Functional morphology of cleaning devices in the damselfly Ischnura elegans (Odonata, Coenagrionidae)

• Silvana Piersanti,
• Gianandrea Salerno,
• Wencke Krings,
• Stanislav Gorb and
• Manuela Rebora

Beilstein J. Nanotechnol. 2024, 15, 1260–1272, doi:10.3762/bjnano.15.102

• Abstract Among the different micro- and nanostructures located on cuticular surfaces, grooming devices represent fundamental tools for insect survival. The present study describes the grooming microstructures of the damselfly Ischnura elegans (Odonata, Coenagrionidae) at the adult stage. These structures

• portion and from the seta to the cuticular lamina. The removal of the grooming devices induces a strong increase in the contaminated areas on the eyes after grooming. Further studies on insect grooming can provide valuable data on the functional morphology of insect micro- and nanostructures and can

• tasks through the presence of micro- and nanostructures located on its cuticular surface, serving functions from sensory reception to surface adhesion, air retention, food grinding, thermoregulation, and color production (reviews in [4][5]). The insect cuticle is frequently exposed to a variety of

Realizing active targeting in cancer nanomedicine with ultrasmall nanoparticles

• André F. Lima,
• Giselle Z. Justo and
• Alioscka A. Sousa

Beilstein J. Nanotechnol. 2024, 15, 1208–1226, doi:10.3762/bjnano.15.98

• unique class of nanostructures for cancer nanomedicine, offering the potential to address significant limitations associated with larger particles, particularly in treating solid tumors. The incorporation of active targeting ligands onto usNPs holds the potential to enhance their performance in cancer

Synthesis, characterization and anticancer effect of doxorubicin-loaded dual stimuli-responsive smart nanopolymers

• Ömür Acet,
• Pavel Kirsanov,
• Burcu Önal Acet,
• Inessa Halets-Bui,
• Dzmitry Shcharbin,
• Şeyda Ceylan Cömert and
• Mehmet Odabaşı

Beilstein J. Nanotechnol. 2024, 15, 1189–1196, doi:10.3762/bjnano.15.96

• . Characterizations of the synthesized nanostructures were carried out including zeta potential measurements, Fourier-transform infrared spectroscopy, and scanning electron microscopy. The loading capacity of the nanopolymers for DOX was investigated, and encapsulation and release studies were carried out. In a final

• [9]. Certain designs in nanostructures are extremely useful to combat diseases [12][13]. Polymeric platforms have attracted great interest in recent years [14][15][16][17][18][19][20]. “Stimulus-sensitive” polymers (smart polymers) exhibit conformational changes or phase transition behavior in

• Centrifugen, USA). The precipitated nanostructures were redispersed in distilled water utilizing a sonicator and dried with a lyophilizer. Then, the nanostructures were stored at 4 °C. Characterization studies Functional group analysis was carried out by Fourier-transform infrared (FTIR) spectroscopy

AI-assisted models to predict chemotherapy drugs modified with C₆₀ fullerene derivatives

• Jonathan-Siu-Loong Robles-Hernández,
• Dora Iliana Medina,
• Katerin Aguirre-Hurtado,
• Marlene Bosquez,
• Roberto Salcedo and
• Alan Miralrio

Beilstein J. Nanotechnol. 2024, 15, 1170–1188, doi:10.3762/bjnano.15.95

• treatments that release substances at specific sites of interest, reducing the required drug amount and side effects. Nanostructures to form these drug delivery systems can be divided into organic and inorganic [19][20], with the latter one being the less extensively studied. One option currently considered

Local work function on graphene nanoribbons

• Daniel Rothhardt,
• Amina Kimouche,
• Tillmann Klamroth and
• Regina Hoffmann-Vogel

Beilstein J. Nanotechnol. 2024, 15, 1125–1131, doi:10.3762/bjnano.15.91

• ] and p-doping by Bi, Sb, and Au substrates [2]. Confining graphene to nanostructures [6][7], for example, to graphene nanoribbons (GNRs), that is, few nanometers wide stripes of graphene, opens additional possibilities of tuning the electronic properties by creating quantum-confined states [8] and

Direct electron beam writing of silver using a β-diketonate precursor: first insights

• Katja Höflich,
• Krzysztof Maćkosz,
• Chinmai S. Jureddy,
• Aleksei Tsarapkin and
• Ivo Utke

