Characterization of ion track-etched conical nanopores in thermal and PECVD SiO₂ using small angle X-ray scattering

• Shankar Dutt,
• Rudradeep Chakraborty,
• Christian Notthoff,
• Pablo Mota-Santiago,
• Christina Trautmann and
• Patrick Kluth

Beilstein J. Nanotechnol. 2025, 16, 899–909, doi:10.3762/bjnano.16.68

• can only be grown on a Si substrate. PECVD, in contrast, allows for the deposition at much lower temperatures on many different substrates with control over the film properties, such as stoichiometry, density, refractive index, and residual stress. As these fabrication methods involve fundamentally

• , and 12.1 keV/nm respectively, remaining almost constant throughout the film (ΔSe ≤ 0.5%). Similarly, the average Se values for PECVD SiO2 for 1.6 GeV, 185 MeV, and 89 MeV Au irradiation are 20.6, 16.3, and 11.8 keV/nm respectively, also with minimal variation across the film (ΔSe ≤ 0.5%). The

• measured the thickness etched from each film after etching in 3% HF for different defined time intervals. The thickness difference before and after etching was measured using ellipsometry, which revealed that thermal SiO2 is etched at 15.6 ± 0.6 nm/min, while PECVD SiO2 is etched at 34.3 ± 1.2 nm/min

Heat-induced transformation of nickel-coated polycrystalline diamond film studied in situ by XPS and NEXAFS

• Olga V. Sedelnikova,
• Yuliya V. Fedoseeva,
• Dmitriy V. Gorodetskiy,
• Yuri N. Palyanov,
• Elena V. Shlyakhova,
• Eugene A. Maksimovskiy,
• Anna A. Makarova,
• Lyubov G. Bulusheva and
• Aleksandr V. Okotrub

Beilstein J. Nanotechnol. 2025, 16, 887–898, doi:10.3762/bjnano.16.67

• coating on the electronic structure and chemical state of graphite layers formed on the surface of a polycrystalline diamond (PCD) film with mixed grain orientation was studied. A synthetic single-crystal diamond (SCD) with a polished (110) face was examined for comparison. The samples were coated with a

• thin nickel film deposited by thermal evaporation. The graphitization of diamond with and without a nickel coating as a result of high-vacuum annealing at a temperature of about 1100 °C was studied in situ using synchrotron-based X-ray photoelectron spectroscopy (XPS) and near-edge X-ray absorption

• fine structure (NEXAFS) methods. XPS data revealed the formation of a thin graphite-like film with low-ordered atomic structure on the surface of the nickel-coated PCD film. The chemical state of sp2-hybridized carbon atoms was found to be insensitive to the face orientation of the diamond micro-sized

Ar⁺ implantation-induced tailoring of RF-sputtered ZnO films: structural, morphological, and optical properties

• Manu Bura,
• Divya Gupta,
• Arun Kumar and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 872–886, doi:10.3762/bjnano.16.66

• promising material for device fabrication in different fields, namely, spintronics, nanoelectronics, and photonics [1][2]. It possesses a wide bandgap of 3.37 eV [3] and has a large exciton binding energy of about 60 meV [4], which assures the stability of ZnO film-based devices such as liquid crystal

• foreign ions in the ZnO film lattice can create an impact on its surface roughness and particle size. Previous reports available discuss the implantation-induced optical longitudinal phonon symmetry in ZnO films using heavy ions with high energy and low implantation fluences [12][13][14][15]. Singh et al

• . [12] observed the evolution of symmetry-forbidden and A1 (LO) modes in 120 MeV Au9+ ion-irradiated ZnO films. Ying et al. [13] described an A1 (LO) mode in the Raman spectra of energy-dependent and dose-dependent krypton ion-implanted ZnO film after varying the fluence in the range from 5 × 1013 to

Insights into the electronic and atomic structures of cerium oxide-based ultrathin films and nanostructures using high-brilliance light sources

• Paola Luches and
• Federico Boscherini

Beilstein J. Nanotechnol. 2025, 16, 860–871, doi:10.3762/bjnano.16.65

• configurations at 110 and 125 eV, respectively [23][25][26][27][28]. Figure 1 reports valence band spectra from an ultrathin cerium oxide film before and after ultrahigh vacuum (UHV) annealing at 600 °C, acquired at the two resonant energies. Using a photon energy at the Ce4+-related resonance (110 eV), the

