Two-step laser synthesis of Ag@TiO₂ nanomaterials for the photocatalytic degradation of rhodamine B

• Marija Kovačević,
• Miloš Tošić,
• Rafaela Radičić,
• Vladimir Rajić,
• Nikša Krstulović,
• Miloš Momčilović and
• Sanja Živković

Beilstein J. Nanotechnol. 2026, 17, 622–634, doi:10.3762/bjnano.17.43

• photocatalyst (Ag@TiO2 200p or Ag@TiO2 2000p) was deposited onto a carbon-coated copper grid and left to dry under ambient conditions. ImageJ software, version 1.54 g, was used for image analysis and interplanar distance computations. Measurements of particle size distribution, zeta potential, and

• electrophoretic mobility Hydrodynamic size distribution and zeta potential of the nanoparticles were measured using a Zetasizer Ultra (Malvern Panalytical, Malvern, Worcestershire, UK). Disposable plastic cuvettes were employed for size distribution analysis, while capillary cells were used for zeta potential and

• ) Cross-sectional TEM micrographs, (b, e) HRTEM images, and (c, f) SAED diffraction patterns of, respectively, Ag@TiO2 200p and Ag@TiO2 2000p NPs. STEM-HAADF images and STEM-EDS compositional maps of titanium, oxygen, and silver of synthesized (a) Ag@TiO2 200p and (b) Ag@TiO2 2000p NPs. Particle size

Laser–material interactions in liquids for the synthesis of nanomaterials: current status and perspectives

• Carlos Doñate Buendia,
• Bilal Gökce and
• Leonid V. Zhigilei

Beilstein J. Nanotechnol. 2026, 17, 571–575, doi:10.3762/bjnano.17.38

• broadly, beam shaping techniques are gaining attention as a means to improve process control and efficiency [24]. For example, non-Gaussian beam profiles, such as donut-shaped beams, have been shown to modify the nanoparticle size distribution [71]. The balance between implementation complexity, cost

Probing internal continua and atomic ultrafast charge transfer within size-controlled nanoparticles by post-collision interaction in core-hole clock spectroscopy

• Johannes Lütgert,
• Erika Giangrisostomi,
• Nomi L. A. N. Sorgenfrei and
• Alexander Föhlisch

Beilstein J. Nanotechnol. 2026, 17, 505–514, doi:10.3762/bjnano.17.33

• nanoparticles via a line-shape analysis revealing post-collision interaction (PCI) effects within the conduction band continuum. We investigate CdSe/ZnS core–shell nanoparticles with a constant CdSe core size of 3.5 nm and varying shell thicknesses of ZnS that allow for atomic layer control with narrow size

• distribution. As indicated below in Figure 1, resonant Auger electron spectra are used to determine atomic charge transfer times based on the branching into localized and delocalized final states during the core-hole lifetime. We observe a significant reduction of charge transfer times within the ZnS shell for

Upcycling agroindustrial waste into graphene oxide supports for gold nanoparticles: toward sustainable nanomaterials

• Juan Marcos Castro-Tapia,
• Selene Acosta,
• Hiram Joazet Ojeda-Galván,
• Elsie Evelyn Araujo-Palomo,
• Edgar Giovanni Villabona-Leal and
• Mildred Quintana

Beilstein J. Nanotechnol. 2026, 17, 489–504, doi:10.3762/bjnano.17.32

• uniform size distribution before pyrolysis. Synthesis of graphene oxide GO was synthesized using the Hummers' method as modified by Marcano and coworkers [9]. Briefly, 3 g of graphite were added to a flask containing a H2SO4/H3PO4 mixture, followed by the gradual addition of 18 g of KMnO4. The reaction

• sites, resulting in the sparse, agglomerated AuNPs observed in Agro-GOC. The final panel of each row shows high-magnification views of spherical AuNPs with diameters ranging from 6.9 to 10.9 nm, consistent with the particle-size distribution analysis. The average particle sizes were 6.9 ± 2.2 nm (AuNP

