Electrical and optical enhancement of ITO/Mo bilayer thin films via laser annealing

• Abdelbaki Hacini,
• Ahmad Hadi Ali,
• Nurul Nadia Adnan and
• Nafarizal Nayan

Beilstein J. Nanotechnol. 2022, 13, 1589–1595, doi:10.3762/bjnano.13.133

• structural results show that both the as-deposited and the annealed ITO/Mo thin films have a polycrystalline structure, and that the annealing treatment enhanced the crystallinity of samples. Moreover, the XRD patterns exhibited a cubic structure preferentially oriented along the (222) and (400) planes. The

• samples show a polycrystalline structure crystallized in a cubic structure (JCPDS:71-2194) [28]. However, the sample treated with 240 mJ shows an amorphous structure because of the high energy that diffuses gas atoms from the chamber into the surface [29]. The obtained peaks correspond to ITO. It can be

• analyses show that the ITO/Mo has a polycrystalline structure. As well, it can be seen from the grain size analysis that the energy of 120 mJ gives the highest grain size and good crystallinity because most of the orientation of the crystallites appears in the XRD results. Figure 5 shows the optical

Structural studies and selected physical investigations of LiCoO₂ obtained by combustion synthesis

• Monika Michalska,
• Paweł Ławniczak,
• Tomasz Strachowski,
• Adam Ostrowski and
• Waldemar Bednarski

Beilstein J. Nanotechnol. 2022, 13, 1473–1482, doi:10.3762/bjnano.13.121

• the investigated LiCoO2 polycrystalline samples were studied using impedance spectroscopy. The measurements were performed for seven samples annealed at selected temperatures, that is, 450, 500, 550, 650, 700, 750, and 900 °C. The typical impedance response of the studied materials is presented in

• constants is related to the microstructure of the studied material as the sample is constructed from pressed powder material of different sizes. A response consisting of two semicircles is often observed in polycrystalline samples of ion conductors and ceramics [66][67]. It is related to two different

Enhanced electronic transport properties of Te roll-like nanostructures

• E. R. Viana,
• N. Cifuentes and
• J. C. González

Beilstein J. Nanotechnol. 2022, 13, 1284–1291, doi:10.3762/bjnano.13.106

• under mild conditions. A large quantity of these polycrystalline nanostructures with a diameter between 100 and 900 nm and a wall thickness around 50 nm were synthesized and characterized by scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), transmission electron microscopy

• the anisotropy of the Te crystal structure [20][21]. However, a fast Fourier transform (FFT) analysis of different areas of the HRTEM images (see Figure 3a) shows that the nanostructures are polycrystalline, with well-oriented large grains and rotated small grains at the edges. Small amorphous areas

A cantilever-based, ultrahigh-vacuum, low-temperature scanning probe instrument for multidimensional scanning force microscopy

• Hao Liu,
• Zuned Ahmed,
• Sasa Vranjkovic,
• Manfred Parschau,
• Andrada-Oana Mandru and
• Hans J. Hug

Beilstein J. Nanotechnol. 2022, 13, 1120–1140, doi:10.3762/bjnano.13.95

• for the coating of high-quality factor cantilevers for magnetic force microscopy [29]. In future work, much thinner coating thicknesses could be used, or the coating could be applied to the cantilever side to reduce energy dissipation processes arising from the grain boundaries of the polycrystalline

Investigation of electron-induced cross-linking of self-assembled monolayers by scanning tunneling microscopy

• Patrick Stohmann,
• Sascha Koch,
• Yang Yang,
• Christopher David Kaiser,
• Julian Ehrens,
• Jürgen Schnack,
• Niklas Biere,
• Dario Anselmetti,
• Armin Gölzhäuser and
• Xianghui Zhang

Beilstein J. Nanotechnol. 2022, 13, 462–471, doi:10.3762/bjnano.13.39

• V and +0.4 to +1.2 V. A z-resolution higher than 0.01 nm could be achieved. The STM tips were prepared from 0.375 mm polycrystalline tungsten wire (Alfa Aesar) by electrochemical etching in a 3 M NaOH solution. The instrument was calibrated by imaging HOPG with atomic resolution. The data was post

