetry is

• region of the Brillouin zone. Oxygen vacancies are commonly linked to the A1(LO) phonon mode. The presence of a small peak at 218 cm−1 denotes the radial movement of Ag atoms. Raman peaks at around 356 cm−1 are specifically attributed to the A1(TO) mode. Also, the results of Ag doping in ZnO coincide

Graphene oxide–chloroquine conjugate induces DNA damage in A549 lung cancer cells through autophagy modulation

• Braham Dutt Arya,
• Sandeep Mittal,
• Prachi Joshi,
• Alok Kumar Pandey,
• Jaime E. Ramirez-Vick,
• Govind Gupta and
• Surinder P. Singh

Beilstein J. Nanotechnol. 2025, 16, 316–332, doi:10.3762/bjnano.16.24

• quantitative estimation of the unbound drug. Physical characterization techniques The functional group and structural analysis of GO and GO–Chl nanoconjugate were studied using a Fourier-transform infrared spectrometer (Cary 630 FTIR, Agilent, CA, USA) in ATR mode and a Raman spectrophotometer (Ranishaw win

• , Raman spectroscopy was utilized to evaluate the formation of GO (after the oxidation of graphite powder) and the GO–Chl nanoconjugate. The structural properties of graphite and GO nanosheets were investigated through the comprehensive analysis of the characteristic graphitic domain band (G band) and

• defect band (D band) in the Raman spectra (recorded at an excitation wavelength of 514 nm) of the compounds. Supporting Information File 1, Figure S1c reveals the appearance of the G band (1581 cm−1) and D band (1352 cm−1) for graphite, corresponding to the E2g symmetric vibrations associated with the

Radiosensitizing properties of dual-functionalized carbon nanostructures loaded with temozolomide

• Radmila Milenkovska,
• Nikola Geskovski,
• Dushko Shalabalija,
• Ljubica Mihailova,
• Petre Makreski,
• Dushko Lukarski,
• Igor Stojkovski,
• Maja Simonoska Crcarevska and
• Kristina Mladenovska

Beilstein J. Nanotechnol. 2025, 16, 229–251, doi:10.3762/bjnano.16.18

• characterization of all formulations regarding interactions of the components and their stability during the preparation procedures, different techniques were used including infrared (IR), ultraviolet–visible (UV–vis), and Raman spectroscopy as well as TGA. For analyzing potential structural changes in the CNs

• blank CNs indicate that the structure of TMZ was preserved during irradiation. Upon its incorporation in the CNs, in vitro dissolution studies, in which UV–vis spectra of TMZ after its release from the irradiated CNs were recorded, were carried out. Raman spectroscopy The Raman spectra of single- and

• of the CNTs; the bands from the Raman modes that result from the vibration of all carbon atoms in the CNTs; and the 2D band occurring between 2600 and 2800 cm−1, which is sensitive to the number of graphene layers and their arrangement. The intensity ratio between the D and the G band was analyzed

Natural nanofibers embedded in the seed mucilage envelope: composite hydrogels with specific adhesive and frictional properties

• Agnieszka Kreitschitz and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2024, 15, 1603–1618, doi:10.3762/bjnano.15.126

• impossible. The complicated preparation procedures and analysis give us often an information limited to just one factor, for example, to specific chemical composition or topology (AFM, FTIR, or Raman microscopy) [45]. Ideally, the comparison of data from diverse visualisation techniques can provide us with

Facile synthesis of size-tunable L-carnosine-capped silver nanoparticles and their role in metal ion sensing and catalytic degradation of p-nitrophenol

• Akash Kumar,
• Ridhima Chadha,
• Abhishek Das,
• Nandita Maiti and
• Rayavarapu Raja Gopal

Beilstein J. Nanotechnol. 2024, 15, 1576–1592, doi:10.3762/bjnano.15.124

• , and Raman spectroscopy, as well as EDX and XRD revealed controlled aggregation, successful capping, and crystalline growth of the ʟ-car-AgNPs. The ʟ-car-AgNPs exhibited promising sensing capabilities with limits of detection of 141.79 ppb (1.2 μM) for Cd2+, 131.33 ppb (0.63 μM) for Pb2+, 215.35 ppb

• Raman spectra of ʟ-carnosine-capped silver nanoparticles, as well as ʟ-carnosine, as solid and in aqueous solution, were recorded at RT using an excitation source of 532 nm. The light source was a diode-pumped solid-state Nd3+:YAG laser (Cobolt Samba 0532-01-0500-500, Cobolt AB, Sweden). For solid ʟ

