Search results

Search for "dynamic light scattering (DLS)" in Full Text gives 163 result(s) in Beilstein Journal of Nanotechnology.

Controllable one-pot synthesis of uniform colloidal TiO2 particles in a mixed solvent solution for photocatalysis

  • Jong Tae Moon,
  • Seung Ki Lee and
  • Ji Bong Joo

Beilstein J. Nanotechnol. 2018, 9, 1715–1727, doi:10.3762/bjnano.9.163

Graphical Abstract
  • TiO2, we conducted SEM under low magnification and dynamic light scattering (DLS) analysis. Supporting Information File 1, Figure S2 shows low magnification SEM images and the DLS results of as-synthesized amorphous TiO2 particles which were prepared by using a volume ratio of EtOH/ACN of 3:1, and
PDF
Album
Supp Info
Full Research Paper
Published 08 Jun 2018

Nanocomposites comprised of homogeneously dispersed magnetic iron-oxide nanoparticles and poly(methyl methacrylate)

  • Sašo Gyergyek,
  • David Pahovnik,
  • Ema Žagar,
  • Alenka Mertelj,
  • Rok Kostanjšek,
  • Miloš Beković,
  • Marko Jagodič,
  • Heinrich Hofmann and
  • Darko Makovec

Beilstein J. Nanotechnol. 2018, 9, 1613–1622, doi:10.3762/bjnano.9.153

Graphical Abstract
  • equipped with STARe 9.3 software (Mettler Toledo, OH, USA). The glass-transition temperature of the nanocomposites was determined on a Mettler Toledo DSC1 instrument. Dynamic light scattering (DLS) was used to measure the distribution of the hydrodynamic diameter of the nanoparticle. The room temperature
  • of the NP-PMMA-3, where the concentration of the NP-MMA was the highest, indicate the relatively high content of the PMMA chains connecting several neighboring nanoparticles. The size of the NP-PMMA-3 nanoparticles and the free PMMA chains were probed using dynamic light scattering (DLS). Two
PDF
Album
Supp Info
Full Research Paper
Published 01 Jun 2018

Closed polymer containers based on phenylboronic esters of resorcinarenes

  • Tatiana Yu. Sergeeva,
  • Rezeda K. Mukhitova,
  • Irek R. Nizameev,
  • Marsil K. Kadirov,
  • Polina D. Klypina,
  • Albina Y. Ziganshina and
  • Alexander I. Konovalov

Beilstein J. Nanotechnol. 2018, 9, 1594–1601, doi:10.3762/bjnano.9.151

Graphical Abstract
  • index (PDI) of 0.23 according to dynamic light scattering (DLS) data (see Supporting Information File 1, Figure S1, Table S1). Hereafter, we studied only the particles formed using this ratio. The nanoparticles were purified by dialysis, washed with acetone and dried to give p(SRA-B) with 66% yield. The
PDF
Album
Supp Info
Full Research Paper
Published 29 May 2018

Formation and development of nanometer-sized cybotactic clusters in bent-core nematic liquid crystalline compounds

  • Yuri P. Panarin,
  • Sithara P. Sreenilayam,
  • Jagdish K. Vij,
  • Anne Lehmann and
  • Carsten Tschierske

Beilstein J. Nanotechnol. 2018, 9, 1288–1296, doi:10.3762/bjnano.9.121

Graphical Abstract
  • above the isotropic–nematic transition temperature. The latter observation arises as seeds of cybotactic clusters are formed in the isotropic phase. Small clusters have also been observed by dynamic light scattering (DLS) [57]. The strength of this process is observed to increase with a reduction in
PDF
Album
Full Research Paper
Published 25 Apr 2018

Surface characterization of nanoparticles using near-field light scattering

  • Eunsoo Yoo,
  • Yizhong Liu,
  • Chukwuazam A. Nwasike,
  • Sebastian R. Freeman,
  • Brian C. DiPaolo,
  • Bernardo Cordovez and
  • Amber L. Doiron