A non-enzymatic electrochemical hydrogen peroxide sensor based on copper oxide nanostructures

• Irena Mihailova,
• Vjaceslavs Gerbreders,
• Marina Krasovska,
• Eriks Sledevskis,
• Valdis Mizers,
• Andrejs Bulanovs and
• Andrejs Ogurcovs

Beilstein J. Nanotechnol. 2022, 13, 424–436, doi:10.3762/bjnano.13.35

• ) shows the surface morphology of a thermally obtained copper oxide film. The resulting film is a homogeneous, polycrystalline oxide layer consisting of grains of arbitrary shape. In practice, this layer exhibits poor adhesion to the surface and can be easily damaged mechanically during post-processing

Electrostatic pull-in application in flexible devices: A review

• Teng Cai,
• Yuming Fang,
• Yingli Fang,
• Ruozhou Li,
• Ying Yu and
• Mingyang Huang

Beilstein J. Nanotechnol. 2022, 13, 390–403, doi:10.3762/bjnano.13.32

• structure. The bridge monolayer graphene electrode is 20 µm long and 3 µm wide, the electrode gap is 500 nm, and the pull-in voltage is less than 5 V. As the electrode material was polycrystalline graphene, fracture of the GR electrode was observed after 4–5 life cycles, resulting in device failure. In 2018

• to the removal of grain boundaries, the single-crystal GR devices are four times more capable of handling current than polycrystalline GR devices. Shen et al. [71] prepared GR ESD switches and analyzed their electrical characteristics and reliability. The switch did work only once. Therefore, ESD

Controllable two- and three-state magnetization switching in single-layer epitaxial Pd_1−xFe_x films and an epitaxial Pd_0.92Fe_0.08/Ag/Pd_0.96Fe_0.04 heterostructure

• Igor V. Yanilkin,
• Amir I. Gumarov,
• Gulnaz F. Gizzatullina,
• Roman V. Yusupov and
• Lenar R. Tagirov

Beilstein J. Nanotechnol. 2022, 13, 334–343, doi:10.3762/bjnano.13.28

• ): 0 Oe → −36 Oe. In both cases, on a time scale of approx. 1000 s, there are no noticeable changes in the magnetic moment of the steady states of the heterostructure. This is fundamentally different from the dynamics of the magnetization of the polycrystalline Pd0.99Fe0.01 film, in which significant

Investigation of a memory effect in a Au/(Ti–Cu)Ox-gradient thin film/TiAlV structure

• Damian Wojcieszak,
• Jarosław Domaradzki,
• Michał Mazur,
• Tomasz Kotwica and
• Danuta Kaczmarek

Beilstein J. Nanotechnol. 2022, 13, 265–273, doi:10.3762/bjnano.13.21

• three areas: (1) a polycrystalline area located from the surface to the near center of the structure, (2) an amorphous area located from the center to the near-substrate region, and (3) a void-rich area located from the near-substrate to the substrate region. In the middle of the structure there is a

Low-energy electron interaction and focused electron beam-induced deposition of molybdenum hexacarbonyl (Mo(CO)₆)

• Po-Yuan Shih,
• Maicol Cipriani,
• Christian Felix Hermanns,
• Jens Oster,
• Klaus Edinger,
• Armin Gölzhäuser and
• Oddur Ingólfsson

Beilstein J. Nanotechnol. 2022, 13, 182–191, doi:10.3762/bjnano.13.13

• ®. Energy-dispersive X-ray analyses was done with a ZEISS Crossbeam system with an integrated Oxford EDX detector. Deposits for EDX analysis were prepared on a 100 nm thick polycrystalline gold substrate on a 4 inch silicon wafer, purchased from Georg Albert PVD. The Au-based substrate was chosen because of

• sum of the relative contributions of all Mo-containing fragments. Using this approach, we found that DEA leads to an average weighted CO loss per incident of about 1.2 while DI leads to an average weighted CO loss of 3.7. For comparison FEBID deposits were created on a polycrystalline gold substrate