• that form the film, while the Pt ions in the 2+ oxidation state are confined at the outermost layers [29]. The interplay of ceria surfaces with adsorbed molecules, a crucial factor in understanding reactivity, has become a significant research focus, also thanks to synchrotron-radiation-based XPS

•  3a shows a sequence of μ-XPS valence band spectra acquired using a photon at the Ce3+-related Ce 4d→Ce 4f1 resonance (hν = 120.8 eV) on a Ce0.4Zr0.6O2−x film upon removal and reintroduction of oxygen (PO2 = 1 × 10−7 mbar) in the experimental chamber. When oxygen is removed (red spectrum in Figure 3b

Synchrotron X-ray photoelectron spectroscopy study of sodium adsorption on vertically arranged MoS₂ layers coated with pyrolytic carbon

• Alexander V. Okotrub,
• Anastasiya D. Fedorenko,
• Anna A. Makarova,
• Veronica S. Sulyaeva,
• Yuliya V. Fedoseeva and
• Lyubov G. Bulusheva

Beilstein J. Nanotechnol. 2025, 16, 847–859, doi:10.3762/bjnano.16.64

• source was simultaneously deposited in vacuum on the surfaces of MoS2, pyrolytic carbon, and a hybrid sample obtained by transferring a pyrolytic carbon film onto the MoS2 film. According to XPS data, sodium easily penetrates into the space between the vertical layers of the uncoated film, and its

• interaction with MoS2 leads to the transformation of the original hexagonal structure into a distorted tetragonal one. Under the experimental conditions, sodium is unable to diffuse through the carbon film consisting of horizontally oriented graphene domains and is almost completely removed by annealing the

• sample at 773 K in ultrahigh vacuum. The presence of the underlying MoS2 film facilitates the diffusion of sodium through the graphitic coating, but not all of the deposited sodium reaches MoS2. As a result, the sodium-induced rearrangement of the carbon-coated MoS2 is less than that of the free MoS2

Facile one-step radio frequency magnetron sputtering of Ni/NiO on stainless steel for an efficient electrode for hydrogen evolution reaction

• Ha Huu Do,
• Khac Binh Nguyen,
• Phuong N. Nguyen and
• Hoai Phuong Pham

Beilstein J. Nanotechnol. 2025, 16, 837–846, doi:10.3762/bjnano.16.63

• and metal oxide phases, offering a potential for HER. These outcomes indicated the successful Ni/NiO thin film fabrication on SS substrates. The uniformity of the electrocatalyst material is a vital factor that has a direct effect on electrode performance. Scanning electron microscopy (SEM) was

• carried out to analyze the morphology of the Ni/NiO thin film on the SS substrate. The as-synthesized Ni/NiO film at 5 sccm of O2 flow rate showed uniform and continuous appearance on the entire surface of the SS substrate (Figure 2a,e). However, at high O2 flow rates, the surface of Ni/NiO/SS-10, Ni/NiO

Supramolecular hydration structure of graphene-based hydrogels: density functional theory, green chemistry and interface application

• Hon Nhien Le,
• Duy Khanh Nguyen,
• Minh Triet Dang,
• Huyen Trinh Nguyen,
• Thi Bang Tam Dao,
• Trung Do Nguyen,
• Chi Nhan Ha Thuc and
• Van Hieu Le

Beilstein J. Nanotechnol. 2025, 16, 806–822, doi:10.3762/bjnano.16.61

• hydroxide hydrogel on polylactide film At first, commercial polylactide granules (PLA Luminy LX175, TotalEnergies Corbion) was put in a steel mold for thermal compression at 190 °C to produce a PLA plate. A piece of the PLA plate was put in a thin plastic mold (polyethylene terephthalate) for thermal

• drawing in Figure 2c is the presentation of a graphene-based nanosheet with a first bound water layer which is responsible for the primary hydration force. In the next stage, after brush coating of the GO-SG-ZH hydrogel on a polylactide film, hydration shells are evaporated in the drying process, and the

• coatings of SG and GO-SG-PLA were formed on the plastic substrates. Regarding appearance, while the blank PLA film was clearly transparent (Figure 7a), the SG/PLA film was slightly opaque (Figure 7b), and the GO-SG-ZH/PLA film was stripy with black lines of GO color (Figure 7c). Light transmittance spectra

Morphology and properties of pyrite nanoparticles obtained by pulsed laser ablation in liquid and thin films for photodetection