• -based materials. Each row represents a hybrid: (a–d) AuNPs@GO, (e–h) AuNPs@rGO, (i–l) AuNPs@Agro-GOP, (m–p) AuNPs@Agro-GOX, and (q–t) AuNPs@Agro-GOC. Columns show increasing magnifications of each sample. Particle size distribution histograms of AuNPs deposited on GO platforms. Relative atomic

Defects and defect-mediated engineering of two-dimensional materials: challenges and open questions

• Arkady V. Krasheninnikov,
• Matthias Batzill,
• Anouar-Akacha Delenda,
• Marija Drndić,
• Chris Ewels,
• Katharina J. Franke,
• Mahdi Ghorbani-Asl,
• Alexander Holleitner,
• Ado Jorio,
• Ute Kaiser,
• Daria Kieczka,
• Hannu-Pekka Komsa,
• Jani Kotakoski,
• Manuel Längle,
• David Lamprecht,
• Yun Liu,
• Steven G. Louie,
• Janina Maultzsch,
• Thomas Michely,
• Katherine Milton,
• Anna Niggas,
• Hanako Okuno,
• Joshua A. Robinson,
• Marika Schleberger,
• Bruno Schuler,
• Alexander Shluger,
• Kazu Suenaga,
• Kristian S. Thygesen,
• Richard A. Wilhelm,
• E. Harriet Åhlgren and
• Carla Bittencourt

Beilstein J. Nanotechnol. 2026, 17, 454–488, doi:10.3762/bjnano.17.31

• host vacancy clusters. The clusters are also size-limited, as clusters growing too large and into the bright areas would force Gr bonds to detach from the substrate. Therefore, vacancies diffusing around avoid attachment to large clusters and prefer to attach to smaller ones, making the size

• distribution rather uniform. The average vacancy cluster size in Figure 9a is twelve vacancies. A similar mechanism of vacancy cluster self-organization applies to the moiré of h-BN with Ir(111) [157]. Figure 9d displays the pristine h-BN moiré with pronounced bright spots. Upon 500 eV He+ ion irradiation at

Nanocarrier-integrated multilayer films produced by 3D printing for improved skin adhesion and curcumin photostability

• Thayse Viana de Oliveira,
• Ana Paula Farias Leão,
• Júlia Leão,
• Cesar Liberato Petzhold and
• Ruy Carlos Ruver Beck

Beilstein J. Nanotechnol. 2026, 17, 440–453, doi:10.3762/bjnano.17.30

• effective photostabilization. Discussion Based on the observed physicochemical properties (Table 2), the formulations developed in the present study exhibited a low polydispersity index and a z-average particle size below 240 nm, indicating a narrow nanometric size distribution. All tested formulations

• conditioning. Furthermore, morphological assessment was performed at both the nano- and the macroscale, using particle size distribution, polydispersity index, and zeta potential as indirect indicators of nanocapsule structural organization, while the morphology and integrity of the multilayer 3D-printed films

Beam shaping techniques for pulsed laser ablation in liquids: Unlocking tunable control of nanoparticle synthesis in liquids

• Sergio Molina-Prados,
• Nadezhda M. Bulgakova,
• Alexander V. Bulgakov,
• Jesus Lancis,
• Gladys Mínguez Vega and
• Carlos Doñate-Buendia

Beilstein J. Nanotechnol. 2026, 17, 309–342, doi:10.3762/bjnano.17.22

• size distribution is also affected by the fluence, obtaining smaller NPs for low fluences of 0.5–4.0 J·cm−2 [130][131][132]. The NP composition is also affected by the fluence. An increase of the laser energy leads to a higher concentration of gas, for example oxygen atoms, that increase O content in

• laser beam has been shown to allow for better control of NP size and to offer an advantage in terms of alignment and reproducibility due to the long length of the central lobe of the Bessel beam [142]. A narrow size distribution of Ag NPs obtained by femtosecond Bessel beam irradiation of a silver