• . Elemental composition of Mo(CO)6 FEBID deposits obtained by EDX measurement of a 1 μm2 pad deposited on a 100 nm thick polycrystalline gold substrate on a 4 inch silicon wafer. Funding This project has received funding from the European Union’s Horizon 2020 research and innovation programme under the Marie

Design aspects of Bi₂Sr₂CaCu₂O_8+δ THz sources: optimization of thermal and radiative properties

• Mikhail M. Krasnov,
• Natalia D. Novikova,
• Roger Cattaneo,
• Alexey A. Kalenyuk and
• Vladimir M. Krasnov

Beilstein J. Nanotechnol. 2021, 12, 1392–1403, doi:10.3762/bjnano.12.103

• of the other two materials, namely Bi-2212 and polycrystalline gold electrodes. At low T both have linear κ(T). For Bi-2212 we assume κab(T) = 0.1 T(K) W·K−1·m−1 [45] with an anisotropy κab/κc = 8 [46]. For a polycrystalline gold thin film we use κ(T) = 3 T(K) W·K−1·m−1 [32]. The heat is produced in

Revealing the formation mechanism and band gap tuning of Sb₂S₃ nanoparticles

• Maximilian Joschko,
• Franck Yvan Fotue Wafo,
• Christina Malsi,
• Danilo Kisić,
• Ivana Validžić and
• Christina Graf

Beilstein J. Nanotechnol. 2021, 12, 1021–1033, doi:10.3762/bjnano.12.76

• et al., who evaluated the accuracy of the Tauc plot for 120 individual analyses of polycrystalline ZnO and found a deviation of about 0.03 eV [52]. XRD For XRD measurements, a minimum amount of 10 mg of dried particles was used. The samples were measured in a capillary in transmission geometry. Two

The role of deep eutectic solvents and carrageenan in synthesizing biocompatible anisotropic metal nanoparticles

• Nabojit Das,
• Akash Kumar and
• Raja Gopal Rayavarapu

Beilstein J. Nanotechnol. 2021, 12, 924–938, doi:10.3762/bjnano.12.69

• nanocrystals with high-index {771} facets. The nanoparticles with high-index planes exhibited higher catalytic activity due to high density of atoms with low coordination number compared to nanoparticles with low-index facets such as {100}, {111}, or {110}. Chirea et al. synthesized polycrystalline gold

Effects of temperature and repeat layer spacing on mechanical properties of graphene/polycrystalline copper nanolaminated composites under shear loading

• Chia-Wei Huang,
• Man-Ping Chang and
• Te-Hua Fang

Beilstein J. Nanotechnol. 2021, 12, 863–877, doi:10.3762/bjnano.12.65

• Chia-Wei Huang Man-Ping Chang Te-Hua Fang Department of Mechanical Engineering, National Kaohsiung University of Science and Technology, Kaohsiung 807618, Taiwan 10.3762/bjnano.12.65 Abstract In the present study, the characteristics of graphene/polycrystalline copper nanolaminated (GPCuNL

• ]. The competition between interface and matrix in deformation and failure of a nanolayered polycrystalline Cu–graphene material has been reported [26]. In 2018, Weng et al. reported the potential strengthening mechanism of graphene/copper composites under compression. The results show that the

• this work, we focus on temperature and microstructure effects on graphene/polycrystalline copper nanolaminated (GPCuNL) composites. As mentioned above, the microstructure plays a crucial role for the mechanical behavior of GPCuNL composites. Thus, in the present study, molecular dynamics (MD

9.1% efficient zinc oxide/silicon solar cells on a 50 μm thick Si absorber

• Rafal Pietruszka,
• Bartlomiej S. Witkowski,
• Monika Ozga,
• Katarzyna Gwozdz,
• Ewa Placzek-Popko and
• Marek Godlewski

