Fingerprints of a size-dependent crossover in the dimensionality of electronic conduction in Au-seeded Ge nanowires

• Maria Koleśnik-Gray,
• Gillian Collins,
• Justin D. Holmes and
• Vojislav Krstić

Beilstein J. Nanotechnol. 2016, 7, 1574–1578, doi:10.3762/bjnano.7.151

• , two regimes were identified for large (lightly doped) and small (stronger doped) nanowires in which the charge-carrier drift is dominated by electron-phonon and ionized-impurity scattering, respectively. This goes in hand with the finding that the electrostatic properties for radii below ca. 37 nm

•  3a). In the case of mobility (Figure 3b), between ≤1015 and ≈1016 cm−3 μNW(Nd) ≈ Nd, indicating that lattice phonon scattering is the main mechanism limiting the carrier drift [25]. The dominance of electron phonon scattering within this density range suggests that the free holes behave similar to

• that a crossover in charge carrier conduction occurs for carrier densities exceeding ≈1016 cm−3, equivalent to the radius decreasing below approximately 37 nm. Analysis of the electrical screening properties shows that this is associated with a shift from a 3D to quasi-1D regime where the carrier drift

Ammonia gas sensors based on In₂O₃/PANI hetero-nanofibers operating at room temperature

• Qingxin Nie,
• Zengyuan Pang,
• Hangyi Lu,
• Yibing Cai and
• Qufu Wei

Beilstein J. Nanotechnol. 2016, 7, 1312–1321, doi:10.3762/bjnano.7.122

• nanofibers sensor could not fully return to the initial state, and there was a baseline drift of 4% after the first exposure to NH3. This bias was smaller than the results in other reports [34][35][36]. On the other hand, the response of this sensor slightly decreased with the increasing number of tests. The

Optical absorption signature of a self-assembled dye monolayer on graphene

• Tessnim Sghaier,
• Sylvain Le Liepvre,
• Céline Fiorini,
• Ludovic Douillard and
• Fabrice Charra

Beilstein J. Nanotechnol. 2016, 7, 862–868, doi:10.3762/bjnano.7.78

• means of atomic resolution obtained on HOPG images in XY-directions and with flame-annealed gold through the height of steps in the Z-direction. All the images were obtained at a quasi-constant current, i.e., in the variable-height mode. The images in Figure 1a,b were corrected for the thermal drift by

Understanding interferometry for micro-cantilever displacement detection

• Alexander von Schmidsfeld,
• Tobias Nörenberg,
• Matthias Temmen and
• Michael Reichling

Beilstein J. Nanotechnol. 2016, 7, 841–851, doi:10.3762/bjnano.7.76

• quasi-linear function of d and the z-piezo offset voltage is adjusted such that the maximum peak-to-peak voltage is obtained. Such fine-tuning can be carefully repeated during a series of measurements to compensate for thermal drift. Note, that the measured amplitude corresponds to the position of the

Microscopic characterization of Fe nanoparticles formed on SrTiO₃(001) and SrTiO₃(110) surfaces

• Miyoko Tanaka

Beilstein J. Nanotechnol. 2016, 7, 817–824, doi:10.3762/bjnano.7.73

• . Electrochemically etched tungsten tips were used. STM images are not highly resolved because vibration and sample drift cannot be completely eliminated due to the relatively non-rigid sample holders that need to be compatible to UTSICS and TEM. TEM images and TED patterns were taken with an acceleration voltage of

High-resolution noncontact AFM and Kelvin probe force microscopy investigations of self-assembled photovoltaic donor–acceptor dyads

• Benjamin Grévin,
• Pierre-Olivier Schwartz,
• Laure Biniek,
• Martin Brinkmann,
• Nicolas Leclerc,
• Elena Zaborova and
• Stéphane Méry

Beilstein J. Nanotechnol. 2016, 7, 799–808, doi:10.3762/bjnano.7.71

• ). The lateral lag (due to thermal drift and piezoelectric actuator creep) between the set of images used for the SPV calculation was corrected by using the lattice tool of the WsXM software [22] (see Figure S9 in Supporting Information File 1). After correcting the images, the residual lateral error in

Magnetic switching of nanoscale antidot lattices

• Ulf Wiedwald,
• Joachim Gräfe,
• Kristof M. Lebecki,
• Maxim Skripnik,
• Felix Haering,
• Gisela Schütz,
• Paul Ziemann,
• Eberhard Goering and
• Ulrich Nowak