• Akshana Parameswaran Sreekala,
• Bindu Krishnan,
• Rene Fabian Cienfuegos Pelaes,
• David Avellaneda Avellaneda,
• Josué Amílcar Aguilar-Martínez and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 785–805, doi:10.3762/bjnano.16.60

• synthesized by PLAL. FeS2 NPs were successfully synthesized in five different solvents, along with a minor phase of iron sulfide (FeS). Additionally, by combining electrophoretic deposition and spin-coating techniques, thin film photodiodes of FeS2 were fabricated on an n-type Si substrate utilizing the

• detectivity in the order of 106–108 Jones is attained. The FeS2/n-Si photodetector works in self-powered mode also in addition to the photoconductive mode. The results show the effective fabrication of nanostructured ultraviolet–visible–near infrared thin film photodetectors using semiconductor nanocolloids

• performance by first fabricating amorphous iron oxide films on normal glass substrates by spray pyrolysis followed by heating in sulfur atmosphere at 350 and 400 °C [20]. For pyrite film fabrication, solvothermal or hydrothermal and chemical synthetic routes are generally adopted [21][22][23]. Henríquez et al

Synthesis of a multicomponent cellulose-based adsorbent for tetracycline removal from aquaculture water

• Uyen Bao Tran,
• Ngoc Thanh Vo-Tran,
• Khai The Truong,
• Dat Anh Nguyen,
• Quang Nhat Tran,
• Huu-Quang Nguyen,
• Jaebeom Lee and
• Hai Son Truong-Lam

Beilstein J. Nanotechnol. 2025, 16, 728–739, doi:10.3762/bjnano.16.56

• significant morphological changes compared to pristine CMC (Figure 2a–c). Specifically, the PGC surface exhibits numerous, uniformly distributed spherical nanoparticles (≈200 nm in diameter), attributed to ZnO nanoparticles. The initial tubular structure of CMC is converted into a film-like structure owing to

High-temperature epitaxial growth of tantalum nitride thin films on MgO: structural evolution and potential for SQUID applications

• Michelle Cedillo Rosillo,
• Oscar Contreras López,
• Jesús Antonio Díaz,
• Agustín Conde Gallardo and
• Harvi A. Castillo Cuero

Beilstein J. Nanotechnol. 2025, 16, 690–699, doi:10.3762/bjnano.16.53

• the present work, superconducting TaN thin films were synthesized using PLD. A high-purity Ta target was ablated in a N2 atmosphere while the N2 pressure was varied to investigate its effect on film properties. The substrate temperature was systematically altered to explore its impact on the growth

• temperature and N2 pressure. This optimization aimed to achieve a low oxygen concentration in the films, surpassing levels reported by other researchers. Low oxygen content is crucial for exhibiting superconducting properties and potentially enhancing Tc. Among the fabricated samples, the film deposited at

• deposition chamber, and a turbo pump was used to pump the gas out during film deposition. The films were transferred to the analysis chamber to characterize them in situ by XPS. Varying the N2 pressure, pN2, in the chamber and analyzing the films, we obtained TaN thin films at 90 mTorr of N2. XPS data were

Colloidal few layered graphene–tannic acid preserves the biocompatibility of periodontal ligament cells

• Teissir Ben Ammar,
• Naji Kharouf,
• Dominique Vautier,
• Housseinou Ba,
• Nivedita Sudheer,
• Philippe Lavalle and
• Vincent Ball

Beilstein J. Nanotechnol. 2025, 16, 664–677, doi:10.3762/bjnano.16.51

• was calculated using the formula where A represents the absorbance of DPPH and B represents the absorbance of the DPPH and TA combination. A similar experiment was conducted to assess the antioxidant activity of FLG–TA deposited on quartz in the form of a film. In this parallel examination, the

• deposited film was put in contact with a 10−4 M DPPH solution in the absence of light, followed by the absorbance measurement at 517 nm. Biological assays Isolation and culture of PDL cells PDL cells were isolated from human alveolar ligament obtained from extracted human teeth. This study was conducted

Nanoscale capacitance spectroscopy based on multifrequency electrostatic force microscopy

• Pascal N. Rohrbeck,
• Lukas D. Cavar,
• Franjo Weber,
• Peter G. Reichel,
• Mara Niebling and
• Stefan A. L. Weber

Beilstein J. Nanotechnol. 2025, 16, 637–651, doi:10.3762/bjnano.16.49

• ][56][57][58][59][60][61][62][63][64][65][66][67][68][69][70][71][72][73]. Compared to optical ellipsometry or reflectance spectroscopy, SCM and SCFM can map surface properties such as film thickness [35][39] and dielectric constants [35][74], with superior spatial resolution. However, in particular

