Combined scanning probe electronic and thermal characterization of an indium arsenide nanowire

• Tino Wagner,
• Fabian Menges,
• Heike Riel,
• Bernd Gotsmann and
• Andreas Stemmer

Beilstein J. Nanotechnol. 2018, 9, 129–136, doi:10.3762/bjnano.9.15

• active devices both in positive and negative ways. In conventional logic devices, hot spots lead to signal degradation and reliability issues. In certain memristive devices, however, the breaking and formation of bonds upon local self-heating is the basis of their function [2]. The importance of electro

The rational design of a Au(I) precursor for focused electron beam induced deposition

• Ali Marashdeh,
• Thiadrik Tiesma,
• Niels J. C. van Velzen,
• Sjoerd Harder,
• Remco W. A. Havenith,
• Jeff T. M. De Hosson and
• Willem F. van Dorp

Beilstein J. Nanotechnol. 2017, 8, 2753–2765, doi:10.3762/bjnano.8.274

• small crystals sitting on a supporting material, the reliability of quantitative EDS is limited. It is also known that crystals of such organometallic complexes can be sensitive to electrons [12]. However, in these experiments we do consider EDS to be very useful. Firstly, the EDS measurements are

Synthesis of [{AgO₂CCH₂OMe(PPh₃)}_n] and theoretical study of its use in focused electron beam induced deposition

• Jelena Tamuliene,
• Julian Noll,
• Peter Frenzel,
• Tobias Rüffer,
• Alexander Jakob,
• Bernhard Walfort and
• Heinrich Lang

Beilstein J. Nanotechnol. 2017, 8, 2615–2624, doi:10.3762/bjnano.8.262

• ]. Values of the hardness >3 eV and softness <0.1 eV indicate high chemical stability and hence 2 can be considered as such, indicating reliability of the approach applied. This nicely corresponds with the experimentally observed properties of 2 (see above). The electronic structure of monomeric 2 is

Amplified cross-linking efficiency of self-assembled monolayers through targeted dissociative electron attachment for the production of carbon nanomembranes

• Sascha Koch,
• Christopher D. Kaiser,
• Paul Penner,
• Michael Barclay,
• Lena Frommeyer,
• Daniel Emmrich,
• Patrick Stohmann,
• Tarek Abu-Husein,
• Andreas Terfort,
• D. Howard Fairbrother,
• Oddur Ingólfsson and
• Armin Gölzhäuser

Beilstein J. Nanotechnol. 2017, 8, 2562–2571, doi:10.3762/bjnano.8.256

• , for instance, helium ion microscopy (HIM) [1][8]. However, since the latter procedure has to be conducted for each individual exposure time it is significantly more labor intensive. Nevertheless, for reasons of reliability, here we have applied both these approaches to follow the cross-linking of the

Laser-assisted fabrication of gold nanoparticle-composed structures embedded in borosilicate glass

• Nikolay Nedyalkov,
• Mihaela Koleva,
• Nadya Stankova,
• Rosen Nikov,
• Mitsuhiro Terakawa,
• Yasutaka Nakajima,
• Lyubomir Aleksandrov and
• Reni Iordanova

Beilstein J. Nanotechnol. 2017, 8, 2454–2463, doi:10.3762/bjnano.8.244

• parameters give an adequate description of the optical properties of gold over a wide spectral range according to [34]. Since the extinction spectrum of small nanoparticles is dominated by their absorption [32], it is used in the analysis presented below. The reliability of the model was checked by comparing

Systematic control of α-Fe₂O₃ crystal growth direction for improved electrochemical performance of lithium-ion battery anodes

• Nan Shen,
• Miriam Keppeler,
• Barbara Stiaszny,
• Holger Hain,
• Filippo Maglia and
• Madhavi Srinivasan

Beilstein J. Nanotechnol. 2017, 8, 2032–2044, doi:10.3762/bjnano.8.204

• lattice constant a, and 13.748 to 13.757 Å for lattice constant c (see Table 1), which is in perfect agreement with reported values [31][32]. The obtained RBragg values vary from ≈3% to ≈7%, indicating a good reliability of the refined data. No reflections of detectable impurities were observed