Beilstein J. Nanotechnol. 2016, 7, 733–750, doi:10.3762/bjnano.7.65

• -optical Kerr effect (MOKE) strongly suffer from drift, Faraday effect background, and they do not provide absolute magnetisation values [23]. However, focused MOKE provides the necessary high spatial resolution, needed for self-organized antidot arrays as shown in Figure 2. To overcome the mentioned MOKE

• limitations we developed a specialized magnetic field sequence applied to the sample, as shown in Figure 4. The field sequence provides two additional anchor points at both positive and negative saturation (3) for every minor loop investigated. This allows correction for drift and normalisation to saturation

Cantilever bending based on humidity-actuated mesoporous silica/silicon bilayers

• Christian Ganser,
• Gerhard Fritz-Popovski,
• Roland Morak,
• Parvin Sharifi,
• Benedetta Marmiroli,
• Barbara Sartori,
• Heinz Amenitsch,
• Thomas Griesser,
• Christian Teichert and
• Oskar Paris

Beilstein J. Nanotechnol. 2016, 7, 637–644, doi:10.3762/bjnano.7.56

• adsorption and after desorption. Such an offset points to an only partially reversible process and perhaps also to slight drift problems. A clear hysteresis is evident between the adsorption and desorption curves above RH = 50%. This hysteresis in cantilever deflection agrees with the hysteresis seen in

• experimentally by placing an uncoated, pristine cantilever in the fluid cell and increasing the relative humidity from 5 to 90% while recording the cantilever deflection. In this experiment, only a drift of the deflection of approximately 5 nm was found but no significant change in deflection. Therefore, the

Correlative infrared nanospectroscopic and nanomechanical imaging of block copolymer microdomains

• Benjamin Pollard and
• Markus B. Raschke

Beilstein J. Nanotechnol. 2016, 7, 605–612, doi:10.3762/bjnano.7.53

• inset with calculated lineshape (solid line) based on the above fit parameters and is Kramers–Kronig consistent. As is often encountered in hybrid imaging, maps from force–distance spectroscopy and from s-SNOM acquired subsequently with the same tip need to be aligned to compensate for sample drift. The

Length-extension resonator as a force sensor for high-resolution frequency-modulation atomic force microscopy in air

• Hannes Beyer,
• Tino Wagner and
• Andreas Stemmer

Beilstein J. Nanotechnol. 2016, 7, 432–438, doi:10.3762/bjnano.7.38

• air using a length-extension resonator operating at small amplitudes. An additional slow feedback compensates for changes in the free resonance frequency, allowing stable imaging over a long period of time with changing environmental conditions. Keywords: ambient conditions; drift compensation

• et al. [19] and Fan et al. [21], applying a feedback based on the Q-factor to stabilise the tip–sample distance. In our implementation the ratio of excitation and amplitude of the first harmonic resonance, and thus the Q-factor, is held constant by a slow feedback to compensate for drift of the free

• 0.42%, respectively. This will strongly affect the desired force gradient setpoint and interpretation of data becomes difficult. Furthermore, in a scenario where operation near the frequency shift minimum Δfmin is desired, environment-induced drift could cause the setpoint Δfset to cross Δfmin, leading

Plasticity-mediated collapse and recrystallization in hollow copper nanowires: a molecular dynamics simulation

• Amlan Dutta,
• Arup Kumar Raychaudhuri and
• Tanusri Saha-Dasgupta

Beilstein J. Nanotechnol. 2016, 7, 228–235, doi:10.3762/bjnano.7.21

• disordered atoms is much higher as compared to their crystalline counterparts since they access a relatively larger free volume. This causes a radially inward drift of the inner surface driven by surface tension. This inward drift results into large local stresses on the residual crystalline parts of the

• (shown as red atoms in Figure 1). This firmly establishes that instead of the conventional notion of slow and diffusive mode of collapse by vacancy migration, the collapse happens through a plasticity mediated mechanism involving the rapid drift of disordered atoms and creation of stacking faults on

Two step formation of metal aggregates by surface X-ray radiolysis under Langmuir monolayers: 2D followed by 3D growth

• Smita Mukherjee,
• Marie-Claude Fauré,
• Michel Goldmann and
• Philippe Fontaine

Beilstein J. Nanotechnol. 2015, 6, 2406–2411, doi:10.3762/bjnano.6.247

• then consider that the fluidity of the monolayer is enhanced, increasing the in-plane mobility of the patches of irradiated material. Thus, the surface region initially irradiated could drift in and out of the footprint area, leading to various thickness of the silver film and thus inducing the

• , between the incident and diffracted beam projected onto the horizontal plane. The X-ray fluorescence signal was measured using a one-element, silicon drift detector (Brüker, Germany) equipped with a collimator and mounted at 30° with respect to the vertical direction towards the X-ray source in order to

