A non-enzymatic electrochemical hydrogen peroxide sensor based on copper oxide nanostructures

• Irena Mihailova,
• Vjaceslavs Gerbreders,
• Marina Krasovska,
• Eriks Sledevskis,
• Valdis Mizers,
• Andrejs Bulanovs and
• Andrejs Ogurcovs

Beilstein J. Nanotechnol. 2022, 13, 424–436, doi:10.3762/bjnano.13.35

• concentration of H2O2 in the range from 10 to 1800 μM was obtained. The sensitivity of the obtained CuO electrode is 439.19 μA·mM−1. The calculated limit of detection is 1.34 μM, assuming a signal-to-noise ratio of 3. The investigation of the system for sensitivity to interference showed that the most common

• signal-to-noise ratio of 3. The results indicate that the nanostructured CuO electrode can be used for accurate and precise detection of H2O2. The obtained results are comparable to several published studies where CuO nanostructures were used for electrode modification for H2O2 detection (Table 1). For

Measurement of polarization effects in dual-phase ceria-based oxygen permeation membranes using Kelvin probe force microscopy

• Kerstin Neuhaus,
• Christina Schmidt,
• Liudmila Fischer,
• Wilhelm Albert Meulenberg,
• Ke Ran,
• Joachim Mayer and
• Stefan Baumann

Beilstein J. Nanotechnol. 2021, 12, 1380–1391, doi:10.3762/bjnano.12.102

• -circuit potential. For all temperatures, the relaxation took less than 40 s for negative polarization and less than 60 s for positive polarization. All relaxation curves showed a clear dependence on exponential rules, although for temperature below 250 °C, the signal-to-noise ratio was very low for the

Cantilever signature of tip detachment during contact resonance AFM

• Devin Kalafut,
• Ryan Wagner,
• Maria Jose Cadena,
• Anil Bajaj and
• Arvind Raman

Beilstein J. Nanotechnol. 2021, 12, 1286–1296, doi:10.3762/bjnano.12.96

• on how the cantilever motion evolves when this essential condition is violated. This is not an uncommon occurrence since higher operating amplitudes tend to yield better signal-to-noise ratio, so users may inadvertently reduce their experimental accuracy by inducing tip–sample detachment in an effort

The effect of cobalt on morphology, structure, and ORR activity of electrospun carbon fibre mats in aqueous alkaline environments

• Markus Gehring,
• Tobias Kutsch,
• Osmane Camara,
• Alexandre Merlen,
• Hermann Tempel,
• Hans Kungl and
• Rüdiger-A. Eichel

Beilstein J. Nanotechnol. 2021, 12, 1173–1186, doi:10.3762/bjnano.12.87

• only in the binding energy range from 770 to 795 eV. Raman spectra were obtained using a Bruker Senterra at room temperature in ambient atmosphere. The excitation wavelength was 532 nm with a power of 2 mW. The signals of two subsequent measurements of 30 s each were added up, to improve the signal-to

• -noise ratio (co-addition mode). The resulting spectra were analysed by fitting a Lorentz distribution and a Breit–Wigner–Fano distribution, as explained in detail in [12]. For the elemental analysis 2 mg of sample was burned in the elemental analyser (VarioelCube, Elementar) for both CHN and O analyses

Uniform arrays of gold nanoelectrodes with tuneable recess depth

• Elena O. Gordeeva,
• Ilya V. Roslyakov,
• Alexey P. Leontiev,
• Alexey A. Klimenko and
• Kirill S. Napolskii

Beilstein J. Nanotechnol. 2021, 12, 957–964, doi:10.3762/bjnano.12.72

• diffusion layers results in the planar diffusion to the NEA surface. Thus, a decrease in the density of active electrodes could be more appropriate because of the decrease in electric double layer charging current and, as a consequence, the growth of the signal-to-noise ratio. A controlled decrease in the

Reducing molecular simulation time for AFM images based on super-resolution methods

• Zhipeng Dou,
• Jianqiang Qian,
• Yingzi Li,
• Rui Lin,
• Jianhai Wang,
• Peng Cheng and
• Zeyu Xu

Beilstein J. Nanotechnol. 2021, 12, 775–785, doi:10.3762/bjnano.12.61

• factors to 2× (25 × 25) and 3× (17 × 17), respectively, to construct super-resolution images. The peak signal to noise ratio (PSNR, expressed as the logarithmic decibel scale) and structural similarity (SSIM, value range is [0,1]) are used to evaluate the quality of the reconstructed image. The PSNR is

A review of defect engineering, ion implantation, and nanofabrication using the helium ion microscope