A formulation containing Cymbopogon flexuosus essential oil: improvement of biochemical parameters and oxidative stress in diabetic rats

• Ailton Santos Sena-Júnior,
• Cleverton Nascimento Santana Andrade,
• Pedro Henrique Macedo Moura,
• Jocsã Hémany Cândido dos Santos,
• Cauãn Torres Trancoso,
• Eloia Emanuelly Dias Silva,
• Deise Maria Rego Rodrigues Silva,
• Ênio Pereira Telles,
• Luiz André Santos Silva,
• Isabella Lima Dantas Teles,
• Sara Fernanda Mota de Almeida,
• Daniel Alves de Souza,
• Jileno Ferreira Santos,
• Felipe José Aidar Martins,
• Ana Mara de Oliveira e Silva,
• Sandra Lauton-Santos,
• Guilherme Rodolfo Souza de Araujo,
• Cristiane Bani Correa,
• Rogéria De Souza Nunes,
• Lysandro Pinto Borges and
• Ana Amélia Moreira Lira

Beilstein J. Nanotechnol. 2025, 16, 617–636, doi:10.3762/bjnano.16.48

• , 0.25 μm film thickness) was used for compound separation, with helium as a 99.999% pure carrier gas (White Martins SA) at a flow rate of 1 mL/min and a split/splitless autoinjector. For the analysis, a solution of EOCF was prepared at a concentration of approximately 10 mg/mL using hexane as a solvent

Polyurethane/silk fibroin-based electrospun membranes for wound healing and skin substitute applications

• Iqra Zainab,
• Zohra Naseem,
• Syeda Rubab Batool,
• Muhammad Waqas,
• Ahsan Nazir and
• Muhammad Anwaar Nazeer

Beilstein J. Nanotechnol. 2025, 16, 591–612, doi:10.3762/bjnano.16.46

• hemostatic agent for trauma treatment [107]. Patil et al. explored three types of silk forms, namely, regular film, lamellar porous film, and electrospun silk nanofibers for wound dressings. Factors such as solvent solution, electric field intensity, spinning distance, and SF concentration affected the

• can be classified as gold–polydopamine blackspheres (AuPBs), capable of absorbing NIR-II light and converting it into heat. These particles were incorporated into an electrospun film by combining poly(ʟ-lactic acid) (PLLA) with SF to obtain a PLLA-SF parallel films. The films had high strength and

Retrieval of B1 phase from high-pressure B2 phase for CdO nanoparticles by electronic excitations in Cd_xZn_1−xO composite thin films

• Arkaprava Das,
• Marcin Zając and
• Carla Bittencourt

Beilstein J. Nanotechnol. 2025, 16, 551–560, doi:10.3762/bjnano.16.43

• . The irradiation was performed with 120 MeV Ag and 80 MeV O ions. Two different fluences were used for each ion type (i.e., 1 × 1013 ions/cm2 and 3 × 1013 ions/cm2). The focus of this study is on a film that underwent a complete transformation to the B2 phase, which is designated as a pristine thin

• film prior to further irradiation. The characterization of the thin films was performed using X-ray diffraction (XRD) on a Bruker high-resolution X-ray diffractometer, employing a Cu Kα beam over a 2θ range of 30–50°. Raman spectroscopic measurements were conducted at room temperature with a SENTERRA

• mode. Table 1 summarizes the irradiation ion energies and fluences for each thin film, along with their corresponding labels. Results and Discussion Influence of Ag and O ion irradiation on crystallographic phase by X-ray diffraction and Raman spectroscopy Figure 1a shows the XRD patterns illustrating

Electron beam-based direct writing of nanostructures using a palladium β-ketoesterate complex

• Chinmai Sai Jureddy,
• Krzysztof Maćkosz,
• Aleksandra Butrymowicz-Kubiak,
• Iwona B. Szymańska,
• Patrik Hoffmann and
• Ivo Utke

Beilstein J. Nanotechnol. 2025, 16, 530–539, doi:10.3762/bjnano.16.41

• of the thin focused electron beam (FEB) deposit containing Pd, C, and O without substrate interference (native silicon oxide and silicon), the SAMx Stratagem thin film correction software, based on the work by Pouchou and Pichoir [43] was employed. Stratagem needs k-ratios (i.e., the ratio of X-ray