Fabrication of carbon nanospheres by the pyrolysis of polyacrylonitrile–poly(methyl methacrylate) core–shell composite nanoparticles

• Dafu Wei,
• Youwei Zhang and
• Jinping Fu

Beilstein J. Nanotechnol. 2017, 8, 1897–1908, doi:10.3762/bjnano.8.190

• FVR of 0.8, 1.6, and 2.4 are denoted as PAN-PMMA1, PAN-PMMA2, and PAN-PMMA3, respectively. All the synthesis experiments were repeated at least once to ensure reliability. Preparation of PAN-based carbon nanospheres PAN-based carbon nanospheres were fabricated via successive drying, preoxidation and

Two-dimensional silicon and carbon monochalcogenides with the structure of phosphorene

• Dario Rocca,
• Ali Abboud,
• Ganapathy Vaitheeswaran and
• Sébastien Lebègue

Beilstein J. Nanotechnol. 2017, 8, 1338–1344, doi:10.3762/bjnano.8.135

• experimentally [17][18]. Also, arsenene and antimonene [19], SiS [20], and SnS, SnSe, GeS, and GeSe [21][22] compounds with a crystal structure similar to the one of phosphorene were investigated by ab initio calculations. The reliability of ab initio calculations to predict and characterize new two dimensional

Metal oxide nanostructures: preparation, characterization and functional applications as chemical sensors

• Dario Zappa,
• Angela Bertuna,
• Elisabetta Comini,
• Navpreet Kaur,
• Nicola Poli,
• Veronica Sberveglieri and
• Giorgio Sberveglieri

Beilstein J. Nanotechnol. 2017, 8, 1205–1217, doi:10.3762/bjnano.8.122

• sensitivity, selectivity, response kinetics and reliability [4]. The design of active materials is essential and it must be the starting point for the control of the functional parameters of the final device. Nonetheless, great attention must be paid to the integration of the active material onto the

Study of the correlation between sensing performance and surface morphology of inkjet-printed aqueous graphene-based chemiresistors for NO₂ detection

• F. Villani,
• C. Schiattarella,
• T. Polichetti,
• R. Di Capua,
• F. Loffredo,
• B. Alfano,
• M. L. Miglietta,
• E. Massera,
• L. Verdoliva and
• G. Di Francia

Beilstein J. Nanotechnol. 2017, 8, 1023–1031, doi:10.3762/bjnano.8.103

• realized by CAD software. This guarantees high precision and accuracy in the deposition process [9][10]. All these features make IJP completely versatile in terms of employable inks and substrates, the latter being either rigid or flexible. In our previous work, we have demonstrated the reliability of IJP

• . Notwithstanding, a reliability in the control of the base parameters (i.e., base resistance, sensing response and stability) has been clearly observed on paper substrate. In this frame, inkjet printing with its ability to control the thickness of the deposited ink appears a more powerful tool to device

CVD transfer-free graphene for sensing applications

• Chiara Schiattarella,
• Sten Vollebregt,
• Tiziana Polichetti,
• Brigida Alfano,
• Ettore Massera,
• Maria Lucia Miglietta,
• Girolamo Di Francia and
• Pasqualina Maria Sarro

Beilstein J. Nanotechnol. 2017, 8, 1015–1022, doi:10.3762/bjnano.8.102

• . 3.5). In our case the estimated I(D)/I(D′) value is around 4.4, indicating that defects in the material are reasonably ascribed to the boundaries. Gas-sensing study In order to investigate the reliability of the fabrication process in terms of gas-sensing behaviour, two identical devices have been

• . In a CMOS-compatible process, all these devices could be directly fabricated on the same chip at micrometre-size. It is finally worth mentioning that, once proven the reliability of this process, it paves the way for the creation of a sensor array, able to provide selective responses towards the

Needs and challenges for assessing the environmental impacts of engineered nanomaterials (ENMs)

• Michelle Romero-Franco,
• Hilary A. Godwin,
• Muhammad Bilal and
• Yoram Cohen

Beilstein J. Nanotechnol. 2017, 8, 989–1014, doi:10.3762/bjnano.8.101

• composition and reactivity)) [37]. The various studies from which information on the nanomaterials (properties and toxicity endpoints) is compiled are then assessed with respect to the reliability of the provided information. Briefly, the application of the modified GreenScreen approach, which is available as