• Frances I. Allen

Beilstein J. Nanotechnol. 2021, 12, 633–664, doi:10.3762/bjnano.12.52

Intracranial recording in patients with aphasia using nanomaterial-based flexible electronics: promises and challenges

• Qingchun Wang and
• Wai Ting Siok

Beilstein J. Nanotechnol. 2021, 12, 330–342, doi:10.3762/bjnano.12.27

• has an excellent temporal resolution at the millisecond scale. ECoG data have a typical sampling rate of 1,000–3,000 Hz. This high temporal resolution offers an opportunity to observe the rapid dynamics of neural activities in precisely localized brain regions. ECoG has a much higher signal-to-noise

• µm PI layers. The bifurcated flap shape was used to achieve good penetration and attachment to the cortical surface and avoid injuring blood vessels on the brain midline (Figure 5c, left). The width of the Au lines was designed to be 100 µm to reach a low impedance value and enhance the signal-to

• -noise ratio (Figure 5c, right). The real-time signals of cortical activities in different medical and drug-induced epileptic states were precisely measured when the iWEBS array was used in freely moving mice. Combined with optogenetic mapping techniques, long-range cortical interactions were

The patterning toolbox FIB-o-mat: Exploiting the full potential of focused helium ions for nanofabrication

• Victor Deinhart,
• Lisa-Marie Kern,
• Jan N. Kirchhof,
• Sabrina Juergensen,
• Joris Sturm,
• Enno Krauss,
• Thorsten Feichtner,
• Sviatoslav Kovalchuk,
• Michael Schneider,
• Dieter Engel,
• Bastian Pfau,
• Bert Hecht,
• Kirill I. Bolotin,
• Stephanie Reich and
• Katja Höflich

Beilstein J. Nanotechnol. 2021, 12, 304–318, doi:10.3762/bjnano.12.25

• modulation setup. The spatial displacement of the focus modulates the signal [61] and the lock-in coupled detector provides an excellent signal-to-noise ratio for individual small scatterers. Figure 7d–f shows the extinction (sum of scattering and absorption) spectra corresponding to the tetramers in Figure

Scanning transmission helium ion microscopy on carbon nanomembranes

• Daniel Emmrich,
• Annalena Wolff,
• Nikolaus Meyerbröker,
• Jörg K. N. Lindner,
• André Beyer and
• Armin Gölzhäuser

Beilstein J. Nanotechnol. 2021, 12, 222–231, doi:10.3762/bjnano.12.18

• capability is the ability to record charge-compensated images on insulating samples such as biological specimen or polymers without requiring a conductive coating layer [2][3][4]. In addition, the ability to record images with high signal-to-noise ratio while using low beam currents (the HIM creates up to

• for ion microscopes. The dark-field STIM detector enables the imaging of very thin carbon nanomembranes with a high signal-to-noise ratio, which could not be achieved using the conventional ETD detector in the HIM. The evaluation of the contrast mechanism suggests that the detector is suitable for end

Toward graphene textiles in wearable eye tracking systems for human–machine interaction

• Ata Jedari Golparvar and
• Murat Kaya Yapici

Beilstein J. Nanotechnol. 2021, 12, 180–189, doi:10.3762/bjnano.12.14

• 11.6 kΩ (at 1 kHz). Additionally, since the operation of the textile electrodes relies on charge flow, moisture and sweat can increase the interface conductivity of the skin electrodes and provide an even better signal-to-noise ratio (SNR) in long-term monitoring applications in contrast to “wet

Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector

• Eduardo Serralta,
• Nico Klingner,
• Olivier De Castro,
• Michael Mousley,
• Santhana Eswara,
• Serge Duarte Pinto,
• Tom Wirtz and
• Gregor Hlawacek

Beilstein J. Nanotechnol. 2020, 11, 1854–1864, doi:10.3762/bjnano.11.167

• phenomena occurring during the projectile–target interaction and can increase the signal-to-noise ratio [23]. Since most likely a considerable fraction of the transmitted particles at this energy range is neutral [24][25], magnetic or electrostatic spectrometers cannot be used. Therefore, ion energy-loss

Mapping of integrated PIN diodes with a 3D architecture by scanning microwave impedance microscopy and dynamic spectroscopy

• Rosine Coq Germanicus,
• Peter De Wolf,
• Florent Lallemand,
• Catherine Bunel,
• Serge Bardy,
• Hugues Murray and
• Ulrike Lüders

Beilstein J. Nanotechnol. 2020, 11, 1764–1775, doi:10.3762/bjnano.11.159

• vertical PIN diode with the associated metallic contacts of the anode. Although the sMIM-R signal shows a low signal-to-noise ratio, it is still possible to differentiate metallic materials from semiconductor layers. Also, the conductivity continuity between the metallic contact and the p+ anode can be

