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Search for "blue" in Full Text gives 944 result(s) in Beilstein Journal of Organic Chemistry. Showing first 200.

Chemical structure metagenomics of microbial natural products: surveying nonribosomal peptides and beyond

  • Thomas Ma and
  • John Chu

Beilstein J. Org. Chem. 2024, 20, 3050–3060, doi:10.3762/bjoc.20.253

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  • ) Incorporation of the first five amino acid BBs in daptomycin (highlighted in blue) is illustrated herein. In NRP biosynthesis, modules are arranged in an assembly line fashion; each module incorporates one BB into the growing peptide intermediate, which is then passed onto the next module. b) Within each module
  • based on a dataset of known pairs of nonribosomal code/substrate BB. c) An analysis that compared the known vs predicted NRP BBs grouped based on their chemical structures found both oversampled (green)/underexplored (blue) niches in the NRP chemical space; the analysis was performed across all bacteria
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Published 20 Nov 2024
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  • fluorescence (Figure 15C,D). Namely, the fluorescence of the initial RCP in DMF was observed as a blue emission by the naked eye, while according to the degradation, the dumbbell species spread throughout the solution and the [3]rotaxane structure disappeared, resulting in the light green color fluorescence of
  • , meaning the introduction of CD units affects the fluorescence in a similar manner to the solvent, probably because two CD units have densely placed many (36) substituents on them. Thus, PAc-α-CD-based [3]rotaxane showed blue-shifted fluorescence compared with the dumbbell 13, which was observed before and
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Published 19 Nov 2024

Tunable full-color dual-state (solution and solid) emission of push–pull molecules containing the 1-pyrindane moiety

  • Anastasia I. Ershova,
  • Sergey V. Fedoseev,
  • Konstantin V. Lipin,
  • Mikhail Yu. Ievlev,
  • Oleg E. Nasakin and
  • Oleg V. Ershov

Beilstein J. Org. Chem. 2024, 20, 3016–3025, doi:10.3762/bjoc.20.251

Graphical Abstract
  • Table S1 and Figure S1, Supporting Information File 1). The electronic absorption spectra were characterized by a pronounced maximum in the visible region centered at 431–448 nm. Emission maxima of compound 1c were more significantly affected by the change of polarity and ranged from 475 nm (blue-green
  • group, a strong blue shift occurred down to 394 nm. The only exception was a solution of 1i in acetic acid, where two peaks were observed. Apparently, the weaker acetic acid caused just a partial protonation of the amino group, and the equilibrium shown in Scheme 2 was observed. This was evidenced by
  • visible region of the spectrum (from blue to red, Figure 3B and Figure 4). Acidic solutions were the most blue-shifted due to the formation of the protonated form 1iH+ (Scheme 2). Two emission maxima were observed in acetic acid and associated with the corresponding absorption maxima. The first, located
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Published 19 Nov 2024

Advances in radical peroxidation with hydroperoxides

  • Oleg V. Bityukov,
  • Pavel Yu. Serdyuchenko,
  • Andrey S. Kirillov,
  • Gennady I. Nikishin,
  • Vera A. Vil’ and
  • Alexander O. Terent’ev

Beilstein J. Org. Chem. 2024, 20, 2959–3006, doi:10.3762/bjoc.20.249

Graphical Abstract
  • -AcrClO4 as the photocatalyst has been disclosed (Scheme 24) [67]. According to the authors, the irradiation of the photocatalyst (Acr+-Mes) A with a blue LED leads to the excited state (Acr·-Mes·+) B. The aliphatic carboxylic acid 66 is converted by deprotonation to the corresponding carboxylate, which is
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Published 18 Nov 2024

4,6-Diaryl-5,5-difluoro-1,3-dioxanes as chiral dopants for liquid crystal compositions

  • Maurice Médebielle,
  • Peer Kirsch,
  • Jérémy Merad,
  • Carolina von Essen,
  • Clemens Kühn and
  • Andreas Ruhl