• significantly reduced NP size, narrowed size distribution, and improved sphericity. The NPs’ size distribution shows only weak dependence on pulse energy. No significant variation of the Au NP size distribution was observed using 85 and 217 µJ pulses [158]. Instead, the observed effects are linked to the

Gold nanoparticle-decorated reduced graphene oxide as a highly effective catalyst for the selective α,β-dehydrogenation of N-alkyl-4-piperidones

• Brenda Flore Kenyim,
• Mihir Tzalis,
• Marilyn Kaul,
• Robert Oestreich,
• Aysenur Limon,
• Chancellin Pecheu Nkepdep and
• Christoph Janiak

Beilstein J. Nanotechnol. 2026, 17, 218–238, doi:10.3762/bjnano.17.15

• scattering (DLS) measurements was 12 nm (Figure 4b). Transmission electron microscopy (TEM) analysis showed spherical and well-dispersed nanoparticles and their particle size distribution (Figure 4c), based on the measurements of approximately 200 nanoparticles, yielded an average diameter of 12 nm with a

Safe and sustainable by design with ML/AI: A transformative approach to advancing nanotechnology

• Georgia Melagraki

Beilstein J. Nanotechnol. 2026, 17, 176–185, doi:10.3762/bjnano.17.11

• and sustainability considerations into nanomaterial development. Need for harmonized testing protocols Establishing standardized and reproducible methodologies for characterizing nanomaterial properties – such as size distribution, surface chemistry, and toxicity profiles – is essential. A unified

Influence of surface characteristics on the in vitro stability and cell uptake of nanoliposomes for brain delivery

• Dushko Shalabalija,
• Ljubica Mihailova,
• Nikola Geskovski,
• Andreas Zimmer,
• Otmar Geiss,
• Sabrina Gioria,
• Diletta Scaccabarozzi and
• Marija Glavas Dodov

Beilstein J. Nanotechnol. 2026, 17, 139–158, doi:10.3762/bjnano.17.9

• qualitatively confirmed by spectrophotometry (e.g., by the absence of fluorescence in the supernatant obtained in the last washing cycle), ensuring that the fluorescence signal in subsequent experiments originates exclusively from liposome-associated dye. Particle size, particle size distribution and z

• highlight the dominant independent variables that have a significant effect in the model, the VIP score was used. Results and Discussion Particle size, particle size distribution and z-potential of the nanoliposomes Several studies have reported that despite the composition and the other surface properties

• ranged from 115–130 nm with PDI < 0.3 (Table 1), which indicates a narrow unimodal size distribution of the NLs in all formulations. According to the literature data, liposomal nanovesicles from 100 to 140 nm exhibit longer half-life in blood circulation and avoid of PC formation when compared those of

Development and in vitro evaluation of liposomes and immunoliposomes containing 5-fluorouracil and R-phycoerythrin as a potential phototheranostic system for colorectal cancer

• Raissa Rodrigues Camelo,
• Vivianne Cortez Sombra Vandesmet,
• Octavio Vital Baccallini,
• José de Brito Vieira Neto,
• Thais da Silva Moreira,
• Luzia Kalyne Almeida Moreira Leal,
• Claudia Pessoa,
• Daniel Giuliano Cerri,
• Maria Vitória Lopes Badra Bentley,
• Josimar O. Eloy,
• Ivanildo José da Silva Júnior and
• Raquel Petrilli

Beilstein J. Nanotechnol. 2026, 17, 97–121, doi:10.3762/bjnano.17.7

• bilayers [38][43][44]. The vesicle size distribution graphs obtained by DLS show that the presence of bimodal peaks in the liposome formulations is associated with higher PDI values. For example, the blank formulation of DPPC 50 exhibited a PDI of 0.31, with two distinct populations: one with an average

Quantitative estimation of nanoparticle/substrate adhesion by atomic force microscopy