• these k-ratios, Stratagem then recalculates the composition for a thin film (multi)layered structure. The native-oxide Si(100) substrate was accounted for by including a 1 nm thick SiO2 layer of density 2.65 g·cm−3 between the Si substrate and the deposit for the thin film correction. This way, the

• prepared on an ultrathin carbon support film spanning a lacey carbon membrane (Figure 2c). The deposit appears smeared because of drift caused by charging effects during the deposition process. High-resolution STEM imaging (Figure 2d,e) revealed a granular nanostructure with nanograins of around 2 nm in

N₂⁺-implantation-induced tailoring of structural, morphological, optical, and electrical characteristics of sputtered molybdenum thin films

• Usha Rani,
• Kafi Devi,
• Divya Gupta and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 495–509, doi:10.3762/bjnano.16.38

• thickness of the as-deposited films. This pattern persists with film thickness even after N2+ implantation. After implantation, crystallinity decreases relative to as-deposited films with the same nominal thickness. The AFM analysis reveals that RMS roughness increases with the thickness of Mo films

• . Optical studies using spectroscopic ellipsometry reveal a significant increase in absorbance and reflectance in as-deposited and N2+-implanted films. Electrical investigations show that the conductivity increases with film thickness in both as-deposited and implanted films. The conductivity decreases for

• the same nominal film thickness after implantation. Keywords: atomic force microscopy; grazing angle X-ray diffractometer; Keithley parametric analyzer; Mo thin films; RF sputtering; spectroscopic ellipsometry; Introduction Molybdenum thin films have garnered significant attention in diverse

Impact of adsorbate–substrate interaction on nanostructured thin films growth during low-pressure condensation

• Alina V. Dvornichenko,
• Vasyl O. Kharchenko and
• Dmitrii O. Kharchenko

Beilstein J. Nanotechnol. 2025, 16, 473–483, doi:10.3762/bjnano.16.36

• well-defined islands or clusters. The strength and nature of these interactions play a pivotal role in determining whether the film growth follows layer-by-layer (Frank–van der Merwe) or island (Volmer–Weber) growth modes [22]. Therefore, central to achieving the control the type and size of surface

• , even for monoatomic layers [34]. The patterns may serve as templates for the later evolution of film textures. Relevant examples of such systems are Al or Cu layers deposited on Si substrates, or SiO2 and TiN layers deposited on Ti or Al substrates [31]. In this article, we perform a computational

• adsorbate matrix due to the percolating structure of the adsorbate. Summarizing, one can conclude that the effects of adsorbate–substrate interactions during nanostructured thin film growth at low-pressure deposition are profound and multifaceted. Understanding and controlling these interactions are

ReactorAFM/STM – dynamic reactions on surfaces at elevated temperature and atmospheric pressure

• Tycho Roorda,
• Hamed Achour,
• Matthijs A. van Spronsen,
• Marta E. Cañas-Ventura,
• Sander B. Roobol,
• Willem Onderwaater,
• Mirthe Bergman,
• Peter van der Tuijn,
• Gertjan van Baarle,
• Johan W. Bakker,
• Joost W. M. Frenken and
• Irene M. N. Groot

Beilstein J. Nanotechnol. 2025, 16, 397–406, doi:10.3762/bjnano.16.30

• voltage of −1 V applied to the sample. RMS surface roughness and RMS current for each image are, correspondingly, (a) 0.17 nm, (b) 50 pA, (c) 0.63 nm, and (d) 760 pA. AFM images of cobalt nanoparticles on a thick (50 nm) Al2O3 film taken (a) before reaction, at RT and high vacuum, (b) at 430 K and 2 bar

• data of various product gases as a function of time during heating and cooling cobalt nanoparticles on a 50 nm thick Al2O3 film. Data shown for masses of m/z 18, 30, 44, and 86, which correspond to water (as byproduct), ethane, propane, and hexane, respectively. Funding We acknowledge funding from the

Tailoring of physical properties of RF-sputtered ZnTe films: role of substrate temperature

• Kafi Devi,
• Usha Rani,
• Arun Kumar,
• Divya Gupta and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 333–348, doi:10.3762/bjnano.16.25

• crystallinity, high transmittance, and high conductivity of the ZnTe film produced at 600 °C make it a suitable candidate for use as a buffer layer in solar cell applications. Keywords: bandgap; physical properties; RF sputtering; substrate temperature; ZnTe; Introduction The industrialization and burning of