• -carnosine and ʟ-car-AgNPs, powdered samples were placed on glass slides, and the Raman signal was collected in a backscattering geometry using a 50× long working distance objective. The incident laser of approximately 10 mW power had a spot size of approximately 50 μm on the sample surface. Aqueous ʟ

Strain-induced bandgap engineering in 2D ψ-graphene materials: a first-principles study

• Kamal Kumar,
• Nora H. de Leeuw,
• Jost Adam and
• Abhishek Kumar Mishra

Beilstein J. Nanotechnol. 2024, 15, 1440–1452, doi:10.3762/bjnano.15.116

• ), and density functional theory (DFT) study suggests that the hydrogenation of graphene with atomic hydrogen leads to the formation of graphone [8]. The full hydrogenation of graphene (graphane) was experimentally obtained by Elias et al., and their TEM and Raman spectroscopy results evidence the

• using different experimental techniques is available. Ni et al. synthesized graphene on a polyethylene terephthalate (PET) substrate and studied the effect of uniaxial strain through Raman spectroscopy [30]. They stretched PET in one direction and found a redshift in the D and G bands for a single

Various CVD-grown ZnO nanostructures for nanodevices and interdisciplinary applications

• The-Long Phan,
• Le Viet Cuong,
• Vu Dinh Lam and
• Ngoc Toan Dang

Beilstein J. Nanotechnol. 2024, 15, 1390–1399, doi:10.3762/bjnano.15.112

• annealing Zn powder under atmospheric pressure conditions, we collected nanocrystals with various morphologies, including rods, pencils, sheets, combs, tetrapods, and multilegs. Raman scattering study reveals that the samples are monophasic with a hexagonal structure, and fall into the P63mc space group

• results prove that ZnO exhibits many novel nanostructures that can foster the development of next-generation optoelectronic nanodevices and new applications in biological and biomedical fields. Keywords: chemical vapour deposition; electron microscopy; Raman and photoluminescent spectra; ZnO

• nanostructures [23][35][36]. Our current work uses this simple method to grow ZnO nanostructures. After fabrication, the crystal quality of nanostructures is assessed through Raman scattering (RS) and photoluminescent (PL) measurements at room temperature. Experimental As mentioned above, CVD was utilized to

Green synthesis of carbon dot structures from Rheum Ribes and Schottky diode fabrication

• Muhammed Taha Durmus and
• Ebru Bozkurt

Beilstein J. Nanotechnol. 2024, 15, 1369–1375, doi:10.3762/bjnano.15.110

• synthesis, which is commonly used in the literature. TEM and zeta potential measurements were used to determine morphology and sizes of the CDs, and XRD, XPS, and FTIR and micro-Raman spectroscopy were used for structural characterization. Optical characterization of the CDs was done by absorption and

• Cary Eclipse fluorescence spectrophotometer were used for transmission electron microscopy (TEM), zeta potential measurements, X-ray diffractometry (XRD), Fourier-transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), micro-Raman spectroscopy, PVD thermal evaporation, scanning

• . The FTIR and XPS results are in agreement. Raman spectroscopy was also carried out to confirm the presence of aromatic carbon atoms in the newly synthesized CDs. The D band was observed at 1150 cm−1, and the G band was observed at 1519 cm−1 (Figure 2f). The D band is associated with defects in the

Out-of-plane polarization induces a picosecond photoresponse in rhombohedral stacked bilayer WSe₂

• Guixian Liu,
• Yufan Wang,
• Zhoujuan Xu,
• Zhouxiaosong Zeng,
• Lanyu Huang,
• Cuihuan Ge and
• Xiao Wang

Beilstein J. Nanotechnol. 2024, 15, 1362–1368, doi:10.3762/bjnano.15.109

• . To enrich the basic characterizations of WSe2, we conducted Raman spectroscopy and scanning electron microscopy (SEM) measurements (Supporting Information File 1, Note 5). The broken symmetry leads to an asymmetric distribution of photogenerated carriers, resulting in a non-zero photocurrent even

• probe power. (d) Photoresponse intensity of heterojunction (red dots) and graphene region (black dots) as a function of probe power. Supporting Information Supporting Information File 20: Characterization of structure, SHG image, SEM and EDS images, Raman and PL spectrum of WSe2 and raw TRPC curves for

Nanoarchitectonics with cetrimonium bromide on metal nanoparticles for linker-free detection of toxic metal ions and catalytic degradation of 4-nitrophenol