• Aydan Çiçek,
• Markus Kratzer,
• Christian Teichert and
• Christian Mitterer

Beilstein J. Nanotechnol. 2026, 17, 1–14, doi:10.3762/bjnano.17.1

• . Since it is assumed that NPs are single-charged [5], the QMF can, on the one hand, be used for scanning the NP mass distribution and, under the common assumption of spherical shape and the theoretical density of Cu, the size distribution. On the other hand, the QMF can be also be employed for filtering

Internal 3D temperature mapping in biological systems using ratiometric light-sheet imaging and lipid-coated upconversion nanothermometers

• Dannareli Barron-Ortiz,
• Enric Pérez-Parets,
• Rubén D. Cadena-Nava,
• Emilio J. Gualda,
• Jacob Licea-Rodríguez,
• Juan Hernández-Cordero,
• Pablo Loza-Álvarez and
• Israel Rocha-Mendoza

Beilstein J. Nanotechnol. 2025, 16, 2306–2316, doi:10.3762/bjnano.16.159

• thin-film hydration method based on Rojas-Gutierrez’s procedure [52]. Based on the size distribution and concentration of the nanoparticles (10 mg·mL−1), a lipid layer was formed with DOPS, cholesterol, and DMPC at a molar ratio of 64:29:7. The three lipids were dispersed in chloroform and mixed with

• with the lipid-functionalized UCNPs (inset), revealing a size distribution of approximately 15–20 nm. Because the lipid shell is an ultrathin organic layer (2–3 nm) with low electron contrast, no distinct morphological differences are expected between coated and uncoated nanoparticles in TEM images

Improving magnetic properties of Mn- and Zn-doped core–shell iron oxide nanoparticles by tuning their size

• Dounia Louaguef,
• Ghouti Medjahdi,
• Sébastien Diliberto,
• Klaus M. Seemann,
• Thomas Gries,
• Joelle Bizeau,
• Damien Mertz,
• Eric Gaffet and
• Halima Alem

Beilstein J. Nanotechnol. 2025, 16, 2285–2295, doi:10.3762/bjnano.16.157

• average size of approximately 40 nm. The size distribution histogram (Figure 1b) confirms the uniformity of particle sizes, while a magnified image (Figure 1c) highlights the polyhedral morphology. The selected-area electron diffraction pattern (Figure 1d) exhibits distinct diffraction spots that can be

• –shell spinel ferrites for magnetic hyperthermia and related biomedical applications. (a) TEM images (bright field) of Zn0.4Fe2.6O4 NPs (40 nm). (b) Size distribution histogram of Zn0.4Fe2.6O4 NPs. (c) Zoom on the framed part in yellow (a). (d) HRTEM image of Zn0.4Fe2.6O4 NPs. (e) Diffraction pattern of

Optical bio/chemical sensors for vitamin B₁₂ analysis in food and pharmaceuticals: state of the art, challenges, and future outlooks

• Seyed Mohammad Taghi Gharibzahedi and
• Zeynep Altintas

Beilstein J. Nanotechnol. 2025, 16, 2207–2244, doi:10.3762/bjnano.16.153

• AuNP suspensions is substantially influenced by their particle size and dispersion speed. 10–20 nm AuNPs with a narrow size distribution tend to absorb light from the blue-green spectrum and reflect red light. In contrast, their aggregation leads to a light absorption shift to longer wavelengths

Ultrathin water layers on mannosylated gold nanoparticles

• Maiara A. Iriarte Alonso,
• Jorge H. Melillo,
• Silvina Cerveny,
• Yujin Tong and
• Alexander M. Bittner

Beilstein J. Nanotechnol. 2025, 16, 2183–2198, doi:10.3762/bjnano.16.151

• , while size and morphology under completely dry conditions were measured by electron microscopy. DLS yields a hydrodynamic diameter of the PEG AuNPs of 67.7 ± 9.4 nm and a polydispersity index (PDI) of 0.35. However, the size distribution (Figure 2) reaches a maximum at 41.1 ± 4.2 nm. In contrast, the