Beilstein J. Nanotechnol. 2024, 15, 1117–1124, doi:10.3762/bjnano.15.90

• Katja Hoflich Krzysztof Mackosz Chinmai S. Jureddy Aleksei Tsarapkin Ivo Utke Ferdinand-Braun-Institut (FBH), Gustav-Kirchhoff-Str. 4, 12489 Berlin, Germany Laboratory of Mechanics for Materials and Nanostructures, Empa – Swiss Federal Laboratories for Material Science and Technology

• , Feuerwerkerstrasse 39, CH 3602 Thun, Switzerland 10.3762/bjnano.15.90 Abstract Direct electron beam writing is a powerful tool for fabricating complex nanostructures in a single step. The electron beam locally cleaves the molecules of an adsorbed gaseous precursor to form a deposit, similar to 3D printing but

• . Keywords: focused electron beam-induced deposition; precursor; silver nanostructures; Introduction Direct writing with an electron beam allows for single-step and maskfree 3D printing of sophisticated nanostructures at the nanoscale [1][2][3][4]. The process relies on the electron beam-induced

Unveiling the potential of alginate-based nanomaterials in sensing technology and smart delivery applications

• Shakhzodjon Uzokboev,
• Khojimukhammad Akhmadbekov,
• Ra’no Nuritdinova,
• Salah M. Tawfik and
• Yong-Ill Lee

Beilstein J. Nanotechnol. 2024, 15, 1077–1104, doi:10.3762/bjnano.15.88

• , to mitigate limitations of simple nanostructures such as low stability and unsuitable drug release features. They investigated capsaicin-loaded alginate nanoparticles embedded in polycaprolactone–chitosan nanofiber mats. This DDS can extend the release time of capsaicin to more than 500 h compared to

Ca_n neutral clusters: a two-step G₀W₀ and DFT benchmark

• Sunila Bakhsh,
• Sameen Aslam,
• Muhammad Khalid,
• Muhammad Sohail,
• Sundas Zafar,
• Sumayya Abdul Wadood,
• Kareem Morsy and
• Muhammad Aamir Iqbal

Beilstein J. Nanotechnol. 2024, 15, 1010–1016, doi:10.3762/bjnano.15.82

• predict the new ground-state structure of Be and Mg and successfully applied to obtain the correct IPs for these elemental clusters [15][16]. This comprehensive benchmark study will help to enhance our understanding of these fascinating nanostructures and lead to their real-world utilization in various

Atomistic insights into the morphological dynamics of gold and platinum nanoparticles: MD simulations in vacuum and aqueous media

• Evangelos Voyiatzis,
• Eugenia Valsami-Jones and
• Antreas Afantitis

Beilstein J. Nanotechnol. 2024, 15, 995–1009, doi:10.3762/bjnano.15.81

• ] nanostructures. We also simulated Au and Pt NPs in aqueous solutions at 300 K, that is, close to room temperature. The interactions among the water molecules are described by the SPC/E model [66]. The interactions among the water molecules and the Au (Pt) atoms are calculated by the force field of Merabia et al

Water-assisted purification during electron beam-induced deposition of platinum and gold

• Cristiano Glessi,
• Fabian A. Polman and
• Cornelis W. Hagen

Beilstein J. Nanotechnol. 2024, 15, 884–896, doi:10.3762/bjnano.15.73

• Cristiano Glessi Fabian A. Polman Cornelis W. Hagen Delft University of Technology, Fac. Applied Sciences, Dept. Imaging Physics, Lorentzweg 1, 2628CJ Delft, Netherlands 10.3762/bjnano.15.73 Abstract Direct fabrication of pure metallic nanostructures is one of the main aims of focused electron

• ) is a nanofabrication technique that allows for the direct writing of three-dimensional nanostructures [1][2][3]. In FEBID, a gaseous precursor, often an organometallic compound, is injected in the vacuum chamber of a scanning electron microscope (SEM), adsorbed on a substrate, and dissociated by a

• pure gold structures in a single process step using the co-injection of the precursor Au(tfac)Me2 and water. This inspired the present work, in which we aim for the direct deposition of high-purity Au and Pt nanostructures achieved through the co-injection of water and the precursors Au(acac)Me2 and

A review on the structural characterization of nanomaterials for nano-QSAR models

• Salvador Moncho,
• Eva Serrano-Candelas,
• Jesús Vicente de Julián-Ortiz and
• Rafael Gozalbes