Beilstein J. Nanotechnol. 2018, 9, 1228–1238, doi:10.3762/bjnano.9.114

Graphical Abstract
  • nanoparticles Dynamic light scattering (DLS) was used to measure the hydrodynamic diameter, polydispersity index, and zeta potential (ζ). The mean hydrodynamic diameter of the samples increased with the addition of PEG and polygallol to the complexation. The polydispersity index of uncoated SPIOs was 0.16
  • distribution, polydispersity index (PDI), and zeta potential of each sample was determined by dynamic light scattering (DLS, Zetasizer, Malvern NanoZS, Worcestershire, UK) at room temperature. For DLS, all samples were suspended in water at a SPIO concentration of 0.05 mg/mL and placed in a DTS1070 folded
PDF
Album
Full Research Paper
Published 18 Apr 2018

Enzymatically promoted release of organic molecules linked to magnetic nanoparticles

  • Chiara Lambruschini,
  • Silvia Villa,
  • Luca Banfi,
  • Fabio Canepa,
  • Fabio Morana,
  • Annalisa Relini,
  • Paola Riani,
  • Renata Riva and
  • Fulvio Silvetti

Beilstein J. Nanotechnol. 2018, 9, 986–999, doi:10.3762/bjnano.9.92

Graphical Abstract
  • . They are here identified as NP@silica@APTES. The morphology and chemical composition of these nanoparticles was studied using field emission scanning electron microscopy (FE-SEM) in combination with energy dispersive X-ray spectroscopy (EDXS) in addition to dynamic light scattering (DLS). In Figure 1A
PDF
Album
Supp Info
Full Research Paper
Published 27 Mar 2018

Optimisation of purification techniques for the preparation of large-volume aqueous solar nanoparticle inks for organic photovoltaics

  • Furqan Almyahi,
  • Thomas R. Andersen,
  • Nathan A. Cooling,
  • Natalie P. Holmes,
  • Matthew J. Griffith,
  • Krishna Feron,
  • Xiaojing Zhou,
  • Warwick J. Belcher and
  • Paul C. Dastoor

Beilstein J. Nanotechnol. 2018, 9, 649–659, doi:10.3762/bjnano.9.60

Graphical Abstract
  • inks, filtrates were collected at each dilution step for both purification methods. For small volume, 0.5 mL of ASNP inks were collected at each dilution step while the collected filtrate was 2 mL. Nanoparticle characterisation Particle size Particle sizes were determined by dynamic light scattering
  • (DLS) (Zetasiser Nano-ZS ZEN3500, Malvern Instruments) with a 633 nm laser and a backscatter detector angle of 173°. Samples for DLS were prepared by diluting 5 µL of NP ink in 10 mL Milli-Q water in order to reduce the solids content from 6 to 0.003%. Free SDS concentration UV-vis spectroscopy: An
PDF
Album
Supp Info
Full Research Paper
Published 20 Feb 2018

Green synthesis of fluorescent carbon dots from spices for in vitro imaging and tumour cell growth inhibition

  • Nagamalai Vasimalai,
  • Vânia Vilas-Boas,
  • Juan Gallo,
  • María de Fátima Cerqueira,
  • Mario Menéndez-Miranda,
  • José Manuel Costa-Fernández,
  • Lorena Diéguez,
  • Begoña Espiña and
  • María Teresa Fernández-Argüelles

Beilstein J. Nanotechnol. 2018, 9, 530–544, doi:10.3762/bjnano.9.51

Graphical Abstract
  • xenon discharge lamp, 1 cm quartz cell at room temperature. For all the fluorescence measurements, excitation and emission slit widths were kept at 5 nm. Dynamic light scattering (DLS) and zeta potential studies were performed on a Horiba nanoPartica SZ-100 instrument (Horiba Scientific, USA). For this
PDF
Album
Supp Info
Full Research Paper
Published 13 Feb 2018

Photocatalytic and adsorption properties of TiO2-pillared montmorillonite obtained by hydrothermally activated intercalation of titanium polyhydroxo complexes

  • Mikhail F. Butman,
  • Nikolay L. Ovchinnikov,
  • Nikita S. Karasev,
  • Nataliya E. Kochkina,
  • Alexander V. Agafonov and
  • Alexandr V. Vinogradov