• concentration of carboxylate) exhibit a lower ZP (approx. −45 mV) at the same pH [1]. To obtain a clearer view of the size distribution, we used SEM to evaluate particle sizes and morphologies in high vacuum (i.e., for completely dried samples). By adjusting a Gaussian fit to the histograms (Figure 3), the

Quality by design optimization of microemulsions for topical delivery of Passiflora setacea seed oil

• Daniel T. Pereira,
• Douglas Dourado,
• Danielle T. Freire,
• Dayanne L. Porto,
• Cícero F. S. Aragão,
• Myla L. de Souza,
• Guilherme R. S. de Araujo,
• Ana Maria Costa,
• Wógenes N. Oliveira,
• Anne Sapin-Minet,
• Éverton N. Alencar and
• Eryvaldo Sócrates T. Egito

Beilstein J. Nanotechnol. 2025, 16, 2116–2131, doi:10.3762/bjnano.16.146

• accurately reflect the true droplet size distribution in the MEgel. This phenomenon is evident from the apparent increase in mean hydrodynamic diameter to 45.1 nm and PdI to 0.27, which is attributed to NaCMC matrix scattering rather than actual droplet growth [40]. A comparison of the hydrodynamic diameter

Rapid synthesis of highly monodisperse AgSbS₂ nanocrystals: unveiling multifaceted activities in cancer therapy, antibacterial strategies, and antioxidant defense

• Funda Ulusu,
• Adem Sarilmaz,
• Yakup Ulusu,
• Faruk Ozel and
• Mahmut Kus

Beilstein J. Nanotechnol. 2025, 16, 2105–2115, doi:10.3762/bjnano.16.145

• , indicating robust crystallization. Moreover, the presence of prominent peaks aligning with (220), (311), (420), and (511) planes confirmed alignment with XRD results. Furthermore, utilizing particle size distribution analysis, the crystallite size of average particles was estimated, as illustrated in the

• inset in Figure 2c. The particle size distribution graphs in this image unequivocally affirmed the successful attainment of the desired homogeneity. Biological applications Antibacterial activity of AgSbS2 NCs Disc diffusion. The antimicrobial activity of AgSbS2 NCs at a concentration of 10 mg/mL

Stereodiscrimination of guests in chiral organosilica aerogels studied by ESR spectroscopy

• Sebastian Polarz,
• Yasar Krysiak,
• Martin Wessig and
• Florian Kuhlmann

Beilstein J. Nanotechnol. 2025, 16, 2034–2054, doi:10.3762/bjnano.16.140

Laser ablation in liquids for shape-tailored synthesis of nanomaterials: status and challenges

• Natalie Tarasenka

Beilstein J. Nanotechnol. 2025, 16, 1963–1997, doi:10.3762/bjnano.16.137

• of NP size and size distribution. As a result, the crucial experimental parameters were determined providing strategies to reduce the formation of large NPs and to produce monodisperse small nanocrystals [1][5]. However, the goal of controlled nanomaterials synthesis by PLAL is still not completely

PEGylated lipids in lipid nanoparticle delivery dynamics and therapeutic innovation

• Peiyang Gao

Beilstein J. Nanotechnol. 2025, 16, 1914–1930, doi:10.3762/bjnano.16.133

• particle size decreasing from 173.9 nm at 1 mol % to 109.1 nm at 5 mol %. Meanwhile, the PDI increased modestly from 0.060 to 0.146 with the increase of PEG density from 1 to 5 mol %, indicating a slight broadening in size distribution and less LNP homogeneity at higher PEG levels. The surface charge on

• ]. Some PEG lipids exhibit sensitivity in encapsulation efficiency at higher PEG molar fraction, while others can maintain stable payload encapsulation regardless of PEG density. Likewise, changes in size distribution and surface charge can be modest or pronounced depending on the specific PEG lipid