Beilstein J. Nanotechnol. 2024, 15, 854–866, doi:10.3762/bjnano.15.71

• light scattering (DLS) is another technique that can be used to describe the hydrodynamic size or the aggregation of the nanoforms in larger nanostructures, depending on the medium and other conditions. In some cases, the size values reported in the papers are not measured on purpose, but are the

Synthesis of silver–palladium Janus nanoparticles using co-sputtering of independent sources: experimental and theorical study

• Maria J. Martínez-Carreón,
• Francisco Solís-Pomar,
• Abel Fundora,
• Claudio D. Gutiérrez-Lazos,
• Sergio Mejía-Rosales,
• Hector N. Fernández-Escamilla,
• Jonathan Guerrero-Sánchez,
• Manuel F. Meléndrez and
• Eduardo Pérez-Tijerina

Beilstein J. Nanotechnol. 2024, 15, 808–816, doi:10.3762/bjnano.15.67

• , confirmed the presence of Janus-type nanostructures. Results of molecular dynamics and TEM simulations show that the differences between the crystalline structures of the Pd and Ag regions observed in the TEM micrographs can be explained by small mismatches in the orientations of the two regions of the

Electron-induced ligand loss from iron tetracarbonyl methyl acrylate

• Hlib Lyshchuk,
• Atul Chaudhary,
• Thomas F. M. Luxford,
• Miloš Ranković,
• Jaroslav Kočišek,
• Juraj Fedor,
• Lisa McElwee-White and
• Pamir Nag

Beilstein J. Nanotechnol. 2024, 15, 797–807, doi:10.3762/bjnano.15.66

• (FEBID). FEBID is an emerging method for the fabrication of 3D nanostructures. It relies on the local decomposition of precursors in the focal area of an electron beam [1][2][3][4]. In the case of deposition of metals, the interaction with the electrons should ideally lead to a cleavage of all metal

• represents perhaps the “cleanest” approach since it probes the reaction of one precursor molecule with at most one electron, without environmental influences (e.g., precursor–precursor or precursor–substrate effects). The possibility of making iron nanostructures is important mainly because of their magnetic

Effect of repeating hydrothermal growth processes and rapid thermal annealing on CuO thin film properties

• Monika Ozga,
• Eunika Zielony,
• Aleksandra Wierzbicka,
• Anna Wolska,
• Marcin Klepka,
• Marek Godlewski,
• Bogdan J. Kowalski and
• Bartłomiej S. Witkowski

Beilstein J. Nanotechnol. 2024, 15, 743–754, doi:10.3762/bjnano.15.62

• -cleaning [1], anti-corrosion [2], and antibacterial [3] coatings. Like other CuO nanostructures, thin films also show potential for applications in photovoltaic cells [4][5], lithium-ion batteries [6], supercapacitors [7], gas sensors [8], and biosensors [9]. Furthermore, the literature reports their

Level set simulation of focused ion beam sputtering of a multilayer substrate

• Alexander V. Rumyantsev,
• Nikolai I. Borgardt,
• Roman L. Volkov and
• Yuri A. Chaplygin

Beilstein J. Nanotechnol. 2024, 15, 733–742, doi:10.3762/bjnano.15.61

• of the prepared boxes was 1 × 1 μm2, and the dwell time value was set at 4.9 ms. The number of the ion beam passes was varied from M = 1 to M = 3. This corresponded to ion fluences from 7.5·1017 to 2.3·1018 cm−2 and resulted in nanostructures with aspect ratios from approximately 1.0 to 1.7 in a

Elastic modulus of β-Ga₂O₃ nanowires measured by resonance and three-point bending techniques

• Annamarija Trausa,
• Sven Oras,
• Sergei Vlassov,
• Mikk Antsov,
• Tauno Tiirats,
• Andreas Kyritsakis,
• Boris Polyakov and
• Edgars Butanovs

Beilstein J. Nanotechnol. 2024, 15, 704–712, doi:10.3762/bjnano.15.58

• , University of Tartu, Nooruse 1, 50411 Tartu, Estonia Estonian Military Academy, Riia 12, 51010 Tartu, Estonia 10.3762/bjnano.15.58 Abstract Due to the recent interest in ultrawide bandgap β-Ga2O3 thin films and nanostructures for various electronics and UV device applications, it is important to understand