Paramagnetism of cobalt-doped ZnO nanoparticles obtained by microwave solvothermal synthesis

• Jacek Wojnarowicz,
• Sylwia Kusnieruk,
• Tadeusz Chudoba,
• Stanislaw Gierlotka,
• Witold Lojkowski,
• Wojciech Knoff,
• Malgorzata I. Lukasiewicz,
• Bartlomiej S. Witkowski,
• Anna Wolska,
• Marcin T. Klepka,
• Tomasz Story and
• Marek Godlewski

Beilstein J. Nanotechnol. 2015, 6, 1957–1969, doi:10.3762/bjnano.6.200

• structure (EXAFS) measurements. EXAFS measurements at the K-edge of Zn and Co were performed at Deutsches Elektronen-Synchrotron (DESY), Hasylab (C1 and A1 stations) at 140 °C using a 7-element silicon fluorescence drift detector for the Co K-edge and in transmission mode for the Zn K-edge. The data were

Lower nanometer-scale size limit for the deformation of a metallic glass by shear transformations revealed by quantitative AFM indentation

• Arnaud Caron and
• Roland Bennewitz

Beilstein J. Nanotechnol. 2015, 6, 1721–1732, doi:10.3762/bjnano.6.176

• compliant sample surface, an extension of the z-scanner also leads to a penetration of the AFM tip into the sample surface by the penetration depth δ = Z − D. While the cantilever deflection D is calibrated independently, the height value Z is subject to drift or creep effects of the piezoelectric scanner

• . The accuracy in δ is thus limited by piezoelectric creep of the AFM scanner. In order to minimize vertical drift, the tip position was equilibrated before each indentation by recording a slow 500 × 500 nm2 scan of the area to be indented by AFM. Indentation measurements were then started from the

• position of the scanner during nc-AFM imaging, i.e., half of the oscillation amplitude or a few nanometers above the surface. In order to further account for piezoelectric creep effects during rate-dependent measurements a drift difference ΔZdrift with regard to the fastest measurement was calculated

Possibilities and limitations of advanced transmission electron microscopy for carbon-based nanomaterials

• Xiaoxing Ke,
• Carla Bittencourt and
• Gustaaf Van Tendeloo

Beilstein J. Nanotechnol. 2015, 6, 1541–1557, doi:10.3762/bjnano.6.158

• metal-oxide semiconductor) sensor up to 1600 fps [50]. The high sensitivity and fast acquisition in detecting has made possible the automated and ultra-fast acquisition of a series of under-exposed images from the same region. After drift correction, the images of such a sequence are stacked and can

Current–voltage characteristics of manganite–titanite perovskite junctions

• Benedikt Ifland,
• Patrick Peretzki,
• Birte Kressdorf,
• Philipp Saring,
• Andreas Kelling,
• Michael Seibt and
• Christian Jooss

Beilstein J. Nanotechnol. 2015, 6, 1467–1484, doi:10.3762/bjnano.6.152

• different, the applicability of a Shockley-like equation is far from obvious. In contrast to inorganic p–n junctions, where the current across the junction is due to drift diffusion and/or recombination within the SCR, the current in organic heterojunctions is carried by hole and electron-type polarons

Improved atomic force microscopy cantilever performance by partial reflective coating

• Zeno Schumacher,
• Yoichi Miyahara,
• Laure Aeschimann and
• Peter Grütter

Beilstein J. Nanotechnol. 2015, 6, 1450–1456, doi:10.3762/bjnano.6.150

• difference is attributed to multiple possible sources. The thermal vibration measurement is more susceptible to temperature drift as it requires longer acquisition time for measuring the cantilevers with higher Q-factors. The fitting can also contribute to a difference in the measured values due to the high

Nano-contact microscopy of supracrystals

• Adam Sweetman,
• Nicolas Goubet,
• Ioannis Lekkas,
• Marie Paule Pileni and
• Philip Moriarty

Beilstein J. Nanotechnol. 2015, 6, 1229–1236, doi:10.3762/bjnano.6.126

• paper, the tip was held at ground potential and the sample was biased. To help stabilise the imaging conditions, a custom-built atom tracking system [37] was used to apply feed-forward correction to reduce the effect of thermal drift and piezo-electric creep. To measure the site-specific force between

• . We also note that, due to instrumental drift and creep, the Δz values are likely to be systematically underestimated. (A) Overview dSTM showing nanocrystal assembly, Vgap = +2 V, = 20 pA. (B) DFM image acquired in the region shown in A. Vgap = 0 V, Δf = −2.3 Hz, A0 = 0.11 nm. (C) Constant height Δf