Targeting the vector of arboviruses Aedes aegypti with nanoemulsions based on essential oils: a review with focus on larvicidal and repellent properties

• Laryssa Ferreira do Nascimento Silva,
• Douglas Dourado,
• Thayse Silva Medeiros,
• Mariana Alice Gonzaga Gabú,
• Maria Cecilia Queiroga dos Santos,
• Daiane Rodrigues dos Santos,
• Mylena Lemos dos Santos,
• Gabriel Bezerra Faierstein,
• Rosângela Maria Rodrigues Barbosa and
• Fabio Rocha Formiga

Beilstein J. Nanotechnol. 2025, 16, 1894–1913, doi:10.3762/bjnano.16.132

Phytol-loaded soybean oil nanoemulsion as a promising alternative against Leishmania amazonensis

• Victória Louise Pinto Freire,
• Mariana Farias Alves-Silva,
• Johny W. de Freitas Oliveira,
• Matheus de Freitas Fernandes-Pedrosa,
• Alianda Maira Cornélio,
• Marcelo de Souza-Silva,
• Thayse Silva Medeiros and
• Arnóbio Antônio da Silva Junior

Beilstein J. Nanotechnol. 2025, 16, 1826–1836, doi:10.3762/bjnano.16.126

• shown in the size distribution graph (Figure 1b). Moreover, the zeta potential (ZP) of both samples was around −20 mV, with no significant changes upon phytol loading. To evaluate the shape and morphological characteristics of the nanoemulsions, transmission electron microscopy (TEM) analysis was

• performed. The results revealed nanodroplets with spherical and oval shapes and a homogeneous size distribution, with diameters up to 250 nm, consistent with the dynamic light scattering (DLS) data (Figure 1c,d). Colloidal and physicochemical stability The colloidal and physicochemical stability of the NEs

• considered statistically significant for p < 0.05. Schematic illustration of PHYT-NE preparation: (a) size distribution of nanodroplets (b) and morphological aspects of blank-NE (c) and PHYT-NE (d). Figure 1a) is adapted from Servier Medical Art (https://smart.servier.com/), licensed under CC BY 4.0 (https

Multifunctional anionic nanoemulsion with linseed oil and lecithin: a preliminary approach for dry eye disease

• Niédja Fittipaldi Vasconcelos,
• Almerinda Agrelli,
• Rayane Cristine Santos da Silva,
• Carina Lucena Mendes-Marques,
• Isabel Renata de Souza Arruda,
• Priscilla Stela Santana de Oliveira,
• Mércia Liane de Oliveira and
• Giovanna Machado

Beilstein J. Nanotechnol. 2025, 16, 1711–1733, doi:10.3762/bjnano.16.120

• resulting formulations, including their thermodynamic stability, size distribution, and optical clarity [47][48]. The packing parameter concept (PPC) provides a theoretical framework for predicting the geometry of amphiphilic systems, based on the ratio of the surfactant molecule’s total volume, the area of

Prospects of nanotechnology and natural products for cancer and immunotherapy

• Jan Filipe Andrade Santos,
• Marcela Bernardes Brasileiro,
• Pamela Danielle Cavalcante Barreto,
• Ligiane Aranha Rocha and
• José Adão Carvalho Nascimento Júnior

Beilstein J. Nanotechnol. 2025, 16, 1644–1667, doi:10.3762/bjnano.16.116

• inhibition of cancer cell migration, invasion, and metastasis [122][123]. The patent characterizes the NPs through DLS and TEM, confirming a uniform size distribution. Additionally, in vitro studies using MCF-7 breast cancer cells demonstrated inhibition of cell proliferation, with the NP inducing apoptosis

• nanoparticles demonstrated stability, spherical shape, and homogeneous size distribution. The use of nanoparticles with sterol compounds associated with Ce6 yielded higher tumor inhibition rates compared to the isolated compounds, especially the nanocarrier with ergosterol, which reached a rate of 86.4% [27][64