Beilstein J. Nanotechnol. 2018, 9, 364–378, doi:10.3762/bjnano.9.36

Graphical Abstract
  • close to the sol formation limit. The materials, produced at various annealing temperatures from the intercalated samples, were characterized by infrared spectroscopy, differential scanning calorimetry (DSC)/thermogravimetric analysis (TGA), X-ray diffraction, dynamic light scattering (DLS) measurements
  • TiO2-pillared MM with the commercial photocatalyst Degussa P25 upon degradation of methyl orange (MO) and rhodamine B (RhB) dyes in aqueous solution. SEM image of the surface of original MM. The fluorescence spectrum of an intercalating solution of titanium polyhydroxo complexes. The dynamic light
  • scattering (DLS) spectrum. Basal distance d001 of the MM, Ti-MM, TiO2-PMMх, and TiO2-PMMHх samples (see Experimental section for abbreviations). Average crystallite size and phase composition of the TiO2-PMMНx samples (see Experimental sections for a description of the sample names). Average values of the
PDF
Album
Full Research Paper
Published 31 Jan 2018

Involvement of two uptake mechanisms of gold and iron oxide nanoparticles in a co-exposure scenario using mouse macrophages

  • Dimitri Vanhecke,
  • Dagmar A. Kuhn,
  • Dorleta Jimenez de Aberasturi,
  • Sandor Balog,
  • Ana Milosevic,
  • Dominic Urban,
  • Diana Peckys,
  • Niels de Jonge,
  • Wolfgang J. Parak,
  • Alke Petri-Fink and
  • Barbara Rothen-Rutishauser

Beilstein J. Nanotechnol. 2017, 8, 2396–2409, doi:10.3762/bjnano.8.239

Graphical Abstract
  • ., AuNPs with 2% DY505 fluorophore, and FeOxNPs with 2% DY615 fluorophore integrated into the polymer shell were synthesized as previously described [44][45]. For both NPs the hydrodynamic radius (dh) was measured by dynamic light scattering (DLS) and a corresponding core diameter (dc = 2·rc) was extracted
PDF
Album
Supp Info
Full Research Paper
Published 14 Nov 2017

Fabrication of carbon nanospheres by the pyrolysis of polyacrylonitrile–poly(methyl methacrylate) core–shell composite nanoparticles

  • Dafu Wei,
  • Youwei Zhang and
  • Jinping Fu

Beilstein J. Nanotechnol. 2017, 8, 1897–1908, doi:10.3762/bjnano.8.190

Graphical Abstract
  • concentrations of MB, respectively, V (L) is the volume of MB aqueous solution, and m (g) is the weight of carbon nanospheres. Characterization The z-average hydrodynamic diameter of the various nanoparticles was determined by dynamic light scattering (DLS) using a Malvern Zeta-sizer (DTS1060, Malvern, UK). The
PDF
Album
Supp Info
Full Research Paper
Published 11 Sep 2017

Carbon nano-onions as fluorescent on/off modulated nanoprobes for diagnostics

  • Stefania Lettieri,
  • Marta d’Amora,
  • Adalberto Camisasca,
  • Alberto Diaspro and
  • Silvia Giordani

Beilstein J. Nanotechnol. 2017, 8, 1878–1888, doi:10.3762/bjnano.8.188

Graphical Abstract
  • laser which can alter the measurements due to background signal. Dynamic light scattering (DLS) was carried out to determine the hydrodynamic radius of the dispersed CNOs (Table 2, Figure 5). DLS experiments were performed on CNOs samples dispersed in 0.01 M PBS to partially mimic the biological
  • emission maximum (λem). Effective hydrodynamic diameter (0.01 M PBS) obtained from dynamic light scattering (DLS) measurements and zeta potential (phosphate buffer) of oxi-CNOs and fluo-CNOs at a concentration of 5 µg mL−1 in PBS. Supporting Information Supporting Information File 82: Additional
PDF
Album
Supp Info
Full Research Paper
Published 07 Sep 2017

Self-assembly of chiral fluorescent nanoparticles based on water-soluble L-tryptophan derivatives of p-tert-butylthiacalix[4]arene

  • Pavel L. Padnya,
  • Irina A. Khripunova,
  • Olga A. Mostovaya,
  • Timur A. Mukhametzyanov,
  • Vladimir G. Evtugyn,
  • Vyacheslav V. Vorobev,
  • Yuri N. Osin and
  • Ivan I. Stoikov