• seen. The sMIM-C map clearly shows the complete architecture of the PIN structure with details of the anode contact and with very clear differences (in terms of contrast, layer location, and signal-to-noise ratio) between the P (p+ anode), I (lightly doped n-type epitaxial silicon), and N (n-type doped

• that the depth profile has a good signal-to-noise ratio for the sMIM-C signal for each layer. This first analysis demonstrates the capability of the sMIM methodology to distinguish, localize, and determine both p-type and n-type semiconductors as well as lightly doped layers, metallic contacts, and

Design of V-shaped cantilevers for enhanced multifrequency AFM measurements

• Mehrnoosh Damircheli and
• Babak Eslami

Beilstein J. Nanotechnol. 2020, 11, 1525–1541, doi:10.3762/bjnano.11.135

• focused on finding the optimum for these geometrical dimensions of a V-shaped cantilever with the aim to enhance the signal-to-noise ratio (SNR) and, consequently, to enhance the second eigenmode phase signal. A numerical study is carried out to model the V-shaped cantilevers given the abovementioned

A wideband cryogenic microwave low-noise amplifier

• Boris I. Ivanov,
• Dmitri I. Volkhin,
• Ilya L. Novikov,
• Dmitri K. Pitsun,
• Dmitri O. Moskalev,
• Ilya A. Rodionov,
• Evgeni Il’ichev and
• Aleksey G. Vostretsov

Beilstein J. Nanotechnol. 2020, 11, 1484–1491, doi:10.3762/bjnano.11.131

• sensitivity and measurement speed of the full measurement setup is obviously defined by the signal-to-noise ratio and, thus, by the gain and the noise temperature of the cLNA. The sample under study contained superconducting X-mon qubits coupled to coplanar quarter wavelength resonators. Each resonator was

• microwave amplifier (marked as rLNA in Figure 5) was used. It was dedicated to increasing the signal level at the output of cLNA before data acquisition. The rLNA did not influence the signal-to-noise ratio of the measurement system since this parameter is mainly defined by the cLNA output noise. The rLNA

Wafer-level integration of self-aligned high aspect ratio silicon 3D structures using the MACE method with Au, Pd, Pt, Cu, and Ir

• Mathias Franz,
• Romy Junghans,
• Paul Schmitt,
• Adriana Szeghalmi and
• Stefan E. Schulz

Beilstein J. Nanotechnol. 2020, 11, 1439–1449, doi:10.3762/bjnano.11.128

• metal–insulator–semiconductor or metal–insulator–metal capacitors with a high effective area on a small footprint. The high surface area of a silicon nanowire array can be used to fabricate ion-sensitive field-effect transistors (ISFETs) with a high signal-to-noise ratio. An ISFET is a pH sensing

Magnetic-field-assisted synthesis of anisotropic iron oxide particles: Effect of pH

• Andrey V. Shibaev,
• Petr V. Shvets,
• Darya E. Kessel,
• Roman A. Kamyshinsky,
• Anton S. Orekhov,
• Sergey S. Abramchuk,
• Alexei R. Khokhlov and
• Olga E. Philippova

Beilstein J. Nanotechnol. 2020, 11, 1230–1241, doi:10.3762/bjnano.11.107

• sufficient to avoid any structural changes or phase degradation in the samples. Under these conditions, the typical total acquisition time to obtain a spectrum with good signal-to-noise ratio was several hours. Temporal variation of pH when 2 mL of the ion mixture (1 M FeCl3 + 0.5 M FeSO4 in 0.1 M HCl) is

Hybridization vs decoupling: influence of an h-BN interlayer on the physical properties of a lander-type molecule on Ni(111)

• Maximilian Schaal,
• Takumi Aihara,
• Marco Gruenewald,
• Felix Otto,
• Jari Domke,
• Roman Forker,
• Hiroyuki Yoshida and
• Torsten Fritz

Beilstein J. Nanotechnol. 2020, 11, 1168–1177, doi:10.3762/bjnano.11.101

• , respectively, and d being the film thickness. Each reflectance spectrum was accumulated over 30 s to increase the signal-to-noise ratio. Furthermore, we used the difference of consecutive reflectance spectra to calculate the ΔDRS intensity using the following formula: The lateral structure of the DBP films was

Uniform Fe₃O₄/Gd₂O₃-DHCA nanocubes for dual-mode magnetic resonance imaging

• Miao Qin,
• Yueyou Peng,
• Mengjie Xu,
• Hui Yan,
• Yizhu Cheng,
• Xiumei Zhang,
• Di Huang,
• Weiyi Chen and
• Yanfeng Meng