• dimensions, particularly at the lower resolution limit [18]. The low symmetry of monoclinic crystal systems, as in the β-Ga2O3 case, might promote the growth of nanostructures with different crystalline orientations, which often leads to the formation of nanostructures with various dimensions, such as NWs

• , studies by Luan et al. [23] have revealed the elastic anisotropy in β-Ga2O3, highlighting the strong directional dependence of Young’s modulus. Available studies hint that various factors could strongly influence the mechanical properties of Ga2O3 one-dimensional nanostructures, which merits to be

Gold nanomakura: nanoarchitectonics and their photothermal response in association with carrageenan hydrogels

• Nabojit Das,
• Vikas,
• Akash Kumar,
• Sanjeev Soni and
• Raja Gopal Rayavarapu

Beilstein J. Nanotechnol. 2024, 15, 678–693, doi:10.3762/bjnano.15.56

• temperature rise for DTAB-AuNR and CTAB-AuNR was attained up to ≈11.3 and ≈9.9 °C, respectively. Discussion In this work, we adopted a seed-mediated approach to synthesize anisotropic nanostructures, viz., pillow shaped named as nanomakura (makura is a Japanese word meaning “pillow”). Surfactants belonging to

• different in terms of synthesis protocol and chemical constituents used. The main synthesis goal of this work was to study the effect of the carbon tail length of surfactants on the morphology of the synthesized nanostructures. Thus, keeping every parameter constant except the surfactant type during the

• reaction was paramount. The AgNO3 to ascorbic acid ratio was kept uniform in respective growth solutions containing CTAB, MTAB, and DTAB of the same concentration to facilitate longitudinal growth of the nanostructures. The disappearance of the yellow colour into a transparent growth solution upon

Laser synthesis of nanoparticles in organic solvents – products, reactions, and perspectives

• Theo Fromme,
• Sven Reichenberger,
• Katharine M. Tibbetts and
• Stephan Barcikowski

Beilstein J. Nanotechnol. 2024, 15, 638–663, doi:10.3762/bjnano.15.54

Exfoliation of titanium nitride using a non-thermal plasma process

• Priscila Jussiane Zambiazi,
• Dolores Ribeiro Ricci Lazar,
• Larissa Otubo,
• Rodrigo Fernando Brambilla de Souza,
• Almir Oliveira Neto and
• Cecilia Chaves Guedes-Silva

Beilstein J. Nanotechnol. 2024, 15, 631–637, doi:10.3762/bjnano.15.53

• and Konstantin Novoselov in 2004 [1], the field of nanostructures has witnessed remarkable advancements. Various methods to fabricate graphene, such as mechanical and chemical exfoliation, combined with innovative characterization techniques, have enabled the preparation of diverse layered two

Directed growth of quinacridone chains on the vicinal Ag(35 1 1) surface

• Niklas Humberg,
• Lukas Grönwoldt and
• Moritz Sokolowski

Beilstein J. Nanotechnol. 2024, 15, 556–568, doi:10.3762/bjnano.15.48

• step edges. Keywords: Ag(100); intermolecular hydrogen bonds; one-dimensional aggregates; organic nanostructures; quinacridone; step-molecule interactions; vicinal surface; Introduction A versatile and powerful method to create nanostructures on surfaces is the self-assembly of atoms and molecules

• . Here, the physical and chemical properties of the substrate and the adsorbate are the key that can be tuned to create nanostructures that fit specific needs [1][2][3][4]. A research focus over the recent years has been the self-assembly of molecules or atoms into one-dimensional (1D) linear aggregates

• , which can be used to direct the growth of nanostructures of adsorbates. The adsorption at step edges, as opposed to that on the terraces in between, is often favored because the additional interactions between the adsorbate and the atoms of the step edge contribute to the adsorption energy Eads. This

Electron-induced deposition using Fe(CO)₄MA and Fe(CO)₅ – effect of MA ligand and process conditions

• Hannah Boeckers,
• Atul Chaudhary,
• Petra Martinović,
• Amy V. Walker,
• Lisa McElwee-White and
• Petra Swiderek

Beilstein J. Nanotechnol. 2024, 15, 500–516, doi:10.3762/bjnano.15.45

• nanostructures produced by FEBID are of interest for diverse applications including magnetic data storage devices [4][5][6], tips for magnetic force microscopy [4][7], or sensors [4][8]. The same applies to cobalt nanostructures, which can be prepared with high purity and shape fidelity using, in particular, the