Beilstein J. Nanotechnol. 2017, 8, 1825–1835, doi:10.3762/bjnano.8.184

Graphical Abstract
  • structure of L-tryptophan, the resulting compounds 8–11 are water soluble. The structure and composition of the synthesized compounds 8–11 were determined by 1H and 13C NMR, IR spectroscopy, ESI mass spectrometry and elemental analysis. The method of dynamic light scattering (DLS) is widely used to study
PDF
Album
Supp Info
Full Research Paper
Published 04 Sep 2017

Synthesis and functionalization of NaGdF4:Yb,Er@NaGdF4 core–shell nanoparticles for possible application as multimodal contrast agents

  • Dovile Baziulyte-Paulaviciene,
  • Vitalijus Karabanovas,
  • Marius Stasys,
  • Greta Jarockyte,
  • Vilius Poderys,
  • Simas Sakirzanovas and
  • Ricardas Rotomskis

Beilstein J. Nanotechnol. 2017, 8, 1815–1824, doi:10.3762/bjnano.8.183

Graphical Abstract
  • (Figure 3c), indicating that the Tween 80 was successfully coated onto the UCNPs. Additionally, dynamic light scattering (DLS) was employed to measure the hydrodynamic diameter of Tween-coated UCNPs in the cell culture medium as well as their surface zeta potential. The measured mean hydrodynamic diameter
  • equations: where ni and Di are the number and diameter of the particle, respectively. Dynamic light scattering (DLS) was used to determine the hydrodynamic particle diameter and zeta potential. These experiments were performed with Brookhaven ZetaPALS zeta potential analyzer (Brookhaven Instruments, USA
PDF
Album
Supp Info
Full Research Paper
Published 01 Sep 2017

Uptake and intracellular accumulation of diamond nanoparticles – a metabolic and cytotoxic study

  • Antonín Brož,
  • Lucie Bačáková,
  • Pavla Štenclová,
  • Alexander Kromka and
  • Štěpán Potocký

Beilstein J. Nanotechnol. 2017, 8, 1649–1657, doi:10.3762/bjnano.8.165

Graphical Abstract
  • diamond nanoparticles The size of the ND particles and their zeta potential was determined by dynamic light scattering (DLS) measurements in water at 25 °C using a Nano-ZetaSizer (Malvern, UK) equipped with an He-Ne laser. A separate disposable folded capillary cell was used for each set of ND
PDF
Album
Supp Info
Full Research Paper
Published 10 Aug 2017

A nanocomplex of C60 fullerene with cisplatin: design, characterization and toxicity

  • Svitlana Prylutska,
  • Svitlana Politenkova,
  • Kateryna Afanasieva,
  • Volodymyr Korolovych,
  • Kateryna Bogutska,
  • Andriy Sivolob,
  • Larysa Skivka,
  • Maxim Evstigneev,
  • Viktor Kostjukov,
  • Yuriy Prylutskyy and
  • Uwe Ritter

Beilstein J. Nanotechnol. 2017, 8, 1494–1501, doi:10.3762/bjnano.8.149

Graphical Abstract
  • of the hydrodynamic size distribution was performed by dynamic light scattering (DLS) on a Zetasizer Nano ZS (Malvern Ins. Ltd) with upload of multiple narrow modes (high resolution) at room temperature. The instrument is equipped with a He–Ne gas laser (max. output power 5 mW) operating at a
PDF
Album
Full Research Paper
Published 20 Jul 2017

Calcium fluoride based multifunctional nanoparticles for multimodal imaging

  • Marion Straßer,
  • Joachim H. X. Schrauth,
  • Sofia Dembski,
  • Daniel Haddad,
  • Bernd Ahrens,
  • Stefan Schweizer,
  • Bastian Christ,
  • Alevtina Cubukova,
  • Marco Metzger,
  • Heike Walles,
  • Peter M. Jakob and
  • Gerhard Sextl