• Akash Kumar and
• Raja Gopal Rayavarapu

Beilstein J. Nanotechnol. 2024, 15, 1312–1332, doi:10.3762/bjnano.15.106

• spectroscopy, atomic emission spectroscopy, surface-enhanced Raman scattering, electrochemical, fluorescence, and colorimetric methods [18][19]. Catalytic hydrogenation is the preferred method for the conversion of 4-nitrophenol to 4-aminophenol, which is less toxic [20]. However, the conversion process is

Interaction of graphene oxide with tannic acid: computational modeling and toxicity mitigation in C. elegans

• Romana Petry,
• James M. de Almeida,
• Francine Côa,
• Felipe Crasto de Lima,
• Diego Stéfani T. Martinez and
• Adalberto Fazzio

Beilstein J. Nanotechnol. 2024, 15, 1297–1311, doi:10.3762/bjnano.15.105

• complete characterization of the GO sample is available in [36]. Atomic force microscopy (AFM), Raman spectroscopy, and X-ray photoelectron spectroscopy (XPS) were used to assess size, morphology, number of layers, and surface chemistry of GO. The GO sample used in this study consists of single layers with

• less than 1.5 nm thickness and a flake size distribution from 18 to 308 nm. The calculated ratio between the intensity of the D (ID) and G (IG) bands of Raman is ID/IG = 0.85, indicating that the material has a high number of defects, an indirect indication of oxidation. The surface chemical

• [45][46]. In the absence of TA, the modulation of the C=0 stretching vibration intensity may indicate coordination of the divalent metal ions Ca2+ and Mg2+ present in EPA medium [47]. The intensity ratio between ID and IG bands in Raman spectroscopy analysis ranges from 0.94 ± 0.01, for the GO sample

Photocatalytic methane oxidation over a TiO₂/SiNWs p–n junction catalyst at room temperature

• Qui Thanh Hoai Ta,
• Luan Minh Nguyen,
• Ngoc Hoi Nguyen,
• Phan Khanh Thinh Nguyen and
• Dai Hai Nguyen

Beilstein J. Nanotechnol. 2024, 15, 1132–1141, doi:10.3762/bjnano.15.92

• a water contact angle of 50.24°. Because of the nanowire array morphology, the p-Si NWs were more hydrophilic nature with a water contact angle of 3.36°, which manifests superior photocatalytic oxidative coupling. Raman spectra were conducted to confirm the surface composition of the synthesized

• photocatalysts. As depicted in Figure 4a, the Raman spectrum of Si exhibits a single peak located at 519 cm−1, corresponding to the first-order transverse optical (TO) mode of Si [46]. For the TiO2/Si photocatalyst, two distinct peaks were observed, namely, (i) the characteristic Eg vibration of TiO2, located at

• 146 cm−1, and (ii) the TO phonon mode of Si (Figure 4b) [47][48][49]. Consequently, the combined surface-sensitive Raman and bulk-sensitive XRD results reveal that the n-type TiO2 coating layer on p-type SiNWs does not influence the crystalline structure. Photocatalytic OCM The photocatalytic OCM

Direct electron beam writing of silver using a β-diketonate precursor: first insights

• Katja Höflich,
• Krzysztof Maćkosz,
• Chinmai S. Jureddy,
• Aleksei Tsarapkin and
• Ivo Utke

Beilstein J. Nanotechnol. 2024, 15, 1117–1124, doi:10.3762/bjnano.15.90

• Raman or FTIR spectroscopy [5][8][37], to study the nature of the desorbed and incorporated molecular fragments ideally during the irradiation process. Up to now, only silver pentafluoropriopionate allowed for three-dimensional growth [30]. However, the use of this compound required relatively high

Effect of wavelength and liquid on formation of Ag, Au, Ag/Au nanoparticles via picosecond laser ablation and SERS-based detection of DMMP

• Sree Satya Bharati Moram,
• Chandu Byram and
• Venugopal Rao Soma

Beilstein J. Nanotechnol. 2024, 15, 1054–1069, doi:10.3762/bjnano.15.86

• -dispersive X-ray spectroscopy. Furthermore, NPs of various sizes ranging from 6 to 35 nm were loaded onto a filter paper by a simple and effective drop-casting approach to achieve flexible surface-enhanced Raman spectroscopy (SERS) substrates/sensors. These substrates were tested using a simple, portable

• Raman device to identify various hazardous chemicals (malachite green, methyl salicylate, and thiram). The stability of the substrates was also systematically investigated by determining the decay percentages in the SERS signals over 60 days. The optimized SERS substrate was subsequently employed to

• simulants was observed at a 325 nm Raman excitation. Our findings reveal that a higher ablation yield was observed at IR irradiation than those obtained at the other wavelengths. A size decrease of the NPs was noticed by changing the liquid environment to an electrolyte. These findings have significant