Beilstein J. Org. Chem. 2024, 20, 2940–2945, doi:10.3762/bjoc.20.246

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  • ) LCDs which need a higher HTP or increased dopant concentrations [8][9]. TN and STN displays are still based on liquid crystals in the nematic or cholesteric mesophase. Even higher concentrations of chiral dopants with extremely high HTP tend to induce a Blue Phase, which is a cubic mesophase composed
  • of double twist cylinders [10][11]. A prototype of a polymer-stabilized Blue Phase LCD with ultra-fast switching times has been presented in 2008 by Samsung [12]. Another class of materials including high HTP chiral dopants are cholesteric films prepared by the polymerization of reactive mesogens
  • the two nematic host mixtures is their polarity: whereas Host 1 is only moderately polar (Δε = 4.0), the mixture Host 2 was developed for Blue Mode LCD application and is extremely polar. As compared to chiral dopants depicted in Figure 1, HTPs are lower and closest analogues for comparison could be
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Published 14 Nov 2024

The charge transport properties of dicyanomethylene-functionalised violanthrone derivatives

  • Sondos A. J. Almahmoud,
  • Joseph Cameron,
  • Dylan Wilkinson,
  • Michele Cariello,
  • Claire Wilson,
  • Alan A. Wiles,
  • Peter J. Skabara and
  • Graeme Cooke

Beilstein J. Org. Chem. 2024, 20, 2921–2930, doi:10.3762/bjoc.20.244

Graphical Abstract
  • anhydrous chlorobenzene (6 mL). To the dark blue mixture titanium tetrachloride (100 μL, 0.840 mmol) and pyridine (130 μL, 1.68 mmol) were added and the mixture was stirred under reflux overnight. After cooling the reaction mixture to room temperature, it was poured into ice-water (50 mL) and extracted with
  • in anhydrous chlorobenzene (6 mL). To the dark blue mixture, titanium tetrachloride (50.0 μL, 0.420 mmol) and pyridine (70.0 μL, 0.84 mmol) were added and the mixture was stirred under reflux overnight. After cooling the reaction mixture to room temperature, it was poured into ice-water (50 mL) and
  • mL). To the dark blue mixture titanium tetrachloride (120 μL, 1.08 mmol) and pyridine (170 μL, 2.16 mmol) were added and the mixture was stirred under reflux overnight. After cooling the reaction mixture to room temperature, it was poured into ice-water (50 mL) and extracted with dichloromethane (3
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Published 13 Nov 2024

Recent advances in transition-metal-free arylation reactions involving hypervalent iodine salts

  • Ritu Mamgain,
  • Kokila Sakthivel and
  • Fateh V. Singh

Beilstein J. Org. Chem. 2024, 20, 2891–2920, doi:10.3762/bjoc.20.243

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  • mechanism by adding 2 equivalents of TEMPO to the reaction mixture. The absence of the desired product indicated the involvement of a radical pathway in the process. The proposed reaction mechanism begins with the activation of eosin Y by visible light from 5 W blue LEDs, transitioning it to its excited
  • corresponding heteroaryl–aryl compounds 32 in moderate to good yield. The use of blue LEDs (456 nm), nitrogen atmosphere, and HFIP/H2O 4:1 solvent mixture improved the yield of the product by up to 90%. Various substituted azauracils were used to study the reaction and it was observed that different substituted
  • Morita–Baylis–Hillman (MBH) acetates using a variety of diaryliodonium triflates [65]. The reaction was carried out with MBH acetate 33 and diphenyliodonium triflate 16 in the presence of different photocatalysts and bases. Methylene blue trihydrate (MB·3H2O) was identified as a highly active
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Published 13 Nov 2024

N-Glycosides of indigo, indirubin, and isoindigo: blue, red, and yellow sugars and their cancerostatic activity