Beilstein J. Nanotechnol. 2017, 8, 1484–1493, doi:10.3762/bjnano.8.148

Graphical Abstract
  • because of the low solubility of NH4F in an ethanol solution and therefore the particle growth is slower [26]. The inset in Figure 1 shows the TEM micrograph of the CaF2:(Tb3+,Gd3+) NPs. The NPs possess a spherical shape with an average diameter of 5–10 nm. The results of the dynamic light scattering (DLS
PDF
Album
Supp Info
Full Research Paper
Published 18 Jul 2017

Development of polycationic amphiphilic cyclodextrin nanoparticles for anticancer drug delivery

  • Gamze Varan,
  • Juan M. Benito,
  • Carmen Ortiz Mellet and
  • Erem Bilensoy

Beilstein J. Nanotechnol. 2017, 8, 1457–1468, doi:10.3762/bjnano.8.145

Graphical Abstract
  • mL ultrapure water using the conditions previously given. Mean particle size distribution and surface charge The mean particle diameter (nm), PDI and zeta potential (mV) of amphiphilic CD nanoparticles were determined by dynamic light scattering (DLS) (NanoZS, Malvern Instruments, UK). All
PDF
Album
Full Research Paper
Published 13 Jul 2017

Cationic PEGylated polycaprolactone nanoparticles carrying post-operation docetaxel for glioma treatment

  • Cem Varan and
  • Erem Bilensoy

Beilstein J. Nanotechnol. 2017, 8, 1446–1456, doi:10.3762/bjnano.8.144

Graphical Abstract
  • was removed from the surface of the PET film to obtain the final product. Nanoparticle characterization Particle size distribution and surface charge analysis: the mean particle diameter and polydispersity index of the nanoparticles were determined by dynamic light scattering (DLS) technique using a
PDF
Album
Full Research Paper
Published 12 Jul 2017

Low uptake of silica nanoparticles in Caco-2 intestinal epithelial barriers

  • Dong Ye,
  • Mattia Bramini,
  • Delyan R. Hristov,
  • Sha Wan,
  • Anna Salvati,
  • Christoffer Åberg and
  • Kenneth A. Dawson

Beilstein J. Nanotechnol. 2017, 8, 1396–1406, doi:10.3762/bjnano.8.141

Graphical Abstract
  • , with no signs of agglomeration, though naturally serum protein adsorption increases the sizes. Table 1 also shows auxiliary dispersion characterisation by dynamic light scattering (DLS), leading to the same conclusions. Nanoparticle dispersions were prepared with and without FBS protein in order to
  • serum (FBS) in Hank's balanced salt solution (HBSS) buffer (with 25 mM 4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid (HEPES), pH 7.4) at 25 °C, using a Malvern Zetasizer Nano ZS90 (Worcestershire, UK) in order to measure the hydrodynamic diameter by dynamic light scattering (DLS). The 150 nm
  • . Nanoparticle dispersion (100 µg/mL) in water, serum free HBSS and HBSS supplemented with 10% foetal bovine serum (FBS) were characterised by differential centrifugal sedimentation (DCS) and dynamic light scattering (DLS) as described in the Experimental section. The table shows the apparent diameter and peak
PDF
Album
Supp Info
Full Research Paper
Published 07 Jul 2017

Synthesis of [Fe(Leq)(Lax)]n coordination polymer nanoparticles using blockcopolymer micelles

  • Christoph Göbel,
  • Ottokar Klimm,
  • Florian Puchtler,
  • Sabine Rosenfeldt,
  • Stephan Förster and
  • Birgit Weber

Beilstein J. Nanotechnol. 2017, 8, 1318–1327, doi:10.3762/bjnano.8.133

Graphical Abstract
  • dynamic light scattering (DLS) in solution, transmission electron microscopy (TEM) and powder X-ray diffraction (PXRD) in the solid. The hydrodynamic diameter of the polymeric micelles loaded with the CP measured by DLS is constant within the error of the measurement throughout all measured samples with
PDF
Album
Supp Info
Full Research Paper
Published 26 Jun 2017

Bright fluorescent silica-nanoparticle probes for high-resolution STED and confocal microscopy

  • Isabella Tavernaro,
  • Christian Cavelius,
  • Henrike Peuschel and
  • Annette Kraegeloh