Beilstein J. Nanotechnol. 2021, 12, 766–774, doi:10.3762/bjnano.12.60

• prepared by the Fraunhofer Institute (Germany), the solar cells (SCs) market is dominated by silicon [2]. In 2019, monocrystalline, polycrystalline, and amorphous silicon accounted for about 95% of the PV market. The highest (laboratory device) efficiency for monocrystalline and polycrystalline silicon

A review of defect engineering, ion implantation, and nanofabrication using the helium ion microscope

• Frances I. Allen

Beilstein J. Nanotechnol. 2021, 12, 633–664, doi:10.3762/bjnano.12.52

High-yield synthesis of silver nanowires for transparent conducting PET films

• Gul Naz,
• Hafsa Asghar,
• Muhammad Ramzan,
• Muhammad Arshad,
• Rashid Ahmed,
• Muhammad Bilal Tahir,
• Bakhtiar Ul Haq,
• Nadeem Baig and
• Junaid Jalil

Beilstein J. Nanotechnol. 2021, 12, 624–632, doi:10.3762/bjnano.12.51

• , template reduction (hard and soft templates), and ultrasonic reduction methods [17][18][19][20][21][22]. Lithographic and hard template methods are used to prepare silver nanowires with well-defined dimensions but both methods produce polycrystalline silver nanowires with rough surface, triggering

Impact of GaAs(100) surface preparation on EQE of AZO/Al₂O₃/p-GaAs photovoltaic structures

• Piotr Caban,
• Rafał Pietruszka,
• Jarosław Kaszewski,
• Monika Ożga,
• Bartłomiej S. Witkowski,
• Krzysztof Kopalko,
• Piotr Kuźmiuk,
• Katarzyna Gwóźdź,
• Ewa Płaczek-Popko,
• Krystyna Lawniczak-Jablonska and
• Marek Godlewski

Beilstein J. Nanotechnol. 2021, 12, 578–592, doi:10.3762/bjnano.12.48

• B series, respectively. From the AFM results shown in Figure 3 and Figure 4, one can see that A1, A2, A4, B1, and B4 samples exhibit uniform surfaces by the means of polycrystalline thin film topography. By taking into consideration the roughness of the surfaces (RMS was measured for an area of 4

Structural and optical characteristics determined by the sputtering deposition conditions of oxide thin films

• Petronela Prepelita,
• Florin Garoi and
• Valentin Craciun

Beilstein J. Nanotechnol. 2021, 12, 354–365, doi:10.3762/bjnano.12.29

• was done to determine the type of structure (e.g., polycrystalline or amorphous) and orientation of the thin films. Figure 1 shows typical XRD patterns of ZnO thin films with increasing thickness and prepared via rfMS. Following the effect of the deposition parameters of the oxide films we found that

Atomic layer deposited films of Al₂O₃ on fluorine-doped tin oxide electrodes: stability and barrier properties

• Hana Krýsová,
• Michael Neumann-Spallart,
• Hana Tarábková,
• Pavel Janda,
• Ladislav Kavan and
• Josef Krýsa

Beilstein J. Nanotechnol. 2021, 12, 24–34, doi:10.3762/bjnano.12.2

• amorphous to polycrystalline γ-Al2O3 [12] or to oriented θ-Al2O3 [13]. However, on thermodynamic grounds, alumina is soluble in both acidic and alkaline media [8]. Besides protection, Al2O3 ALD layers have also been used for passivating surface states on water-oxidizing hematite photoanodes [14][15]. Very

Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector

• Eduardo Serralta,
• Nico Klingner,
• Olivier De Castro,
• Michael Mousley,
• Santhana Eswara,
• Serge Duarte Pinto,
• Tom Wirtz and
• Gregor Hlawacek

Beilstein J. Nanotechnol. 2020, 11, 1854–1864, doi:10.3762/bjnano.11.167

• also detect channeling-related contrast on polycrystalline silicon, thallium chloride nanocrystals, and single-crystalline silicon by comparing the signal transmitted at different directions for the same data set. Keywords: bright-field; channeling; dark-field; delay line detector; helium ion