Closed-loop conductance scanning tunneling spectroscopy: demonstrating the equivalence to the open-loop alternative

• Chris Hellenthal,
• Kai Sotthewes,
• Martin H. Siekman,
• E. Stefan Kooij and
• Harold J. W. Zandvliet

Beilstein J. Nanotechnol. 2015, 6, 1116–1124, doi:10.3762/bjnano.6.113

• preamplifier at a fixed gain of 108 V·A−1 and were performed within a short timeframe to minimize the effects of drift and possible changes to the tip or sample. Experimental parameters were chosen to prevent changes in tip–sample distance between experiments. As such, z(V) measurements were performed at a

High sensitivity and high resolution element 3D analysis by a combined SIMS–SPM instrument

• Yves Fleming and
• Tom Wirtz

Beilstein J. Nanotechnol. 2015, 6, 1091–1099, doi:10.3762/bjnano.6.110

• topographies are taken as reference maps for linearly extrapolating the z-position of each of the intermittent SIMS recorded voxels. SARINA was developed as a plugin for the ImageJ software [13]. The drift correction of the different recorded SIMS stacks were performed using the OpenMIMS software [14], which

Automatic morphological characterization of nanobubbles with a novel image segmentation method and its application in the study of nanobubble coalescence

• Yuliang Wang,
• Huimin Wang,
• Shusheng Bi and
• Bin Guo

Beilstein J. Nanotechnol. 2015, 6, 952–963, doi:10.3762/bjnano.6.98

• the image of the PS surface immersed in DI water. The entire surface is covered with spherical cap-like domains, which are identified as NBs [6]. The Rrms is 2.8 nm, which is a value much larger than that obtained in air. Due to the mechanical instrumentation drift [42] that occurs during imaging, the

Pt- and Pd-decorated MWCNTs for vapour and gas detection at room temperature

• Hamdi Baccar,
• Atef Thamri,
• Pierrick Clément,
• Eduard Llobet and
• Adnane Abdelghani

Beilstein J. Nanotechnol. 2015, 6, 919–927, doi:10.3762/bjnano.6.95

• molecules to the metal nanoparticle–carbon nanotube system is rather strong, since the full recovery of the baseline resistance of the sensors is not reached, and a significant drift appears in the successive detection/recovery events shown in Figure 6. Nitrogen dioxide strongly binds to the surface of

Stiffness of sphere–plate contacts at MHz frequencies: dependence on normal load, oscillation amplitude, and ambient medium

• Jana Vlachová,
• Rebekka König and
• Diethelm Johannsmann

Beilstein J. Nanotechnol. 2015, 6, 845–856, doi:10.3762/bjnano.6.87

• experimental error. In particular, there were no systematic differences between increasing and decreasing ramps. Occasionally, a slow drift was superimposed onto the ramps. Quartz resonators respond to changes in temperature and static stress with slow drifts. Drifts can be reduced by mounting the crystals in

Capillary and van der Waals interactions on CaF₂ crystals from amplitude modulation AFM force reconstruction profiles under ambient conditions

• Annalisa Calò,
• Oriol Vidal Robles,
• Sergio Santos and
• Albert Verdaguer

Beilstein J. Nanotechnol. 2015, 6, 809–819, doi:10.3762/bjnano.6.84

• relative to the drive force, and Q is the quality factor due to dissipation with the medium. The experimental APD curves cover the approach and the retract part during one cycle, with a drift smaller than 0.5 nm (see Supporting Information File 1, Figure S1). Only approach curves for which the cantilever

A versatile strategy towards non-covalent functionalization of graphene by surface-confined supramolecular self-assembly of Janus tectons

• Ping Du,
• David Bléger,
• Fabrice Charra,
• Vincent Bouchiat,
• David Kreher,
• Fabrice Mathevet and
• André-Jean Attias

Beilstein J. Nanotechnol. 2015, 6, 632–639, doi:10.3762/bjnano.6.64

• strategy and expected organization on C(sp2)-carbon-based supports of the self-assembled Janus tectons, exposing a wide range of external interfacial compositions. Self-assembly of a Janus tecton precursor (JAP) and the Janus tectons (JA). Drift-corrected STM images obtained at the interface between HOPG

• illustrate the agreement between all Janus tecton lattices. Figure adapted with permission from [25], copyright 2014 Wiley-VCH Verlag GmbH & Co. Self-assembly on graphene. Drift-corrected STM images obtained in air on a monolayer graphene substrate grown by chemical vapor deposition on a polycrystalline