  • Peter Langer

Beilstein J. Org. Chem. 2024, 20, 2840–2869, doi:10.3762/bjoc.20.240

Graphical Abstract
  • their activity against various types of cancer. N-Glycosides of indigo, indirubin, and isoindigo, blue, red, and yellow sugars, turned out to be of special interest because of their high cancerostatic activity and structural novelty. The present article provides an account on the synthesis and
  • anticancer activity of these compounds. Keywords: cancerostatic activity; carbohydrates; heterocycles; N-glycosides; indirubin; Introduction Indigo (1a), known for more than 6000 years and originally produced from indigo plants in India, represents a famous traditional blue pigment which was an expensive
  • , indirubin, and isoindigo which can be regarded as blue, red, and yellow sugars, respectively. Review Indigo-N-glycosides (blue sugars) In 2002, Laatsch and Maskey reported the isolation of the akashins A, B and C, indigo-N-glycosides, from terrestric Streptomyces (Scheme 2) [17][18]. These natural products
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Published 08 Nov 2024

Investigation of a bimetallic terbium(III)/copper(II) chemosensor for the detection of aqueous hydrogen sulfide

  • Parvathy Mini,
  • Michael R. Grace,
  • Genevieve H. Dennison and
  • Kellie L. Tuck

Beilstein J. Org. Chem. 2024, 20, 2818–2826, doi:10.3762/bjoc.20.237

Graphical Abstract
  • the presence of various anions/sulfur compounds; spectra measured in 10 mM Tris HCl buffer (pH 7.4) with λex = 250 nm. Green bar: [Tb.1·3Cu]3+ alone (5 µM). Blue bar: [Tb.1·3Cu]3+ (5 µM) and Na2S (15 µM). Grey bars: [Tb.1·3Cu]3+ (5 µM) and anion/sulfur compound (50 µM). Black bars: [Tb.1·3Cu]3+ (5 µM
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Published 05 Nov 2024

Interaction of a pyrene derivative with cationic [60]fullerene in phospholipid membranes and its effects on photodynamic actions

  • Hayato Takagi,
  • Çetin Çelik,
  • Ryosuke Fukuda,
  • Qi Guo,
  • Tomohiro Higashino,
  • Hiroshi Imahori,
  • Yoko Yamakoshi and
  • Tatsuya Murakami

Beilstein J. Org. Chem. 2024, 20, 2732–2738, doi:10.3762/bjoc.20.231

Graphical Abstract
  • -methyl-1-pyrrolidone-N-oxide (DEPMPO) were respectively used (schemes in Figure 5). Our previous study demonstrated that both 1O2 and O2•– were generated under irradiation of triad molecules in DMSO/H2O [8]. Under irradiation by a blue LED (464–477 nm, 23 lm·W–1), significant ESR signals corresponding to
  • Sciences AG (Farmingdale, NY, USA). FeSO4, DETAPAC and NADH was bought from Sigma-Aldrich (St. Louis, Missouri, USA). DMPO was bought from TCI (Tokyo Chemical Industry Co. Ltd., Tokyo, Japan). Irradiation was performed by blue LED light (464–477 nm, 23 lm·W–1) from Lumiflex300 Pro RGB LED Stripes
  • solution (335 µM) was added instead of 10 µM of PBS(–). The solution was subjected to O2 bubbling for 30 seconds and then taken into 50 µL capillary and sealed. The solution was then irradiated with blue LED light for 30 minutes. The capillary was taken into the ESR tube for measurement at room temperature
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Published 30 Oct 2024

Synthesis of spiroindolenines through a one-pot multistep process mediated by visible light

  • Francesco Gambuti,
  • Jacopo Pizzorno,
  • Chiara Lambruschini,
  • Renata Riva and
  • Lisa Moni

Beilstein J. Org. Chem. 2024, 20, 2722–2731, doi:10.3762/bjoc.20.230

Graphical Abstract
  • materials (Scheme 1d). The synthetic procedure is achieved using blue light irradiation and bromotrichloromethane (BrCCl3), as a one-pot procedure, minimizing chemical wastes, avoiding purification of intermediates, and simplifying practical aspects. Results and Discussion We have recently published the one
  • synthetic process in a one-pot manner, adding all the components from the very beginning. So, the blue-light-promoted reaction between N-Ph-THIQ, 3-methoxyaniline and tert-butyl isocyanide in the presence of BrCCl3 was extensively optimized by varying several parameters, such as solvent, relative quantity
  • of components and temperature (Table 2). We firstly irradiated with blue LEDs (451 nm) the mixture of the three components in the presence of 1.5 equiv of BrCCl3 for 18 h at room temperature under argon atmosphere (Table 2, entry 1). To our surprise, the reaction provided only traces of the expected
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Published 29 Oct 2024