• ][18][19][20][21][22][23] which show that chemical composition and morphology of the substrate affect the properties of grown films. Therefore, a suitable substrate needs to selected before the deposition of films. The thermal expansion coefficient of substrate and the lattice mismatch between film and

• substrate are two important parameters for substrate selection. To the best of our knowledge, studies related to the impact of the substrate (silicon and quartz) and film deposition temperature up to 600 °C on the structural, morphological, optical, and electrical behaviour of RF-sputtered ZnTe films are

Enhancing mechanical properties of chitosan/PVA electrospun nanofibers: a comprehensive review

• Nur Areisman Mohd Salleh,
• Amalina Muhammad Afifi,
• Fathiah Mohamed Zuki and
• Hanna Sofia SalehHudin

Beilstein J. Nanotechnol. 2025, 16, 286–307, doi:10.3762/bjnano.16.22

• electrospinning only PVA, and preparing a separate film containing aloe vera and chitosan using a film applicator. The electrospun PVA was then layered on top of the aloe vera/chitosan film to improve mechanical properties. The chitosan/aloe vera film fabricated using this method, however, is in the form of a non

• -fibrous thin film; hence. it may not suit applications that highly depend on the properties of a nanofibrous structure, such as large surface area-to-volume ratio or high permeability of the material. Similarly, Kang et al. [110] fabricated chitosan-coated PVA nanofibers by coating the heat-treated PVA

Recent advances in photothermal nanomaterials for ophthalmic applications

• Jiayuan Zhuang,
• Linhui Jia,
• Chenghao Li,
• Rui Yang,
• Jiapeng Wang,
• Wen-an Wang,
• Heng Zhou and
• Xiangxia Luo

Beilstein J. Nanotechnol. 2025, 16, 195–215, doi:10.3762/bjnano.16.16

• sufficiently soft film to tightly cover the tissue can ensure direct contact between the VNBs produced by the film and tumor cells. The experimental results indicate that using more and higher-energy laser pulses produces more and larger vapor bubbles, which can kill cells at some distance from the film. A

A review of metal-organic frameworks and polymers in mixed matrix membranes for CO₂ capture

• Charlotte Skjold Qvist Christensen,
• Nicholas Hansen,
• Mahboubeh Motadayen,
• Nina Lock,
• Martin Lahn Henriksen and
• Jonathan Quinson

Beilstein J. Nanotechnol. 2025, 16, 155–186, doi:10.3762/bjnano.16.14

• of MOF-based MMMs in a general context have been published by Lin et al. [27] and Kitao and coworkers [28]. Focusing on gas separation in general, Daglar et al. [29] have summarized computational approaches to simulate gas transport in thin-film MOF membranes and MOF-based MMMs. With an emphasis on

TiO₂ immobilized on 2D mordenite: effect of hydrolysis conditions on structural, textural, and optical characteristics of the nanocomposites

• Marina G. Shelyapina,
• Rosario Isidro Yocupicio-Gaxiola,
• Gleb A. Valkovsky and
• Vitalii Petranovskii

Beilstein J. Nanotechnol. 2025, 16, 128–140, doi:10.3762/bjnano.16.12

• . For a correct transformation of relative pressure (P/P0) to t, we used the formulas proposed in [38][39] for hierarchical microporous/mesoporous zeolites. In this method, a linear fit at low thickness of adsorbate film (low relative pressure) provides the micropore volume Vmicro (the intercept) and

Characterization of ZnO nanoparticles synthesized using probiotic Lactiplantibacillus plantarum GP258

• Prashantkumar Siddappa Chakra,
• Aishwarya Banakar,
• Shriram Narayan Puranik,
• Vishwas Kaveeshwar,
• C. R. Ravikumar and
• Devaraja Gayathri

Beilstein J. Nanotechnol. 2025, 16, 78–89, doi:10.3762/bjnano.16.8

• ZnO NPs confirms the XRD results, that is, the hexagonal wurtzite structure (Figure 3). SEM and EDX analysis SEM was used to analyze the surface morphology of a modified nanocomposite film, and the image displays a consistent coverage of a web-like structure. Close-up views revealed a crumpled and

• analysis. TEM was employed to study the shape, size, and distribution of the ZnO NPs. FESEM analysis showed a web-like structure with defined diameters; EDX spectroscopy confirmed the presence of ZnO NPs on the film surface. Zeta potential measurements and DLS analysis were conducted using the SZ-100