Beilstein J. Nanotechnol. 2017, 8, 1283–1296, doi:10.3762/bjnano.8.130

Graphical Abstract
  • (5% size distribution; FD15_Atto647N) or 25 nm (4%; FD25_Atto647N) could be obtained (Figure 1). Hydrodynamic diameters determined by dynamic light scattering (DLS) were in accordance with diameters obtained from SEM or TEM image analysis (Table 1). These results show that no agglomerates of the
  • ), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Dynamic light scattering: DLS measurements were performed with a StabiSizer Nano 250 from Particle Metrix (Meerbusch, Germany) or the Nanosizer ZSP from Malvern Instruments (Herrenberg, Germany). For the DLS measurements the
PDF
Album
Supp Info
Full Research Paper
Published 21 Jun 2017

Study of the correlation between sensing performance and surface morphology of inkjet-printed aqueous graphene-based chemiresistors for NO2 detection

  • F. Villani,
  • C. Schiattarella,
  • T. Polichetti,
  • R. Di Capua,
  • F. Loffredo,
  • B. Alfano,
  • M. L. Miglietta,
  • E. Massera,
  • L. Verdoliva and
  • G. Di Francia

Beilstein J. Nanotechnol. 2017, 8, 1023–1031, doi:10.3762/bjnano.8.103

Graphical Abstract
  • LPE graphene dispersion has been investigated by dynamic light scattering (DLS) to determine the size distribution profile of the suspended graphene flakes. An almost monomodal distribution characterized by a low polydispersity has been detected, so indicating the homogeneity of the sample. The
  • of five measurements, have been evaluated by the Owen, Wendt, Rabel and Kaelble (OWRK) method [21]. Both disperse and polar components of SE have been estimated. Dynamic light scattering (DLS) analysis has been performed at T = 25 °C by means of a Zetasizer Nano (Malvern Instruments). DLS
PDF
Album
Supp Info
Full Research Paper
Published 09 May 2017

Selective detection of Mg2+ ions via enhanced fluorescence emission using Au–DNA nanocomposites

  • Tanushree Basu,
  • Khyati Rana,
  • Niranjan Das and
  • Bonamali Pal

Beilstein J. Nanotechnol. 2017, 8, 762–771, doi:10.3762/bjnano.8.79

Graphical Abstract
  • AuNPs. The TEM images of AuNSs and AuNRs are shown in Figure 3, which reveal the formation of Au–DNA NCs [29]. These AuNSs were found to be separated from each other due to the CTAB coating on their surface, which renders them to have a positive charge [30]. The dynamic light scattering (DLS) results
PDF
Album
Supp Info
Full Research Paper
Published 03 Apr 2017

Dispersion of single-wall carbon nanotubes with supramolecular Congo red – properties of the complexes and mechanism of the interaction

  • Anna Jagusiak,
  • Barbara Piekarska,
  • Tomasz Pańczyk,
  • Małgorzata Jemioła-Rzemińska,
  • Elżbieta Bielańska,
  • Barbara Stopa,
  • Grzegorz Zemanek,
  • Janina Rybarska,
  • Irena Roterman and
  • Leszek Konieczny

Beilstein J. Nanotechnol. 2017, 8, 636–648, doi:10.3762/bjnano.8.68

Graphical Abstract
  • . The aim of the study was to explain the mechanism of this interaction. The interaction of CR and carbon nanotubes was studied using spectral analysis of the SWNT–CR complex, dynamic light scattering (DLS), differential scanning calorimetry (DSC) and microscopic methods: atomic force microscopy (AFM
  • complexes at increased temperature allows the aggregation of nanotubes, followed by the reassociation of CR with the surface of SWNT bundles (thus the supernatant is colourless). Dynamic light scattering analyses Dynamic light scattering (DLS) applied to SWNT–CR complexes analysis does not provide precise
  • buffers). Each set of data was analysed using NanoAnalyze software supplied by TA Instruments. Dynamic light scattering (DLS) The interaction of CR with carbon nanotubes was studied using the DynaPro NanoStar (Wyatt Technology). The measurements were done after 3 min incubation at 25 °C within the
PDF
Album
Full Research Paper
Published 16 Mar 2017
Other Beilstein-Institut Open Science Activities