• transmission-channeling contrast using polycrystalline silicon, thallium chloride samples and beam steering in single-crystalline silicon. Experimental The new STIM detector comprises a stack of two MCPs and a resistive anode layer with a delay line readout structure behind it, as represented in Figure 1c. The

• responsible for the observed mismatch. Beam steering and channeling Polycrystalline silicon A 15 nm thick nanoporous polycrystalline silicon membrane (available from Electron Microscopy Sciences, item number: 76042–79) has been investigated using STIM. In Figure 4b–f we present several STIM images, which were

Molecular dynamics modeling of the influence forming process parameters on the structure and morphology of a superconducting spin valve

• Alexander Vakhrushev,
• Aleksey Fedotov,
• Vladimir Boian,
• Roman Morari and
• Anatolie Sidorenko

Beilstein J. Nanotechnol. 2020, 11, 1776–1788, doi:10.3762/bjnano.11.160

• structure of each layer does not form an ideal single crystal, but rather a polycrystalline system is formed. The influence of the interface quality on the spin valve functionality is an especially important issue, which has been experimentally investigated in previous works [16][17][18][19] where the

• nanosystem resulting from the mathematical modeling is presented in Figure 5. Figure 5 clearly demonstrates the niobium and cobalt layered nanosystem formation: the layers formed by niobium and cobalt atoms have a polycrystalline structure. In this case, groups of atoms are combined into domains with

High-responsivity hybrid α-Ag₂S/Si photodetector prepared by pulsed laser ablation in liquid

• Raid A. Ismail,
• Hanan A. Rawdhan and
• Duha S. Ahmed

Beilstein J. Nanotechnol. 2020, 11, 1596–1607, doi:10.3762/bjnano.11.142

• (SEM), energy-dispersive X-ray spectroscopy (EDX), and UV–vis spectroscopy. The optical absorption decreased and the optical energy gap of α-Ag2S increased from 1.5 to 2 eV after the CTAB surfactant was added to the Tu solution. XRD studies revealed that the synthesized Ag2S NPs were polycrystalline

Atomic defect classification of the H–Si(100) surface through multi-mode scanning probe microscopy

• Jeremiah Croshaw,
• Thomas Dienel,
• Taleana Huff and
• Robert Wolkow

Beilstein J. Nanotechnol. 2020, 11, 1346–1360, doi:10.3762/bjnano.11.119

• . Methods Experiments were performed using an Omicron LT STM and an Omicron qPlus LT AFM [88][89] system operating at 4.5 K and ultrahigh vacuum (3 × 10−11 Torr). STM tips were electrochemically etched from polycrystalline tungsten wire, resistively heated, and field-evaporated to clean and sharpen the apex

Proximity effect in [Nb(1.5 nm)/Fe(x)]₁₀/Nb(50 nm) superconductor/ferromagnet heterostructures

• Yury Khaydukov,
• Sabine Pütter,
• Laura Guasco,
• Roman Morari,
• Gideok Kim,
• Thomas Keller,
• Anatolie Sidorenko and
• Bernhard Keimer

Beilstein J. Nanotechnol. 2020, 11, 1254–1263, doi:10.3762/bjnano.11.109

• thickness from 2 to 4 nm improves the film quality. The Fe layer becomes polycrystalline while the Nb layer remains amorphous. In contrast, for sample s6, which was grown on the 30 °C Nb buffer, both layers reveal polycrystallinity with a certain texture (Figure 2e,f). Finally, the Pt cap is always

• polycrystalline (Figure 2b). X-ray diffraction Figure 3a shows the diffraction pattern measured on sample s3. Together with two reflections from the substrate we observed a Nb(200) peak at 2θ = 55°with mosaicity of the same order as the substrate peak. In agreement with the observation by RHEED (Figure 4b) we

• observed that the Nb(200) peak is tilted off-specular by a few degrees, which is a well-known feature of Nb growth on Al2O3() substrates [45][46]. Similar patterns were measured for all samples, except for sample s6, which was grown at room temperature. For this sample we measured a typical polycrystalline