• ) trifluoroacetylacetonate (Au(tfac)Me2) [16] or neopentasilane (Si5H12) [17] to produce Fe–Au alloy nanostructures and Fe–Si binary compounds, respectively. More recently, diiron nonacarbonyl (Fe2(CO)9) has received particular attention [5][6][18][19][20]. With this precursor and applying high beam energies, nanopillars

• electron beam-induced surface activation (EBISA) [24][25], it can compromise spatial control by the electron beam and selectivity when aiming for 3D nanostructures [3][26]. Strategies to suppress autocatalytic deposit growth are thus desirable to devise FEBID processes with optimum performance [27

Aero-ZnS prepared by physical vapor transport on three-dimensional networks of sacrificial ZnO microtetrapods

• Veaceslav Ursaki,
• Tudor Braniste,
• Victor Zalamai,
• Emil Rusu,
• Vladimir Ciobanu,
• Vadim Morari,
• Daniel Podgornii,
• Pier Carlo Ricci,
• Rainer Adelung and
• Ion Tiginyanu

Beilstein J. Nanotechnol. 2024, 15, 490–499, doi:10.3762/bjnano.15.44

• processes, including those related to oxygen species adsorbed by the huge surface of the aeromaterial, as previously observed in ZnS nanostructures [42]. Some of these states may be related to oxygen vacancies and complex centers. Under ambient conditions, some oxygen species from the air are adsorbed at

Heat-induced morphological changes in silver nanowires deposited on a patterned silicon substrate

• Elyad Damerchi,
• Sven Oras,
• Edgars Butanovs,
• Allar Liivlaid,
• Mikk Antsov,
• Boris Polyakov,
• Annamarija Trausa,
• Veronika Zadin,
• Andreas Kyritsakis,
• Loïc Vidal,
• Karine Mougin,
• Siim Pikker and
• Sergei Vlassov

Beilstein J. Nanotechnol. 2024, 15, 435–446, doi:10.3762/bjnano.15.39

• organics. However, when the size of the structures is reduced to the nanoscale, metals exhibit distinct behavior at elevated temperatures compared to their larger counterparts [20][21]. Generally, a reduction in the melting point occurs as the size and dimensionality of the nanostructures decrease [20][22

• for various novel applications where arrays of metal nanostructures are used, such as surface-enhanced Raman spectroscopy substrates [36][37][38]. In this work, we deposited Ag NWs on specially patterned silicon (Si) substrates, so large fractions of NWs are partially suspended over the holes. Samples

Potential of a deep eutectic solvent in silver nanoparticle fabrication for antibiotic residue detection

• Le Hong Tho,
• Bui Xuan Khuyen,
• Ngoc Xuan Dat Mai and
• Nhu Hoa Thi Tran

Beilstein J. Nanotechnol. 2024, 15, 426–434, doi:10.3762/bjnano.15.38

• biosensors are commonly made of LSPR materials [17]. With the development of synthesis techniques, numerous nanostructures of noble metals have been extensively studied to improve the intrinsic parameters of sensors. Silver nanoparticles (Ag NPs) exhibit great performance in sensing applications owing to the

• presence of the fcc Ag lattice planes, we claim that Ag NPs-DES have been successfully synthesized [41]. The development of clusters into nanoparticles following our strategy is supported by the DES. DESs have been reported to be potential shape-controlling agents, and highly branched nanostructures were

Investigating ripple pattern formation and damage profiles in Si and Ge induced by 100 keV Ar⁺ ion beam: a comparative study

• Indra Sulania,
• Harpreet Sondhi,
• Tanuj Kumar,
• Sunil Ojha,
• G R Umapathy,
• Ambuj Mishra,
• Ambuj Tripathi,
• Richa Krishna,
• Devesh Kumar Avasthi and
• Yogendra Kumar Mishra

Beilstein J. Nanotechnol. 2024, 15, 367–375, doi:10.3762/bjnano.15.33

• structures. Although these structures may not be visible to the naked eye, they certainly have a visible impact on the mentioned applications. Nanopatterning is a very delicate procedure that is only possible with special techniques such as ion beam sputtering (IBS), with which one can achieve nanostructures

• observed [15], which may be achieved by altering the ion incidence angle [16]. However, there are some inconsistencies and replicability issues between the studies, which might mean that other experimental parameters might be important for the formation of these nanostructures. Computational studies have