Beilstein J. Nanotechnol. 2020, 11, 1000–1009, doi:10.3762/bjnano.11.84

• imaging (T1WI) and T2-weighted imaging (T2WI) were performed in Sprague Dawley (SD) rats. After intravenous injection of a 0.8 mg Fe/kg dose, FGDA nanocubes spread systemically through the bloodstream. The lumbar muscle was chosen as the MRI region of interest and the signal-to-noise ratio (ΔSNR) was

Measurement of electrostatic tip–sample interactions by time-domain Kelvin probe force microscopy

• Christian Ritz,
• Tino Wagner and
• Andreas Stemmer

Beilstein J. Nanotechnol. 2020, 11, 911–921, doi:10.3762/bjnano.11.76

• effect is amplified when a significant change in the capacitance gradient is present. To reduce the impact of this component onto the height measurement, the modulation amplitude Uac must be minimized. Since the signal-to-noise ratio (SNR) scales with Uac, this is only possible to a certain extent

Light–matter interactions in two-dimensional layered WSe₂ for gauging evolution of phonon dynamics

• Avra S. Bandyopadhyay,
• Chandan Biswas and
• Anupama B. Kaul

Beilstein J. Nanotechnol. 2020, 11, 782–797, doi:10.3762/bjnano.11.63

• a function of P at T = 298 K. In order to minimize the laser-induced effects on the crystallinity and structural changes in the WSe2, a laser P ≤ 3.35 mW was used. It was also found that the minimum P required to get a good signal-to-noise ratio for the Raman and PL data was when P ≥ 0.31 mW

• cell allowed the temperature to reach 523 K. During the cooling process, it was found that the signal to noise ratio was very poor when both the T and P became very low, particularly in case of PL measurements. The best signal to noise ratio in both the Raman and PL measurements was found for P = 3.35

Current measurements in the intermittent-contact mode of atomic force microscopy using the Fourier method: a feasibility analysis

• Berkin Uluutku and
• Santiago D. Solares

Beilstein J. Nanotechnol. 2020, 11, 453–465, doi:10.3762/bjnano.11.37

• trend. Reconstruction of the tip–sample current should be possible if one can record its power spectrum. It is of course desirable to be able to record as many harmonics as possible, although this may not always be possible, in part due to signal-to-noise ratio limitations for very high frequencies or

• -conductive tip. Electrical noise is anticipated to also introduce challenges. Although classical C-AFM can be affected by noise as well, the expected current magnitude in this mode of imaging should be larger than for ICM-AFM for the reasons described above, such that the current signal-to-noise ratio for

An advanced structural characterization of templated meso-macroporous carbon monoliths by small- and wide-angle scattering techniques

• Felix M. Badaczewski,
• Marc O. Loeh,
• Torben Pfaff,
• Dirk Wallacher,
• Daniel Clemens and
• Bernd M. Smarsly

Beilstein J. Nanotechnol. 2020, 11, 310–322, doi:10.3762/bjnano.11.23

• templates were infiltrated by two different carbon precursors, namely a mesophase pitch and a formaldehyde resole. The template was removed with hydrofluoric acid. Further information can be found in a recent study [41]. SANS data with a very good signal-to-noise ratio were acquired utilizing the V16

Self-assembly of a terbium(III) 1D coordination polymer on mica

• Quentin Evrard,
• Giuseppe Cucinotta,
• Felix Houard,
• Guillaume Calvez,
• Yan Suffren,
• Carole Daiguebonne,
• Olivier Guillou,
• Andrea Caneschi,
• Matteo Mannini and
• Kevin Bernot

Beilstein J. Nanotechnol. 2019, 10, 2440–2448, doi:10.3762/bjnano.10.234

• it is. The static magnetic measurements of [Tb(hfac)3·2H2O]n and [Tb(hfac)3·2H2O]n@mica have been performed at 1.8 K using a conventional SQUID magnetometer (Figure S2, Supporting Information File 1). A very good signal-to-noise ratio is observed on the deposits, which validates the use of TbIII as a

A novel method to remove impulse noise from atomic force microscopy images based on Bayesian compressed sensing

• Yingxu Zhang,
• Yingzi Li,
• Zihang Song,
• Zhenyu Wang,
• Jianqiang Qian and
• Junen Yao

Beilstein J. Nanotechnol. 2019, 10, 2346–2356, doi:10.3762/bjnano.10.225

• images used in the paper is 256 × 256 pixels. The proposed method, median filter (window size: 7 × 7 pixels) and adaptive median filter (maximum window size: 7 × 7 pixels, minimum window: 3 × 3 pixels) are used separately to remove the impulse noise. The peak signal-to-noise ratio (PSNR) [35] and the