Ion beam profiling from the interaction with a freestanding 2D layer

• Ivan Shorubalko,
• Kyoungjun Choi,
• Michael Stiefel and
• Hyung Gyu Park

Beilstein J. Nanotechnol. 2017, 8, 682–687, doi:10.3762/bjnano.8.73

• Ivan Shorubalko Kyoungjun Choi Michael Stiefel Hyung Gyu Park Laboratory for Reliability Science and Technology, Empa (Swiss Federal Laboratories for Materials Science and Technology), Überlandstrasse 129, CH-8600 Dübendorf, Switzerland Nanoscience for Energy Technology and Sustainability

The longstanding challenge of the nanocrystallization of 1,3,5-trinitroperhydro-1,3,5-triazine (RDX)

• Florent Pessina and
• Denis Spitzer

Beilstein J. Nanotechnol. 2017, 8, 452–466, doi:10.3762/bjnano.8.49

• . Innovative techniques such as spin freezing [126] or spray drying enhance the processability, and potentially the performance, but the rigorous testing of their reliability is yet an open issue. The ball milling techniques raise concerns about the purity of the product. It is well know that after such an

• acetone around 5 wt %, whereas scCO2 is formed from 74–500 bar for a solubility from null to 0.025 wt %. The SFE technology has proven its high level of versatility and reliability, and is now entering advanced stages of development. Scale-up studies are performed and advanced in situ characterization is

Influence of hydrofluoric acid treatment on electroless deposition of Au clusters

• Rachela G. Milazzo,
• Antonio M. Mio,
• Giuseppe D’Arrigo,
• Emanuele Smecca,
• Alessandra Alberti,
• Gabriele Fisichella,
• Filippo Giannazzo,
• Corrado Spinella and
• Emanuele Rimini

Beilstein J. Nanotechnol. 2017, 8, 183–189, doi:10.3762/bjnano.8.19

• that probably results from the heating of the sample due to the higher Ar+ ion energy. In order to avoid artifacts, we therefore adopted the gentle milling procedure for all the samples to be analyzed by TEM. We tested the reliability of the mechanical thinning procedure by repeating both the HF

Structural and tribometric characterization of biomimetically inspired synthetic "insect adhesives"

• Matthias W. Speidel,
• Malte Kleemeier,
• Andreas Hartwig,
• Klaus Rischka,
• Angelika Ellermann,
• Rolf Daniels and
• Oliver Betz

Beilstein J. Nanotechnol. 2017, 8, 45–63, doi:10.3762/bjnano.8.6

Grazing-incidence optical magnetic recording with super-resolution

• Gunther Scheunert,
• Sidney. R. Cohen,
• René Kullock,
• Ryan McCarron,
• Katya Rechev,
• Ifat Kaplan-Ashiri,
• Ora Bitton,
• Paul Dawson,
• Bert Hecht and
• Dan Oron

Beilstein J. Nanotechnol. 2017, 8, 28–37, doi:10.3762/bjnano.8.4

• the next major step in the storage industry: it is predicted to increase the storage capacity, the read/write speed and the data lifetime of future hard disk drives. However, despite more than a decade of development work, the reliability is still a prime concern. Featuring an inherently fragile

Low temperature co-fired ceramic packaging of CMOS capacitive sensor chip towards cell viability monitoring

• Niina Halonen,
• Joni Kilpijärvi,
• Maciej Sobocinski,
• Timir Datta-Chaudhuri,
• Antti Hassinen,
• Someshekar B. Prakash,
• Peter Möller,
• Pamela Abshire,
• Sakari Kellokumpu and
• Anita Lloyd Spetz

Beilstein J. Nanotechnol. 2016, 7, 1871–1877, doi:10.3762/bjnano.7.179

• , to a printed circuit board (PCB). Figure 3a,b shows the manufactured package and Figure 3c the prototype package with microfluidic channel. Results and Discussion Reliability of the packaging method The new LTCC material was first tested using a dummy chip packaged in the LTCC and connected to a PCB