Photoluminescence color-tuning with polymer-dispersed fluorescent films containing two fluorinated diphenylacetylene-type fluorophores

  • Kazuki Kobayashi,
  • Shigeyuki Yamada,
  • Motohiro Yasui and
  • Tsutomu Konno

Beilstein J. Org. Chem. 2024, 20, 2682–2690, doi:10.3762/bjoc.20.225

Graphical Abstract
  • and effective luminescence color-tuning method is proposed to investigate the photoluminescence behavior of two-component polymer dispersion films blended with two types of fluorinated diphenylacetylenes, namely blue- and yellow- or red-fluorescent fluorinated diphenylacetylenes. It is confirmed that
  • if blue and green–yellow or yellow fluorophores are blended in appropriate ratios, a binary blend with color coordinates (0.20, 0.32) can be achieved, which approaches the white point of pure white emission. These findings contribute to the development of effective lighting and display devices as new
  • has been severely delayed [4][5][6]. However, since Tang et al. first reported the aggregation-induced emission phenomenon in 2001 [7], the development of solid-state light-emitting materials has accelerated significantly [8][9][10]. Many photoluminescent materials that emit blue, green, and yellow
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Published 23 Oct 2024

Computational design for enantioselective CO2 capture: asymmetric frustrated Lewis pairs in epoxide transformations

  • Maxime Ferrer,
  • Iñigo Iribarren,
  • Tim Renningholtz,
  • Ibon Alkorta and
  • Cristina Trujillo

Beilstein J. Org. Chem. 2024, 20, 2668–2681, doi:10.3762/bjoc.20.224

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  • (PO) and CO2 and the five catalyst scaffolds under study. The position of the LB along with an appropriate number of substituents is indicated by blue dots and that of the LA by pink dots. Capture reactions of CO2 or an epoxide by FLP. Asymmetric catalysis studied. On the left, the catalyst proposed
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Published 22 Oct 2024

Applications of microscopy and small angle scattering techniques for the characterisation of supramolecular gels

  • Connor R. M. MacDonald and
  • Emily R. Draper

Beilstein J. Org. Chem. 2024, 20, 2608–2634, doi:10.3762/bjoc.20.220

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Published 16 Oct 2024

Anion-dependent ion-pairing assemblies of triazatriangulenium cation that interferes with stacking structures

  • Yohei Haketa,
  • Takuma Matsuda and
  • Hiromitsu Maeda

Beilstein J. Org. Chem. 2024, 20, 2567–2576, doi:10.3762/bjoc.20.215

Graphical Abstract
  • (Figures S22–25 in Supporting Information File 1) [31]. The absorption band at 524 nm was blue-shifted by 4 nm compared to that of N-phenyl-substituted 1b+-BF4− [15]. This can be ascribed to the lesser conjugation of the core TATA+ unit with the introduced 2,6-dimethylphenyl moieties owing to the more
  • ) packing structures and (ii) enlarged views for the columnar structures. In (i), cation and anion are represented in cyan and magenta colors, respectively. In (ii), brown, pink, yellow, blue, yellow green, orange, and green (spherical) refer to carbon, hydrogen, boron, nitrogen, fluorine, phosphorus, and
  • chlorine, respectively. Hirshfeld surface analysis mapped with dnorm of closely contacted two 2+ in (a) 2+-BF4− and (b) 2+-PF6−. Atom color code: brown, pink, and blue refer to carbon, hydrogen, and nitrogen, respectively. Hirshfeld surface analysis mapped with dnorm of closely contacted ion pairs: (a) 2
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Published 10 Oct 2024

A review of recent advances in electrochemical and photoelectrochemical late-stage functionalization classified by anodic oxidation, cathodic reduction, and paired electrolysis

  • Nian Li,
  • Ruzal Sitdikov,
  • Ajit Prabhakar Kale,
  • Joost Steverlynck,
  • Bo Li and
  • Magnus Rueping