A new approach to grain boundary engineering for nanocrystalline materials

• Shigeaki Kobayashi,
• Sadahiro Tsurekawa and
• Tadao Watanabe

Beilstein J. Nanotechnol. 2016, 7, 1829–1849, doi:10.3762/bjnano.7.176

• nanocrystalline and submicrometer-grained Ni Segregation-induced intergranular embrittlement is a serious problem that degrades the performance reliability of various types of structural materials. In nanocrystalline and submicrometer-grained materials possessing a very high density of grain boundaries and triple

Precise in situ etch depth control of multilayered III−V semiconductor samples with reflectance anisotropy spectroscopy (RAS) equipment

• Ann-Kathrin Kleinschmidt,
• Lars Barzen,
• Johannes Strassner,
• Christoph Doering,
• Henning Fouckhardt,
• Wolfgang Bock,
• Michael Wahl and
• Michael Kopnarski

Beilstein J. Nanotechnol. 2016, 7, 1783–1793, doi:10.3762/bjnano.7.171

• – depending on the relevance of the trench depth for the device function. To examine the reliability of RAS in controlling the etch depth, the etched sample pieces I–IV (corresponding to specific etch times – see Figure 2) and, for reference, a not reactive-ion-etched piece of the same sample (type A) are

Morphology of SiO₂ films as a key factor in alignment of liquid crystals with negative dielectric anisotropy

• Volodymyr Tkachenko,
• Antigone Marino,
• Eva Otón,
• Noureddine Bennis and
• Josè Manuel Otón

Beilstein J. Nanotechnol. 2016, 7, 1743–1748, doi:10.3762/bjnano.7.167

• technique as a reference for such materials. The measure of the optical constants [21], tilt distribution and anchoring strength [22] in nematic LC cells is well reported. The integration of VASE with other techniques [23] has also been investigated to improve the reliability and accuracy of the optical

Nanostructured germanium deposited on heated substrates with enhanced photoelectric properties

• Ionel Stavarache,
• Valentin Adrian Maraloiu,
• Petronela Prepelita and
• Gheorghe Iordache

Beilstein J. Nanotechnol. 2016, 7, 1492–1500, doi:10.3762/bjnano.7.142

• . This is closely related to the increase of high-speed operation, good reliability, low power consumption and the decrease of unit price that led to the rapid development of the semiconductor device market and to the continuous downscaling of devices. Regarding the downscaling process, high mobility

Polystyrene-block-poly(ethylene oxide) copolymers as templates for stacked, spherical large-mesopore silica coatings: dependence of silica pore size on the PS/PEO ratio

• Roberto Nisticò,
• Giuliana Magnacca,
• Sushilkumar A. Jadhav and
• Dominique Scalarone

Beilstein J. Nanotechnol. 2016, 7, 1454–1460, doi:10.3762/bjnano.7.137

• refer, from top to bottom, to the 95/5 (dashed line) and 93/7 (dotted line) experimental fitting curves, respectively. Reliability of regressions: R2 > 0.98 and 0.83 (A), R2 > 0.96 and 0.88 (B). Black square in panel A is the zoomed area reported in panel C. Calculations of the pore size for the sample

Functional diversity of resilin in Arthropoda

• Jan Michels,
• Esther Appel and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2016, 7, 1241–1259, doi:10.3762/bjnano.7.115

• are not absolutely specific. Therefore, it is strongly advisable to apply not only one single method but a combination of several different ones to increase the reliability of the identification and detection of resilin. In recent years, an antibody to a recombinant Drosophila melanogaster pro-resilin

Influence of synthesis conditions on microstructure and phase transformations of annealed Sr₂FeMoO_6−x nanopowders formed by the citrate–gel method

• Marta Yarmolich,
• Nikolai Kalanda,
• Sergey Demyanov,
• Herman Terryn,
• Jon Ustarroz,
• Maksim Silibin and
• Gennadii Gorokh

Beilstein J. Nanotechnol. 2016, 7, 1202–1207, doi:10.3762/bjnano.7.111

• capacity measurement has a higher sensitivity compared to the XRD investigations and makes it possible to determine the above-mentioned inclusions of the indirect phases with high reliability. In consideration of the highly λ-shaped transition at 330 K, we may presume that it is due to the transition of