Beilstein J. Org. Chem. 2024, 20, 2500–2566, doi:10.3762/bjoc.20.214

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  • in the late functionalization of complex drug molecules. Due to the versatility of the azide group, the direct C(sp3)–H azidation is an extremely valuable transformation. Lei and coworkers achieved this transformation using electrochemistry upon irradiation with blue LEDs [69]. Under photoelectric
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Published 09 Oct 2024

Photoredox-catalyzed intramolecular nucleophilic amidation of alkenes with β-lactams

  • Valentina Giraldi,
  • Giandomenico Magagnano,
  • Daria Giacomini,
  • Pier Giorgio Cozzi and
  • Andrea Gualandi

Beilstein J. Org. Chem. 2024, 20, 2461–2468, doi:10.3762/bjoc.20.210

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  • reaction was carried out in DCM with acridinium PC IV (5 mol %), 50 mol % of PhSSPh as HAT catalyst, and lutidine (50 mol %) as the base. Upon 72 hours of irradiation with a blue light at 456 nm, the product 11c was obtained in a satisfactory yield as a mixture of diastereoisomers in a 1.4:1 ratio (Table 1
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Published 01 Oct 2024

Evaluating the halogen bonding strength of a iodoloisoxazolium(III) salt

  • Dominik L. Reinhard,
  • Anna Schmidt,
  • Marc Sons,
  • Julian Wolf,
  • Elric Engelage and
  • Stefan M. Huber

Beilstein J. Org. Chem. 2024, 20, 2401–2407, doi:10.3762/bjoc.20.204

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  • ). Halogen bonding dimer found in the crystal structure of 7Br. Ellipsoids are shown at 50% probability (carbon: grey, nitrogen: blue, oxygen: red, bromine: orange, iodine: purple) and hydrogen atoms are shown in standard ball-and-stick model (white). Halogen and hydrogen bonding is indicated dashed. 1H NMR
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Published 23 Sep 2024

Improved deconvolution of natural products’ protein targets using diagnostic ions from chemical proteomics linkers

  • Andreas Wiest and
  • Pavel Kielkowski

Beilstein J. Org. Chem. 2024, 20, 2323–2341, doi:10.3762/bjoc.20.199

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  • field have the potential to facilitate this advancement. Overall chemical proteomics strategy to identify protein targets of natural products (NPs) and similar active small compounds. The example protein (blue) is an AlphaFold v2.0-generated prediction of bovine serum albumin (BSA) [23][24]. A) Design
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Published 12 Sep 2024

Hydrogen-bond activation enables aziridination of unactivated olefins with simple iminoiodinanes

  • Phong Thai,
  • Lauv Patel,
  • Diyasha Manna and
  • David C. Powers

Beilstein J. Org. Chem. 2024, 20, 2305–2312, doi:10.3762/bjoc.20.197

Graphical Abstract
  • (denoted by asterisk *) of HFIP in the presence of iminoiodinane 2c suggesting hydrogen bonding observed in 1H NMR spectra (CD3CN) of: 8.0 mM 2c with no HFIP (blue line), 8.0 mM 2c with 32 mM HFIP (green line), 4.0 mM of 4-(trifluoromethyl)benzenesulfonamide with 32 mM HFIP (purple line), only 32 mM HFIP
  • (red line). b) Cyclic voltammogram of iminoiodinane 2c (8.0 mM) with varying amounts of HFIP in 5.0 mL solution of MeCN (0.10 M TBABF4) under N2 atmosphere: 2c with no HFIP (black line); 2c with 5, 10, 15 µL HFIP (grey line); 2c with 25 µL HFIP (red line); only 25 µL (blue line). c) Diastereomeric
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Published 11 Sep 2024

Metal-free double azide addition to strained alkynes of an octadehydrodibenzo[12]annulene derivative with electron-withdrawing substituents

  • Naoki Takeda,
  • Shuichi Akasaka,
  • Susumu Kawauchi and
  • Tsuyoshi Michinobu

Beilstein J. Org. Chem. 2024, 20, 2234–2241, doi:10.3762/bjoc.20.191

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  • profiles (ΔG298 in kJ mol−1) calculated at the ωB97X-D/6-31G(d,p)/PCM (in CH2Cl2). Absorption (blue) and fluorescence (red) spectra of 6a (2 × 10−5 M) in CH2Cl2. (a) Crosslinking reaction of PVC-N3 (x = 0.11) with compound 5. (b,c) Strain-stress curves of PVC-N3 before (blue) and after (red) crosslinking
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Published 04 Sep 2024

Finding the most potent compounds using active learning on molecular pairs

  • Zachary Fralish and
  • Daniel Reker

Beilstein J. Org. Chem. 2024, 20, 2152–2162, doi:10.3762/bjoc.20.185

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  • shown in the inlet with a green bar while the times it ‘stays’ in the same cluster is shown with a light blue bar. Arrow gradient towards darker grey indicates increasing iteration number. Tree-based model navigation of chemical space. T-SNE of a representative dataset (CHEMBL232-1, Alpha-1b adrenergic
  • another is shown in the inlet with a green bar while the times it ‘stays’ in the same cluster is shown with a light blue bar. Arrow gradient towards darker grey indicates increasing iteration number. Supporting Information Supporting Information File 54: Supplementary figures and tables
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Published 27 Aug 2024

Efficacy of radical reactions of isocyanides with heteroatom radicals in organic synthesis

  • Akiya Ogawa and
  • Yuki Yamamoto

Beilstein J. Org. Chem. 2024, 20, 2114–2128, doi:10.3762/bjoc.20.182

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  • quinoxaline synthesis was reported to proceed by irradiation with visible light in the presence of dibenzylamine ((PhCH2)2NH, MeCN, rt, blue LED) [64]. This reaction involves a visible-light-induced single electron transfer (SET) process. An efficient radical cascade cyclization has also been reported, in
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Published 26 Aug 2024

Multicomponent syntheses of pyrazoles via (3 + 2)-cyclocondensation and (3 + 2)-cycloaddition key steps

  • Ignaz Betcke,
  • Alissa C. Götzinger,
  • Maryna M. Kornet and
  • Thomas J. J. Müller

Beilstein J. Org. Chem. 2024, 20, 2024–2077, doi:10.3762/bjoc.20.178

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  • synthesized 4 halopyrazoles 111 and their Suzuki products 110 fluoresce blue in solution and have quantum yields of 29–72 % (Scheme 40) [137]. The Suzuki coupling can also be used for the functionalization of pyrazoles. For this purpose, p-bromo-substituted terminal alkynes 112, acyl chlorides 114, and
  • pathway enables the synthesis of 3,5-bis(biphenyl)-1-methyl pyrazole. To stabilize the catalyst, additional triphenylphosphane is added as a ligand during the Suzuki coupling. The resulting products fluoresce blue, with the five biaryl-substituted derivatives 113 showing the highest quantum yields of up
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Published 16 Aug 2024

Understanding X-ray-induced isomerisation in photoswitchable surfactant assemblies

  • Beatrice E. Jones,
  • Camille Blayo,
  • Jake L. Greenfield,
  • Matthew J. Fuchter,
  • Nathan Cowieson and
  • Rachel C. Evans

Beilstein J. Org. Chem. 2024, 20, 2005–2015, doi:10.3762/bjoc.20.176

Graphical Abstract
  • ) that contains mostly Z isomers. This can be reversed using blue light or heat in a process that is stable over many cycles [7]. Isomerisation of azobenzene leads to a change in its conformation and polarity which, when combined into a surfactant molecule, modifies the resulting molecular geometry and
  • on their own and in mixed micelles with lipids, on irradiation with either UV or blue light [21][22]. In addition, Ober et al. showed that in-situ UV irradiation stimulates a steady decrease in bilayer thickness for vesicles formed using Azo-modified phosphatidylcholine lipids, due to the shorter
  • pattern to that of the native, E isomer (Figure 2). Changes occur immediately, after 1 s of X-ray exposure, and saturate after ca. 5 s. The changes are comparable to those observed on Z–E isomerisation induced using blue (460 nm) light or heating to 55 °C but occur at a much faster rate (Figure S2
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Published 14 Aug 2024
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